CN218923845U - Anthocyanin's separation and purification device - Google Patents
Anthocyanin's separation and purification device Download PDFInfo
- Publication number
- CN218923845U CN218923845U CN202222952445.2U CN202222952445U CN218923845U CN 218923845 U CN218923845 U CN 218923845U CN 202222952445 U CN202222952445 U CN 202222952445U CN 218923845 U CN218923845 U CN 218923845U
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- China
- Prior art keywords
- anthocyanin
- beaker
- constant temperature
- liquid pump
- filter
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- 229930002877 anthocyanin Natural products 0.000 title claims abstract description 47
- 235000010208 anthocyanin Nutrition 0.000 title claims abstract description 47
- 239000004410 anthocyanin Substances 0.000 title claims abstract description 47
- 150000004636 anthocyanins Chemical class 0.000 title claims abstract description 47
- 238000000746 purification Methods 0.000 title claims abstract description 20
- 238000000926 separation method Methods 0.000 title claims abstract description 15
- 239000007788 liquid Substances 0.000 claims abstract description 36
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000002904 solvent Substances 0.000 claims description 10
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 claims description 9
- 238000012546 transfer Methods 0.000 claims description 9
- 238000001914 filtration Methods 0.000 claims description 3
- 239000011148 porous material Substances 0.000 claims description 2
- 230000000149 penetrating effect Effects 0.000 claims 2
- 239000002994 raw material Substances 0.000 abstract description 12
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract description 11
- 239000011347 resin Substances 0.000 abstract description 11
- 229920005989 resin Polymers 0.000 abstract description 11
- 239000000243 solution Substances 0.000 abstract description 10
- 239000007864 aqueous solution Substances 0.000 abstract description 7
- 238000001179 sorption measurement Methods 0.000 abstract description 4
- 239000012535 impurity Substances 0.000 abstract description 3
- 239000012528 membrane Substances 0.000 abstract description 3
- 238000000108 ultra-filtration Methods 0.000 abstract description 3
- 239000003125 aqueous solvent Substances 0.000 abstract 1
- 230000005540 biological transmission Effects 0.000 description 6
- 230000010355 oscillation Effects 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 238000009423 ventilation Methods 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 229930003935 flavonoid Natural products 0.000 description 1
- -1 flavonoid compounds Chemical class 0.000 description 1
- 235000017173 flavonoids Nutrition 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 231100000956 nontoxicity Toxicity 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
Images
Classifications
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
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- Extraction Or Liquid Replacement (AREA)
Abstract
The utility model discloses a separation and purification device for anthocyanin, which belongs to the technical field of separation and purification and comprises a crushing stirrer, wherein raw materials containing anthocyanin are placed in the crushing stirrer, warm water is added in the crushing stirrer to soak the raw materials, the anthocyanin in the raw materials is separated through an aqueous solvent, an obtained aqueous solution is filtered through an ultrafiltration membrane, impurities in the aqueous solution are separated from liquid, the filtered aqueous solution is sucked by a first liquid pump and poured into a first beaker, a filter is placed in the first beaker, macroporous resin is placed in the filter to adsorb the anthocyanin, a first constant-temperature oscillator is arranged at the bottom of the first beaker to accelerate the adsorption of the anthocyanin by the macroporous resin, the macroporous resin after the adsorption is poured into a second beaker on the right, an ethanol solution is added in the second beaker, and then the filter is oscillated, so that the anthocyanin after the purification can be obtained.
Description
Technical Field
The utility model relates to the technical field of separation and purification, in particular to a separation and purification device for anthocyanin.
Background
Anthocyanin belongs to flavonoid compounds, is a water-soluble natural food pigment with bright color, safety, no toxicity, nutrition and health care, and has wide development and application prospect. Research shows that the natural anthocyanin extracted from the plant has the advantages of low cost, good safety and the like, and becomes a hot spot for people to study increasingly.
In the process of producing and extracting anthocyanin, raw materials containing anthocyanin are required to be stirred, crushed, separated and purified, and at present, equipment for extracting anthocyanin is huge, various in equipment, high in price and limited in popularization.
Disclosure of Invention
The utility model aims to provide a separation and purification device for anthocyanin, which solves the problems of huge equipment, various equipment types, high price and limited popularization in the prior art.
