CN219185890U - Device for extracting astaxanthin from haematococcus pluvialis - Google Patents

Device for extracting astaxanthin from haematococcus pluvialis Download PDF

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CN219185890U
CN219185890U CN202221473570.9U CN202221473570U CN219185890U CN 219185890 U CN219185890 U CN 219185890U CN 202221473570 U CN202221473570 U CN 202221473570U CN 219185890 U CN219185890 U CN 219185890U
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haematococcus pluvialis
astaxanthin
finished product
product storage
vacuum
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吴君石
弭永利
解鹏
吴向东
陈璨然
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Ailirong Chemical Technology Huizhou Co ltd
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Ailirong Chemical Technology Huizhou Co ltd
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    • Y02P20/54Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids

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Abstract

The utility model discloses a device for extracting astaxanthin from haematococcus pluvialis, which comprises a raw material storage mechanism, a vacuum low-temperature freeze drying mechanism, a high-pressure homogenizing mechanism, a supercritical extraction mechanism and a finished product storage mechanism which are sequentially communicated; wherein, supercritical carbon dioxide fluid is used as extraction solvent in the supercritical extraction mechanism. According to the utility model, the haematococcus pluvialis is subjected to vacuum freeze drying by the vacuum low-temperature freeze drying mechanism, so that the haematococcus pluvialis is frozen into a solid state in a vacuum environment, the cell wall structure of the haematococcus pluvialis is embrittled, and meanwhile, the cell wall surface of the haematococcus pluvialis forms a porous structure, so that the haematococcus pluvialis is subjected to cell wall breaking and mixing homogenization by the subsequent high-pressure homogenizing mechanism, and the risk of denaturation and inactivation of astaxanthin products at high temperature is effectively avoided.

Description

Device for extracting astaxanthin from haematococcus pluvialis
Technical Field
The utility model relates to the technical field of astaxanthin extraction, in particular to a device for extracting astaxanthin from haematococcus pluvialis.
Background
Astaxanthin is a main carotenoid component in aquatic organisms in nature and has important significance for the life activities of the aquatic organisms. Like most animals, human beings cannot synthesize carotenoid substances in vivo, but can only obtain the carotenoid substances through food intake, and the astaxanthin is contained in aquatic products such as shrimps, crabs, certain cold water fishes and the like, so that the carotenoid substances become animal sources for supplementing the carotenoid. Astaxanthin is a carotene in an oxidation state, and researches show that the astaxanthin has the antioxidant capacity which is 500 times that of vitamin E and more than 11 times that of carotene, and has obvious effects of resisting oxidation and eliminating active singlet oxygen.
Haematococcus pluvialis is a special fresh water unicellular green algae, can accumulate a large amount of carotenoid under specific conditions, and has the content of 1.5% of the dry weight of cells. In the current industry, the method for extracting astaxanthin from haematococcus pluvialis mainly adopts a chemical solvent extraction method, and the extractant mainly adopts methanol, ethanol, acetone, chloroform and the like. Meanwhile, in order to improve the extraction efficiency of the astaxanthin, the haematococcus pluvialis is subjected to pretreatment such as crushing or wall breaking before the astaxanthin is industrially extracted, and the treatment method is generally a mechanical wall breaking mode such as crushing by a bead mill. However, the organic solvent used in the extraction has certain toxicity, the extraction process is easy to explode, and the organic solvent residues in the extract are easy to cause harm to human bodies. The mechanical wall breaking modes such as the wall breaking of the bead mill have the defects of long wall breaking time, low wall breaking rate, large noise pollution and the like, and the temperature rising phenomenon exists in the mechanical treatment process, so that astaxanthin is easy to inactivate and the active components are reduced.
Disclosure of Invention
Aiming at the defects of the prior art, the utility model provides a device for extracting astaxanthin from haematococcus pluvialis.
