CN218853529U - Water separator - Google Patents

Water separator Download PDF

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Publication number
CN218853529U
CN218853529U CN202223431540.4U CN202223431540U CN218853529U CN 218853529 U CN218853529 U CN 218853529U CN 202223431540 U CN202223431540 U CN 202223431540U CN 218853529 U CN218853529 U CN 218853529U
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Prior art keywords
separator
recovery
tube
pipe
reaction
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CN202223431540.4U
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陈虎
王献
张敬彬
李玉生
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YOUCARE PHARMACEUTICAL GROUP ANHUI NATURAL PHARMACEUTICAL CO Ltd
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YOUCARE PHARMACEUTICAL GROUP ANHUI NATURAL PHARMACEUTICAL CO Ltd
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Abstract

The utility model discloses a water separator, which comprises a separation liquid storage component, a separator and a control component, wherein the separator is provided with an oil-water separation cavity and a separation liquid recovery cavity from top to bottom; the liquid separation pipe is integrally formed with the separator, and the oil phase separated from the oil-water separation cavity is introduced into the chaotropic recovery cavity through the liquid separation pipe; and the quick connection mounting seats are respectively arranged at two ends of the separator, and the separator is fixedly connected with the external reaction device through the quick connection mounting seats. The utility model discloses can realize effectively reducing the water knockout drum volume, improve the device wholeness to the simple installation has better stability.