In order to achieve the above purpose, the present utility model provides the following technical solutions: including the thermostated container, the operation panel is installed to the top of thermostated container, first constant temperature oscillator and second constant temperature oscillator are installed to the internally mounted of operation panel, first beaker has been placed to the top of first constant temperature oscillator, the switch is installed to the top of first beaker is provided with the bottom of water guide pipe and water guide pipe, the second constant temperature oscillator is installed the right side of first constant temperature oscillator, the second beaker has been placed to the top of second constant temperature oscillator, the top of second beaker is provided with the ethanol water pipe.
Preferably, the bottom of the incubator is connected with a support column, and the bottom of the support column is provided with a antiskid plate.
Preferably, the crushing mixer is installed to the top left end of thermostated container, the motor is installed in the left side of crushing mixer, the output shaft of motor has the transfer line, the transfer line runs through and installs the inside of crushing mixer, the bearing is installed at the inside right side center of crushing mixer, the transfer line links to each other with the bearing, the fixed surface of transfer line installs rotary blade, the feed inlet is installed at the top of crushing mixer.
Preferably, the bottom of smashing the mixer is installed the discharge gate, the internally mounted of discharge gate has the milipore filter, the bottom of discharge gate is connected with the liquid storage pot, the liquid storage pot is installed the inside bottom of thermostated container.
Preferably, the first liquid pump and the second liquid pump are installed to the inside right-hand member of thermostated container, the aqueduct of first liquid pump with the liquid storage pot links to each other, the aqueduct runs through to be installed the inside of operation panel, the left side of second liquid pump is connected with the solvent holding vessel, the ethanol water pipe with the solvent holding vessel links to each other, the ethanol water pipe runs through to be installed the inside of operation panel, the bottom of first liquid pump and second liquid pump is connected with the second bearing platform, the second bearing platform is installed the inside bottom of thermostated container.
Preferably, a filter is placed in the first beaker, one side of the filter is connected with a connecting rod, the top end of the connecting rod is provided with an anti-slip layer, the bottom of the filter is provided with a filter hole, and a ventilation pipeline is installed on the side face of the operating platform.
Compared with the prior art, the utility model has the beneficial effects that: this device is through at the internally mounted first constant temperature oscillator and the second constant temperature oscillator of operation panel, place the top at first constant temperature oscillator with first beaker, then place the filter in the inside of first beaker, place macroporous resin in the inside of filter, then pour into first beaker inside with the aqueous solution that contains anthocyanin that the stirring obtained, the solution impurity content that obtains at this moment is higher, adsorb anthocyanin through adding macroporous resin in the solution, improve the enrichment degree of anthocyanin, first constant temperature oscillator can accelerate macroporous resin and to the collection speed of anthocyanin, later take out the filter and put into the inside of second beaker, add ethanol and dissolve anthocyanin this moment, can obtain anthocyanin after the purification.
Drawings
FIG. 1 is a front view of an anthocyanin separation and purification device according to the present utility model;
FIG. 2 is a block diagram of a filter apparatus of the present utility model;
FIG. 3 is a top view of the filter device of the present utility model;
in the figure: 1 thermostated container, 2 support column, 3 antiskid ribbed tile, 4 crushing mixer, 5 motor, 6 transfer lines, 7 bearings, 8 rotary blade, 9 feed inlets, 10 first bearing platform, 11 discharge gates, 12 milipore filter, 13 liquid storage pot, 14 aqueduct, 141 ethanol water pipe, 15 first liquid pump, 16 second liquid pump, 17 solvent holding vessel, 18 second bearing platform, 19 operation panel, 20 switches, 21 first thermostated oscillator, 211 second thermostated oscillator, 22 first beaker, 222 second beaker, 23 filter, 24 connecting rod, 25 antiskid layer, 26 filtration pore, 27 air pipe.
Detailed Description
The following description of the embodiments of the present utility model will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present utility model, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the utility model without making any inventive effort, are intended to be within the scope of the utility model.