The utility model discloses a device for extracting astaxanthin from haematococcus pluvialis, which comprises a raw material storage mechanism, a vacuum low-temperature freeze drying mechanism, a high-pressure homogenizing mechanism, a supercritical extraction mechanism and a finished product storage mechanism which are sequentially communicated; wherein, supercritical carbon dioxide fluid is used as extraction solvent in the supercritical extraction mechanism.
According to an embodiment of the present utility model, the device further comprises a semi-finished product storage mechanism, and the high-pressure homogenizing mechanism, the semi-finished product storage mechanism and the supercritical extraction mechanism are sequentially communicated.
According to an embodiment of the utility model, the device further comprises a drying and filtering mechanism, and the high-pressure homogenizing mechanism is communicated with the semi-finished product storage mechanism through the drying and filtering mechanism.
According to an embodiment of the utility model, it further comprises a low temperature freezing mechanism, through which the semi-finished product storage mechanism is in communication with the high pressure homogenizing mechanism.
According to an embodiment of the utility model, it further comprises a granulation mechanism; the semi-finished product storage mechanism, the granulating mechanism and the supercritical extraction mechanism are communicated in sequence.
According to one embodiment of the present utility model, the raw material storage mechanism, the vacuum low-temperature freeze-drying mechanism, the high-pressure homogenizing mechanism, the semi-finished product storage mechanism, the granulating mechanism, the supercritical extraction mechanism and the finished product storage mechanism are sequentially arranged at intervals.
According to one embodiment of the utility model, the vacuum cryogenic freeze-drying mechanism is a vacuum cryogenic freeze-dryer.
According to one embodiment of the utility model, the high-pressure homogenizing mechanism is a high-pressure homogenizer.
According to an embodiment of the present utility model, the cryogenic refrigeration mechanism is a cryogenic refrigeration compartment.
According to one embodiment of the present utility model, the supercritical extraction mechanism is a supercritical extractor.
Compared with the prior art, the vacuum freeze-drying mechanism is used for vacuum freeze-drying the haematococcus pluvialis, so that the haematococcus pluvialis is frozen into a solid state in a vacuum environment, the cell wall structure of the haematococcus pluvialis is embrittled, and meanwhile, the cell wall surface of the haematococcus pluvialis forms a porous structure, so that the haematococcus pluvialis is subjected to cell wall breaking and mixed homogenization by the subsequent high-pressure homogenizing mechanism, and the risk of denaturation and inactivation of astaxanthin products at high temperature is effectively avoided. In addition, the supercritical extraction mechanism adopts supercritical carbon dioxide fluid as an extraction solvent to extract astaxanthin in haematococcus pluvialis, so that the use of an organic solvent with certain toxicity is avoided, the astaxanthin is extracted in a green and environment-friendly pollution-free mode, and the food safety and the pure naturalness of the end product are ensured.
Drawings
The accompanying drawings, which are included to provide a further understanding of the application and are incorporated in and constitute a part of this application, illustrate embodiments of the application and together with the description serve to explain the application and do not constitute an undue limitation to the application. In the drawings:
FIG. 1 is a schematic diagram showing the structure of an apparatus for extracting astaxanthin from Haematococcus pluvialis in an embodiment;
FIG. 2 is a schematic diagram of a material storage mechanism according to an embodiment;
FIG. 3 is a comparative table showing the results of the detection of astaxanthin oil concentrated extract products in the examples.
Detailed Description
Various embodiments of the utility model are disclosed in the following drawings, in which details of the practice are set forth in the following description for the purpose of clarity. However, it should be understood that these practical details are not to be taken as limiting the utility model. That is, in some embodiments of the utility model, these practical details are unnecessary. Moreover, for the purpose of simplifying the drawings, some conventional structures and components are shown in the drawings in a simplified schematic manner.