Description

Water separator
Technical Field
The utility model relates to an oil-water separation technical field especially relates to a water knockout drum.
Background
The water separator is a common test device, is mainly used for esterification reaction, can separate water generated in a reaction system, continuously heats the reaction system, condenses an oil phase and a water phase after rising, and leads the oil phase exceeding the reserved volume back to the reaction system by utilizing the characteristics of water at the lower layer and oil at the upper layer through different oil-water densities.
But the volume of current water knockout drum is general great, and the device wholeness is poor, and stability is lower when leading to the use, is unfavorable for building with reaction unit. Therefore, a water separator is provided for solving the problems.
SUMMERY OF THE UTILITY MODEL
The utility model aims at providing a water knockout drum to solve the problem that above-mentioned prior art exists, can realize effectively reducing the water knockout drum volume, improve the device wholeness, and simple installation has better stability.
In order to achieve the above object, the utility model provides a following scheme: the utility model provides a water separator, which comprises,
the separation liquid storage assembly comprises a separator and a control element, wherein an oil-water separation cavity and a chaotropic recovery cavity are arranged in the separator from top to bottom, the control element is arranged on the separator, and the oil-water separation cavity is communicated or separated with the chaotropic recovery cavity through the control element;
the liquid separating pipe and the separator are integrally formed, and the oil phase separated from the oil-water separation cavity is introduced into the separation liquid recovery cavity through the liquid separating pipe;
and the quick connection mounting seats are respectively arranged at two ends of the separator, and the separator is fixedly connected with an external reaction device through the quick connection mounting seats.
Preferably, the separator includes by last reaction tube and the recovery tube that sets gradually down, the reaction tube with the recovery tube sets up on same axis, just the bottom of reaction tube stretches into the recovery tube with the recovery tube intercommunication, the control is located be close to on the reaction tube the recovery tube top sets up, the control with the reaction tube rotates to be connected, the reaction tube pass through the control with the recovery tube intercommunication or separate.
Preferably, the control part comprises a gate, one end of the gate penetrates through the reaction tube, the gate is rotatably connected with the reaction tube, a through hole is formed in the middle of the gate, the through hole is formed in the reaction tube, and the reaction tube is communicated with or separated from the recovery tube through the gate.
Preferably, divide the liquid pipe the reaction tube with the recovery tube is integrated into one piece mechanism, wherein, divide the liquid pipe to set up in one side of reaction tube, divide the one end of liquid pipe with the top intercommunication of reaction tube, divide the other end of liquid pipe to stretch into in the recovery tube, the recovery tube pass through divide the liquid pipe with the top intercommunication of reaction tube.
Preferably, the quick-connection mounting base comprises an outer grinding opening and an inner grinding opening, the outer grinding opening is fixedly connected to the outer wall of the bottom end of the recovery tube, and the inner grinding opening is fixedly connected to the inner wall of the top end of the reaction tube.
Preferably, the side wall surface of the reaction tube is provided with scales.
The utility model discloses a following technological effect:
the utility model discloses a set up the separator, utilize the oil water density difference to set up oil-water separation chamber and seperated recovery chamber by last under with in the separator, through liquid separation pipe and separator integrated into one piece, improve the reaction unit wholeness, and set up the control in the separator, can select to retrieve chamber intercommunication or partition with oil-water separation chamber and seperated according to actual conditions, promptly when the control separates the two, oil-water separation intracavity upper strata is the oil phase lower floor for the aqueous phase, upper oil phase lets in the seperated recovery intracavity through the liquid separation pipe, so as to carry out the repetitive reaction, and after the reaction, staff's operation control piece is with oil-water separation chamber and seperated recovery chamber intercommunication, under the action of gravity, lower floor's aqueous phase is discharged through seperated recovery chamber, compare in traditional water knockout drum mutually, the device volume has effectively been reduced to this patent, and all be provided with the fast even mount pad in separator top and bottom, when improving the speed of separator and reaction unit installation, still have higher stability.
Drawings
In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings required to be used in the embodiments will be briefly described below, and it is obvious that the drawings in the following description are only some embodiments of the present invention, and for those skilled in the art, other drawings can be obtained according to these drawings without inventive labor.
FIG. 1 is a schematic view of the overall apparatus;
FIG. 2 is a schematic structural view of example 2;
FIG. 3 is a partial detailed view at A in FIG. 2;
wherein, 1, grinding the outer side; 2. a door section; 3. a separator; 301. a reaction tube; 302. a recovery pipe; 4. a liquid separating pipe; 5. grinding the inner side; 6. a plunger; 7. a post handle; 8. a communicating pipe; 9. a spring; 10. a limit ring.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