The utility model provides a separation and purification device for anthocyanin, which is characterized in that raw materials containing anthocyanin are crushed through a crushing stirrer, the anthocyanin is separated from the raw materials and is dissolved in warm water, the contact area between the anthocyanin and the warm water is increased, then an aqueous solution containing anthocyanin is placed in a first beaker, macroporous resin is placed in the first beaker, the anthocyanin is separated from the aqueous solution through high adsorptivity of the macroporous resin to organic matters, the aim of purification is achieved, a first constant-temperature oscillator is used for accelerating the adsorption speed, the macroporous resin is placed in a second beaker, and an ethanol solution is added, so that the anthocyanin after purification can be obtained through oscillation;
referring to fig. 1, the incubator 1 is used for keeping a suitable storage environment for anthocyanin, and meanwhile, a support column 2 connected with the bottom of the incubator 1 and a antiskid plate 3 arranged at the bottom of the support column are used for improving the support of the incubator 1, and in order to separate anthocyanin from raw materials, a crushing stirrer 4 is arranged on the left side of the top of the incubator 1, and anthocyanin in the raw materials is released through the crushing stirrer 4, so that the collection efficiency of anthocyanin can be improved; the crushing stirrer 4 comprises a motor 5, the motor 5 is arranged at the left side of the crushing stirrer 4, meanwhile, the output shaft of the motor 5 is connected with a transmission rod 6, the transmission rod 6 is arranged inside the crushing stirrer 4, the transmission rod 6 is driven to rotate by the power of the motor 5, meanwhile, a bearing 7 is arranged at the right end of the inner side of the crushing stirrer 4, the transmission rod 6 is connected with the bearing 7, the transmission rod 6 is convenient to rotate, a rotary blade 8 is arranged on the surface of the transmission rod 6 at equal distance and is used for crushing raw materials, meanwhile, a feed inlet 9 is arranged at the top of the crushing stirrer 4, the feed inlet 9 is convenient for throwing the extracted raw materials, meanwhile, hot water is also convenient to be added into the crushing stirrer 4, anthocyanin is convenient to dissolve in warm water, the solubility of anthocyanin is improved, after a period of stirring, the water containing anthocyanin is collected through a discharge port 11 connected with the bottom of the crushing stirrer 4, meanwhile, in order to prevent larger impurities from entering a solution, the influence on the purification of the anthocyanin is reduced, an ultrafiltration membrane 12 is arranged inside the discharge port, a part of the ultrafiltration membrane 12 is used for filtering a part of the raw materials, and then the filtered raw materials are poured into a tank 13 below the solution;
referring to fig. 1-2, a first liquid pump 15 and a second liquid pump 16 are installed at the right end inside the incubator 1, meanwhile, a water guide pipe 14 of the first liquid pump 15 is connected with a liquid storage tank 13, the second liquid pump 16 is connected with a solvent storage tank 17, meanwhile, a second bearing table 18 is installed at the bottom of the first liquid pump 15 and the second liquid pump 16, the second bearing table 18 is installed at the bottom end inside the incubator 1 and is used for fixedly supporting the two liquid pumps, a semi-closed operation table 19 is installed at the right end of the top of the incubator 1, a first constant temperature oscillator 21 and a second constant temperature oscillator 211 are installed on the operation table 19, the water guide pipe 14 of the first liquid pump 15 is fixedly installed above the first constant temperature oscillator 21, the flow rate of the water guide pipe is controlled through a switch 20, then the solution in the liquid storage tank 13 is poured into the interior of a first beaker 22 at the bottom, an ethanol water guide pipe 141 of the second liquid pump 16 is fixedly installed above the second constant temperature oven 211, an absolute ethanol solvent is placed in the solvent storage tank 17, and then the ethanol solvent is poured into the interior 222 of a second beaker at the bottom;
referring to fig. 2-3, in order to purify the anthocyanin solution in the liquid storage tank 13, a filter 23 is placed in the first beaker, a groove is formed in the filter 23, macroporous resin is placed in the groove, a connecting rod 24 is installed on the side edge of the filter 23, an anti-slip layer 25 is sleeved on the top of the connecting rod 24, the connecting rod 24 is installed to facilitate the removal of the filter 23, a filter hole 26 is formed in the bottom of the filter 23, a switch 20 of a water guide pipe 14 is opened, the solution in the liquid storage tank 13 is poured into the first beaker 22, the anthocyanin is adsorbed from the aqueous solution through the characteristic of the macroporous resin, a first constant-temperature oscillator 21 placed at the bottom is started to accelerate the adsorption speed, after a period of oscillation, the filter 23 is taken out and placed in the second beaker 22, then an ethanol water pipe 141 is opened to add an ethanol solvent, the anthocyanin is dissolved, and the purified anthocyanin is obtained, and a ventilation pipeline 27 is installed on the side surface of an operation table 19.