In addition, the descriptions of the "first," "second," and the like, herein are for descriptive purposes only and are not intended to be specifically construed as order or sequence, nor are they intended to limit the utility model solely for distinguishing between components or operations described in the same technical term, but are not to be construed as indicating or implying any relative importance or order of such features. Thus, a feature defining "a first" or "a second" may explicitly or implicitly include at least one such feature. In addition, the technical solutions of the embodiments may be combined with each other, but it is necessary to base that the technical solutions can be realized by those skilled in the art, and when the technical solutions are contradictory or cannot be realized, the combination of the technical solutions should be considered to be absent and not within the scope of protection claimed in the present utility model.
Referring to fig. 1, fig. 1 is a schematic diagram showing the structure of an apparatus for extracting astaxanthin from haematococcus pluvialis according to an embodiment. The device for extracting astaxanthin from haematococcus pluvialis in the embodiment comprises a raw material storage mechanism 1, a vacuum low-temperature freeze drying mechanism 2, a high-pressure homogenizing mechanism 3, a supercritical extraction mechanism 4 and a finished product storage mechanism 5 which are sequentially communicated; wherein, supercritical carbon dioxide fluid is used as extraction solvent by the supercritical extraction mechanism 4.
The haematococcus pluvialis is subjected to vacuum freeze-drying through the vacuum low-temperature freeze-drying mechanism 2, so that the haematococcus pluvialis is frozen into a solid state in a vacuum environment, the cell wall structure of the haematococcus pluvialis is embrittled, and meanwhile, the cell wall surface of the haematococcus pluvialis forms a porous structure, so that the haematococcus pluvialis is subjected to cell wall breaking and mixing homogenization by the subsequent high-pressure homogenizing mechanism 3, and the risk of denaturation and inactivation of astaxanthin products at high temperature is effectively avoided. In addition, the supercritical extraction mechanism 4 adopts supercritical carbon dioxide fluid as an extraction solvent to extract astaxanthin in haematococcus pluvialis, so that the use of an organic solvent with certain toxicity is avoided, the astaxanthin is extracted in a green and pollution-free mode, and the food safety and the pure naturalness of the end product are ensured.
Referring back to fig. 1, further, the device for extracting astaxanthin from haematococcus pluvialis in this embodiment further includes a semi-finished product storage mechanism 6, and the high-pressure homogenizing mechanism 3, the semi-finished product storage mechanism 6 and the supercritical extraction mechanism 4 are sequentially connected. The haematococcus pluvialis after wall breaking and homogenizing is temporarily stored by a semi-finished product storage mechanism 6.
Referring back to fig. 1, further, the apparatus for extracting astaxanthin from haematococcus pluvialis in this embodiment further includes a drying and filtering mechanism 7. The high-pressure homogenizing mechanism 3 communicates with the semi-finished product storage mechanism 6 through a drying filter mechanism 7. The haematococcus pluvialis subjected to wall breaking and homogenization is filtered and dried by a drying and filtering mechanism 7 so as to facilitate the subsequent supercritical extraction.
Referring back to fig. 1, further, the apparatus for extracting astaxanthin from haematococcus pluvialis in the present embodiment further includes a low temperature freezing mechanism 8. The semi-finished product storage mechanism 6 is communicated with the high-pressure homogenizing mechanism 3 through the low-temperature freezing mechanism 8, and the wall-broken and homogenized haematococcus pluvialis stored in the semi-finished product storage mechanism 6 enters the high-pressure homogenizing mechanism 3 for secondary wall breaking and homogenizing after passing through the low-temperature freezing mechanism 8.
It can be understood that the wall breaking rate of the haematococcus pluvialis raw material after primary high-pressure homogenization is more than 90%, and in order to further improve the extraction efficiency of astaxanthin, the haematococcus pluvialis raw material is subjected to secondary high-pressure homogenization wall breaking treatment. In order to ensure the wall breaking effect, the low-temperature freezing mechanism 8 is arranged, so that the haematococcus pluvialis raw material liquid which is subjected to primary high-pressure homogenization by the high-pressure homogenizing mechanism 3 is subjected to a low-temperature freezing process, and the freeze-drying embrittlement process is performed again on the cell walls of haematococcus pluvialis cells which are not subjected to successful wall breaking in the haematococcus pluvialis raw material liquid, so that the high-pressure homogenization wall breaking can be performed better during secondary homogenization. The wall breaking rate of the haematococcus pluvialis raw material liquid after two times of high-pressure homogenization wall breaking can be more than 98%.