In order to make the above objects, features and advantages of the present invention more comprehensible, the present invention is described in detail with reference to the accompanying drawings and the detailed description.
Example 1
Referring to fig. 1, the present invention provides a water separator, comprising,
the separation liquid storage assembly comprises a separator 3 and a control piece, wherein the separator 3 is provided with an oil-water separation cavity and a chaotropic recovery cavity from top to bottom, the control piece is arranged on the separator 3, and the oil-water separation cavity is communicated or separated with the chaotropic recovery cavity through the control piece;
the liquid separating pipe 4, the liquid separating pipe 4 and the separator 3 are integrally formed, and the oil phase separated from the oil-water separation cavity is introduced into the separation liquid recovery cavity through the liquid separating pipe 4;
and the quick connection mounting seats are respectively arranged at two ends of the separator 3, and the separator 3 is fixedly connected with an external reaction device through the quick connection mounting seats.
The utility model discloses a set up separator 3, utilize the profit density difference to set up oil-water separation chamber and seperated liquid recovery chamber by last under with separator 3 in, through liquid separation pipe 4 and 3 integrated into one piece of separator, improve the reaction unit wholeness, and set up the control in separator 3, can select oil-water separation chamber and seperated liquid recovery chamber intercommunication or partition according to actual conditions, when the control separates the two promptly, oil-water separation intracavity upper strata is the aqueous phase for oil phase lower floor, upper oil phase lets in the seperated liquid recovery intracavity through liquid separation pipe 4, so as to carry out the repetitive reaction, and after the reaction, staff's operation control communicates oil-water separation chamber and seperated liquid recovery chamber, under the action of gravity, lower floor's aqueous phase is through the chamber of retrieving of seperated liquid, compare in traditional water knockout drum, the device volume has effectively been reduced to this patent, and all be provided with the fast even mount pad on separator 3 tops and bottom, when improving the speed of separator 3 and reaction unit installation, still have higher stability.
Further, the whole device all adopts common transparent glass material preparation, and the liquid level height of staff's accessible observation oil water separation intracavity combines the control to regulate and control, makes the oil phase that surpasss the oil water separation chamber and predetermine the volume let in the chaotropic recovery intracavity through liquid separating pipe 4 to provide the needs of the required oil phase of different reactions or aqueous phase volume, improve the device suitability.
Further optimize the scheme, separator 3 includes reaction tube 301 and recovery tube 302 by setting gradually from top to bottom, and reaction tube 301 and recovery tube 302 set up on same axis, and the bottom of reaction tube 301 stretches into recovery tube 302 and recovery tube 302 intercommunication, and the control is located reaction tube 301 and is close to recovery tube 302 top and set up, and the control is connected with reaction tube 301 rotation, and reaction tube 301 passes through the control and is linked together or separate with recovery tube 302.
Further optimize the scheme, the control piece includes the throttle 2, and the one end of throttle 2 runs through reaction tube 301, and throttle 2 rotates with reaction tube 301 to be connected, and the through-hole has been seted up to the intermediate position of throttle 2, and the through-hole setting is in reaction tube 301, and reaction tube 301 passes through throttle 2 and recovery tube 302 intercommunication or separate.
Through twisting festival door 2, when the both ends that the through-hole was seted up to festival door 2 intermediate position correspond reaction tube 301 and recovery tube 302 respectively, reaction tube 301 and recovery tube 302 intercommunication, when the through-hole both ends correspond reaction tube 301's inside wall, through reaction tube 301 with the through-hole shutoff promptly, reaction tube 301 separates with recovery tube 302 this moment, thereby be convenient for the staff rotates the demand that festival door 2 control adjusted reaction liquid, and reaction tube 301 sets up at same axis with recovery tube 302, the wholeness of improving the device, reduce the equipment volume.
Further, the liquid volume that stores in reaction tube 301 is excessive, and the volume of oil phase can not satisfy reaction unit test demand, rotate the water phase of throttle 2 with lower floor in reaction tube 301 and pass through recovery tube 302 and flow, the liquid volume that stores in reaction tube 301 keeps proper amount degree through the control of throttle 2, and when the volume of oil phase satisfied reaction unit test demand, twist and change throttle 2 and separate reaction tube 301 and recovery tube 302, and be connected recovery tube 302 bottom through the fast-connecting mount pad with reaction unit, make the oil phase of upper strata in reaction tube 301 pass through in dividing liquid pipe 4 lets in recovery tube 302, realize oil phase separation repetitive reaction.
In an embodiment of the present invention, the gate 2 is preferably, but not limited to, a tetrafluoro gate.
Further optimize the scheme, divide liquid pipe 4, reaction tube 301 and recovery tube 302 to be integrated into one piece mechanism, and wherein, divide liquid pipe 4 to set up in one side of reaction tube 301, divide the one end of liquid pipe 4 and the top intercommunication of reaction tube 301, divide the other end of liquid pipe 4 to stretch into in recovery tube 302, recovery tube 302 is through dividing the top intercommunication of liquid pipe 4 and reaction tube 301.