Although the utility model has been described hereinabove with reference to embodiments, various modifications thereof may be made and equivalents may be substituted for elements thereof without departing from the scope of the utility model. In particular, the features of the disclosed embodiments may be combined with each other in any manner so long as there is no structural conflict, and the exhaustive description of these combinations is not given in this specification merely for the sake of brevity and resource saving. Therefore, it is intended that the utility model not be limited to the particular embodiment disclosed, but that the utility model will include all embodiments falling within the scope of the appended claims.
Claims (6)
1. An anthocyanin separation and purification device is characterized in that: including oven (1), operation panel (19) are installed to the top of oven (1), first constant temperature oscillator (21) and second constant temperature oscillator (211) are installed to the internally mounted of operation panel (19), first beaker (22) have been placed to the top of first constant temperature oscillator (21), switch (20) are installed to the top of first beaker (22) being provided with aqueduct (14) and aqueduct (14)'s bottom, second constant temperature oscillator (211) are installed the right side of first constant temperature oscillator (21), second beaker (222) have been placed to the top of second constant temperature oscillator (211), the top of second beaker (222) is provided with ethanol water pipe (141).
2. The anthocyanin separation and purification device according to claim 1, wherein: the bottom of thermostated container (1) is connected with support column (2), antiskid ribbed tile (3) are installed to the bottom of support column (2).
3. The anthocyanin separation and purification device according to claim 2, wherein: crushing mixer (4) are installed to the top left end of thermostated container (1), motor (5) are installed in the left side of crushing mixer (4), the output shaft of motor (5) has transfer line (6), transfer line (6) run through and install the inside of crushing mixer (4), bearing (7) are installed at the inside right side center of crushing mixer (4), transfer line (6) link to each other with bearing (7), the fixed surface of transfer line (6) installs rotary blade (8), feed inlet (9) are installed at the top of crushing mixer (4).
4. A separation and purification apparatus for anthocyanin according to claim 3, wherein: the bottom of smashing mixer (4) is installed discharge gate (11), the internally mounted of discharge gate (11) has milipore filter (12), the bottom of discharge gate (11) is connected with reservoir (13), reservoir (13) are installed the inside bottom of thermostated container (1).
5. The anthocyanin separation and purification device of claim 4, wherein: the intelligent constant temperature box is characterized in that a first liquid pump (15) and a second liquid pump (16) are arranged at the right end of the inside of the constant temperature box (1), a water guide pipe (14) of the first liquid pump (15) is connected with a liquid storage tank (13), the other end of the first liquid pump is connected with the water guide pipe (14) in a penetrating mode, the inside of an operation table (19) is arranged in the second liquid pump (16), a solvent storage tank (17) is connected to the left side of the second liquid pump (16), an ethanol water pipe (141) is connected with the solvent storage tank (17), the ethanol water pipe (141) is installed in the operation table (19) in a penetrating mode, the bottoms of the first liquid pump (15) and the second liquid pump (16) are connected with a second bearing table (18), and the second bearing table (18) is installed at the bottom end of the inside of the constant temperature box (1).
6. The anthocyanin separation and purification device of claim 5, wherein: the filter (23) has been placed to the inside of first beaker (22), one side of filter (23) is connected with connecting rod (24), the top of connecting rod (24) is provided with anti-skidding layer (25), the bottom of filter (23) is provided with filtration pore (26), air pipe (27) are installed to the side of operation panel (19).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202222952445.2U CN218923845U (en) | 2022-11-07 | 2022-11-07 | Anthocyanin's separation and purification device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202222952445.2U CN218923845U (en) | 2022-11-07 | 2022-11-07 | Anthocyanin's separation and purification device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN218923845U true CN218923845U (en) | 2023-04-28 |
Family
ID=86093520
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202222952445.2U Active CN218923845U (en) | 2022-11-07 | 2022-11-07 | Anthocyanin's separation and purification device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN218923845U (en) |
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2022
- 2022-11-07 CN CN202222952445.2U patent/CN218923845U/en active Active
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