Referring again to fig. 1, further, the apparatus for extracting astaxanthin from haematococcus pluvialis in this embodiment further comprises a granulating mechanism 9. The semi-finished product storage mechanism 6, the granulation mechanism 9 and the supercritical extraction mechanism 4 are communicated in sequence. It will be appreciated that if the particles of haematococcus pluvialis raw material are too small, they will be dispersed by supercritical carbon dioxide during supercritical extraction, and astaxanthin oil cannot be extracted, and the haematococcus pluvialis raw material stored in the semi-finished product storage mechanism 6 is granulated by the granulating mechanism 9, so that the best extraction effect can be achieved during the subsequent supercritical extraction.
Referring back to fig. 1, in this embodiment, the raw material storage mechanism 1, the vacuum low-temperature freeze-drying mechanism 2, the high-pressure homogenizing mechanism 3, the semi-finished product storage mechanism 6, the granulating mechanism 9, the supercritical extraction mechanism 4 and the finished product storage mechanism 5 are sequentially arranged at intervals, so that the arrangement of each mechanism in the device for extracting astaxanthin from haematococcus pluvialis in this embodiment is standardized, and the smooth process of extracting astaxanthin from haematococcus pluvialis is ensured.
Referring to fig. 2 again, fig. 2 is a schematic structural diagram of a raw material storage mechanism in an embodiment. In this embodiment, the raw material storage mechanism 1 includes a raw material tank 11, a raw material stirring assembly 12, and a raw material tank holder 13. The raw material storage tank 11 is in a tank shape, a space for storing haematococcus pluvialis raw materials is formed in the raw material storage tank, a feed inlet 111 is formed in the upper end of the raw material storage tank 11 so that the haematococcus pluvialis raw materials can be conveniently added, and a discharge outlet 112 is formed in the lower end of the raw material storage tank 11. The raw material stirring assembly 12 comprises a stirring driver 121, a stirring rod 122 and stirring blades 123, wherein the stirring driver 121 is arranged on the outer wall of the upper end of the raw material storage tank 11, the stirring blades 123 are located in the inner space of the raw material storage tank 11 and are close to the lower end of the raw material storage tank 11, one end of the stirring rod 122 is connected with the driving end of the stirring driver 121, the other end of the stirring rod 122 extends into the raw material storage tank 11 and is connected with the stirring blades 123, the stirring driver 121 drives the stirring rod 122 to rotate so as to drive the stirring blades 123 to rotate, the stirring blades 123 stir the haematococcus pluvialis raw material in the raw material storage tank 11, condensation of the haematococcus pluvialis raw material is avoided, the haematococcus pluvialis raw material can flow out from the discharge hole 112 of the raw material storage tank 11, and subsequent pipeline transmission of the haematococcus pluvialis raw material is facilitated, the stirrer 121 in the embodiment can adopt a motor, and the stirring blades 123 can adopt a multi-layer blade structure so as to ensure the stirring effect. The lower extreme of raw materials storage tank 11 is located on the raw materials jar support 13, carries out unsettled support to raw materials storage tank 11 through raw materials jar support 13 to the layout of conveying pipeline 100 of being convenient for. One end of the material conveying pipeline 100 is communicated with a material outlet 112, the other end is communicated with the vacuum low-temperature freeze drying mechanism 2, and the material conveying pipeline 100 is provided with a control valve 101 and a pneumatic diaphragm pump 102. The haematococcus pluvialis raw material added into the raw material storage tank 11 flows into the material conveying pipeline 100 through the material outlet 112 under the action of gravity, and is pumped into the vacuum low-temperature freeze-drying mechanism 2 under the action of the pneumatic diaphragm pump 102. The control valve 101 is used for controlling the on-off of the feed pipeline 100. Preferably, the material conveying pipeline 100 is further provided with a sampling valve 103, the sampling valve 103 is located between the material outlet 112 and the control valve 101, and the sampling valve 103 is provided with a sampling port so as to facilitate sampling detection of haematococcus pluvialis raw materials. Preferably, the material conveying pipeline 100 is further provided with a material discharging valve 104, the material discharging valve 104 is located between the sampling valve 103 and the control valve 101, the material discharging valve 104 is provided with a material discharging port, and the material discharging valve 104 is arranged so as to facilitate the material discharging of haematococcus pluvialis raw materials.
Preferably, the vacuum low-temperature freeze-drying mechanism 2 is a vacuum low-temperature freeze-drying machine, which can perform vacuum low-temperature freeze-drying treatment on haematococcus pluvialis raw materials, and uses vacuum and low-temperature environment to freeze the haematococcus pluvialis raw materials into a solid state, and the cell wall surface of haematococcus pluvialis can also form a porous structure while embrittling the cell wall structure of haematococcus pluvialis so as to facilitate subsequent wall breaking and homogenization. In the embodiment, the vacuum environment is air pressure less than 10 Pa, the low-temperature environment is at a temperature between-50 ℃ and-70 ℃, the ultralow temperature can cause the cell wall surface of haematococcus pluvialis to freeze and embrittle under the vacuum and ultralow-temperature environment, the vacuum environment can cause the moisture of the cell wall of haematococcus pluvialis not to sublimate directly into a gaseous state from a liquid state, and the moisture penetrates through the cell wall subjected to ultralow-temperature freeze and embrittle during sublimation, so that a porous structure is formed on the outer surface of the cell wall. Compared with a single low-temperature freezing environment, the method has the advantages that the purposes of embrittling cell walls of haematococcus pluvialis and forming a porous structure can be achieved simultaneously by combining low-temperature freezing in a vacuum environment, and the subsequent wall breaking and homogenizing of haematococcus pluvialis are facilitated. In specific applications, the existing vacuum low-temperature freeze dryer capable of achieving vacuum, low-temperature and drying functions can be adopted, and details are omitted here.
Further, the high-pressure homogenizing mechanism 3 is a high-pressure homogenizer. The haematococcus pluvialis raw material subjected to vacuum low-temperature freeze drying enters a high-pressure homogenizer for wall breaking operation, and the high-pressure homogenizer forms a high-pressure and extrusion-grinding environment under the combined action of mechanical action and hydrodynamic effect, so that haematococcus pluvialis is sheared under the action of high pressure and strong impact and is expanded under the action of decompression, and finally the purposes of breaking cell walls and mixing and homogenizing are achieved. In specific applications, existing high pressure homogenizers may be employed. Specifically, the haematococcus pluvialis material subjected to vacuum freeze drying passes through a gap with the width smaller than 0.1mm under the action of high pressure of 20-100 MPa, so that the haematococcus pluvialis material forms a high-speed state of 100-200 m/s, in the state, haematococcus pluvialis cells are subjected to strong shearing force, meanwhile, as cellular particles in the haematococcus pluvialis material can collide with an organism at high speed and the swirling action of the raw material liquid is generated when the raw material liquid passes through a liquid drop homogenizing valve, the cell walls of the haematococcus pluvialis after embrittlement are thoroughly disintegrated, and the cellular liquid containing astaxanthin is released, so that the purpose of wall breaking and homogenizing is achieved.
Preferably, the drying and filtering mechanism 7 is a drying and filtering bin, which performs drying and filtering on the haematococcus pluvialis raw material homogenized under high pressure, and in specific application, an existing drying and filtering bin can be adopted, and no description is repeated here.
Preferably, the semi-finished product storage mechanism 6 is used for storing the dried and filtered haematococcus pluvialis materials, and the structure and the action principle of the semi-finished product storage mechanism 6 are similar to those of the raw material storage mechanism 1, and are not repeated here. Preferably, the semi-finished product storage mechanism 6 is provided with a backflow pipeline piece 61, the semi-finished product storage mechanism 6 is communicated with the low-temperature freezing mechanism 8 through the backflow pipeline piece 61, and haematococcus pluvialis materials which are subjected to primary wall breaking and homogenization in the semi-finished product storage mechanism 6 are backflow to the low-temperature freezing mechanism 8 through the backflow pipeline piece 61 for secondary low-temperature freezing. In this embodiment, the return pipe 61 is a pipe, a valve, and a pneumatic diaphragm pump, and the low-temperature freezing mechanism 8 is a low-temperature freezing chamber. After the haematococcus pluvialis materials subjected to primary wall breaking and homogenization pass through a low-temperature freezing bin, the cell walls of haematococcus pluvialis cells which are not subjected to successful wall breaking are subjected to a freeze drying embrittlement process again, and then enter a high-pressure homogenizing mechanism 3 for secondary wall breaking and homogenization.
Preferably, the haematococcus pluvialis material subjected to secondary wall breaking and homogenization enters a granulating mechanism 9 for granulating, and the granulating mechanism 9 in the embodiment can adopt a granulator. The haematococcus pluvialis material with the secondary wall breaking and homogenizing is subjected to vacuum dehydration in a granulator, and then is prepared into haematococcus pluvialis particles with the particle size of 40 meshes in a spiral extrusion granulating mode, so that the subsequent supercritical carbon dioxide extraction process is facilitated.
Referring to fig. 3 again, fig. 3 is a table showing comparison of detection results of astaxanthin oil concentrated extract products in the embodiment, wherein the detection basis is a liquid chromatography for measuring astaxanthin in haematococcus rhodochrous of GB/T31520-2015, the source of raw materials is artificial haematococcus pluvialis produced by malaysia, wherein the astaxanthin content is 1.5% -3.0%, sample No. 1 is an astaxanthin concentrate product after one high-pressure homogenizing wall breaking, sample No. 2 is an astaxanthin concentrate product after two high-pressure homogenizing wall breaking, sample No. 3 is a 5% astaxanthin concentrate standard, and further, the supercritical extraction mechanism 4 is a supercritical extractor. The haematococcus pluvialis particles are added into a supercritical extractor, and astaxanthin in haematococcus pluvialis is extracted by using supercritical carbon dioxide fluid as an extraction solvent. The supercritical extractor mainly comprises three extraction kettles and three separation kettles, wherein the highest design pressure in the system is 75MPa, the working pressure is 35-70 MPa, the highest temperature is 80 ℃, and the working temperature is 30-60 ℃. The design pressure and the working pressure of the whole device follow the related design requirements and specifications of the national high-pressure container and parts, and the design of the reaction kettle body used in the whole system is carried out according to the reference standards of GB 150.1-150.4-2011 and GB 4732. Meanwhile, the supercritical extraction machine is also provided with a reliable overvoltage protection system and a safety interlocking device, so that absolute safety of equipment is guaranteed. The sealing ring of each extraction kettle is made of high-pressure, high-temperature and corrosion resistant materials, and can be used for a long time without replacing the sealing ring. The sealing degree is quite reliable, the reliability and stability of the quality of the astaxanthin extracted from the product are guaranteed, and the astaxanthin extracted from the product can be easily opened and closed, so that the operation is convenient. The charging barrel sealing ring can effectively form a seal with the inner wall of the kettle body. The two sealing rings are directly arranged on the plug and the kettle body, can not be swelled in high-pressure carbon dioxide, and are not required to be taken out when materials are replaced every time, so that the kettle is convenient and safe. In order to increase the reliability of the system and avoid human errors, the operation of each device in the whole system is completed by a central control system, and the intelligent device is realized and the safety of the supercritical extractor is improved through the real-time monitoring of the pressure and the temperature and the automatic operation of the device.
In conclusion, the haematococcus pluvialis is subjected to vacuum freeze drying through the vacuum low-temperature freeze drying mechanism, so that the haematococcus pluvialis is frozen into a solid state in a vacuum environment, the cell wall structure of the haematococcus pluvialis is embrittled, and meanwhile, the cell wall surface of the haematococcus pluvialis forms a porous structure, so that the haematococcus pluvialis is subjected to cell wall breaking and mixed homogenization through the subsequent high-pressure homogenizing mechanism, and the wall breaking rate of the haematococcus pluvialis raw material liquid can be more than 98% through the secondary circulation wall breaking of the high-pressure homogenizing machine, and the risk of denaturation and inactivation of astaxanthin products at high temperature is effectively avoided. In addition, the supercritical extraction mechanism adopts supercritical carbon dioxide fluid as an extraction solvent to extract astaxanthin in haematococcus pluvialis, so that the use of an organic solvent with certain toxicity is avoided, the astaxanthin is extracted in a green and environment-friendly pollution-free mode, and the food safety and the pure naturalness of the end product are ensured.
The foregoing description is only illustrative of the utility model and is not to be construed as limiting the utility model. Various modifications and variations of the present utility model will be apparent to those skilled in the art. Any modification, equivalent replacement, improvement, or the like, which is within the spirit and principles of the present utility model, should be included in the scope of the claims of the present utility model.

Claims (10)

1. The device for extracting astaxanthin from haematococcus pluvialis is characterized by comprising a raw material storage mechanism, a vacuum low-temperature freeze-drying mechanism, a high-pressure homogenizing mechanism, a supercritical extraction mechanism and a finished product storage mechanism which are sequentially communicated; wherein, supercritical carbon dioxide fluid is adopted as extraction solvent by the supercritical extraction mechanism.
2. The apparatus for extracting astaxanthin from haematococcus pluvialis according to claim 1, further comprising a semi-finished product storage mechanism, wherein said high pressure homogenizing mechanism, said semi-finished product storage mechanism and said supercritical extraction mechanism are in communication in this order.
3. The apparatus for extracting astaxanthin from haematococcus pluvialis according to claim 2, further comprising a dry filter mechanism through which said high pressure homogenizing mechanism communicates with said semi-finished product storage mechanism.
4. The apparatus for extracting astaxanthin from haematococcus pluvialis according to claim 3, further comprising a low temperature freezing mechanism through which said semi-finished product storage mechanism communicates with said high pressure homogenizing mechanism.
5. The apparatus for extracting astaxanthin from haematococcus pluvialis according to claim 2, further comprising a granulating mechanism; the semi-finished product storage mechanism, the granulating mechanism and the supercritical extraction mechanism are sequentially communicated.
6. The apparatus for extracting astaxanthin from haematococcus pluvialis according to claim 5, wherein said raw material storage means, said vacuum low-temperature freeze-drying means, said high-pressure homogenizing means, said semi-finished product storage means, said granulating means, said supercritical extraction means and said finished product storage means are arranged at a predetermined interval in this order.
7. The apparatus for extracting astaxanthin from haematococcus pluvialis of claim 1, wherein said vacuum cryogenic freeze-drying mechanism is a vacuum cryogenic freeze-dryer.
8. The apparatus for extracting astaxanthin from haematococcus pluvialis as defined in claim 4, wherein said high pressure homogenizing mechanism is a high pressure homogenizer.
9. The apparatus for extracting astaxanthin from haematococcus pluvialis according to claim 8, wherein said low temperature freezing mechanism is a low temperature freezing chamber.
10. The apparatus for extracting astaxanthin from haematococcus pluvialis according to claim 1, wherein the supercritical extraction mechanism is a supercritical extractor.
CN202221473570.9U 2022-06-13 2022-06-13 Device for extracting astaxanthin from haematococcus pluvialis Active CN219185890U (en)

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