Further optimize the scheme, the fast connection mount pad includes outside mill's mouth 1 and inboard mill's mouth 5, and outside mill's mouth 1 rigid coupling is at the bottom outer wall of recovery tube 302, and inboard mill's mouth 5 rigid coupling is at the top inner wall of reaction tube 301.
Through dividing liquid pipe 4, reaction tube 301 and recovery tube 302 integrated into one piece, improve the device wholeness, under the inboard mill run 5 of reaction tube 301 top rigid coupling and the outside mill run 1 combined action of recovery tube 302 bottom rigid coupling, improve the installation of device and dismantle speed to outside mill run 1 and inboard mill run 5 are toper dull polish structure, when being connected with reaction unit, increase the gas tightness, improve the installation effectiveness.
In a further optimized scheme, the side wall surface of the reaction tube 301 is provided with scales.
Example 2
Referring to fig. 2-3, a communicating pipe 8 is communicated with the side wall surface of the recovery pipe 302, a plunger 6 is slidably connected in the communicating pipe 8, one end of the plunger 6 is fixedly connected with a column handle 7, one end of the column handle 7, which is far away from the plunger 6, extends out of the communicating pipe 8, one end of the communicating pipe 8, which is far away from the recovery pipe 302, is fixedly connected with a limit ring 10, the column handle 7 is slidably connected with the limit ring 10, a spring 9 is arranged between the limit ring 10 and the plunger 6, and two ends of the spring 9 are fixedly connected with the plunger 6 and the limit ring 10 respectively.
Because divide the structure of buckling of liquid pipe 4, be detained easily when the oil phase leads to and solidify in the inflection, long-time use is easy to divide liquid pipe 4 to block up, rotate the throttle 2 through the staff this moment and separate reaction tube 301 and recovery tube 302, then pulling column handle 7 drives plunger 6 and removes, thereby suction recovery tube 302 and divide the air in the liquid pipe 4, make the oil phase in dividing liquid pipe 4 lead to fast under the negative pressure effect and go out, the realization is to the mediation of liquid pipe 4, and reset under the spring 9 effect, ensure the normal use of recovery tube 302.
The working principle is as follows: install through outside mill 1 and the quick whole device of inboard mill 5 with reaction unit, go on along with esterification reaction, the liquid volume of storing in the reaction tube 301 is excessive, and when the volume of oil phase can not satisfy the experimental demand of reaction unit, rotate the overhead door 2 and pass through recovery tube 302 with the aqueous phase of lower floor in the reaction tube 301 and flow, the liquid volume of storing in the reaction tube 301 keeps right amount degree through overhead door 2 control, and when the volume of oil phase satisfies the experimental demand of reaction unit, twist overhead door 2 and separate reaction tube 301 and recovery tube 302, and be connected with recovery tube 302 bottom through outside mill 1, make the oil phase of upper strata in the reaction tube 301 pass through in the branch liquid pipe 4 lets in recovery tube 302, realize oil phase separation repetitive reaction.
In the description of the present invention, it is to be understood that the terms "longitudinal", "lateral", "upper", "lower", "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outer", and the like indicate orientations or positional relationships based on the orientations or positional relationships shown in the drawings, and are merely for convenience of description of the present invention, and do not indicate or imply that the device or element referred to must have a particular orientation, be constructed and operated in a particular orientation, and thus, are not to be construed as limiting the present invention.
The above-mentioned embodiments are only described in the preferred embodiments of the present invention, but not limited to the scope of the present invention, and various modifications and improvements made by the technical solutions of the present invention by those skilled in the art should fall within the protection scope defined by the claims of the present invention without departing from the design spirit of the present invention.

Claims (6)

1. A water separator, characterized in that: comprises the steps of (a) preparing a mixture of a plurality of raw materials,
the separation liquid storage assembly comprises a separator (3) and a control piece, wherein an oil-water separation cavity and a chaotropic recovery cavity are arranged in the separator (3) from top to bottom, the control piece is arranged on the separator (3), and the oil-water separation cavity is communicated with or separated from the chaotropic recovery cavity through the control piece;
the liquid separating pipe (4) and the separator (3) are integrally formed, and the oil phase separated from the oil-water separation cavity is introduced into the separation liquid recovery cavity through the liquid separating pipe (4);
and the quick connection mounting seats are respectively arranged at two ends of the separator (3), and the separator (3) is fixedly connected with an external reaction device through the quick connection mounting seats.
2. The water separator of claim 1, wherein: separator (3) include by last reaction tube (301) and recovery tube (302) that set gradually down, reaction tube (301) with recovery tube (302) set up on same axis, just the bottom of reaction tube (301) stretches into recovery tube (302) with recovery tube (302) intercommunication, the control is located be close to on reaction tube (301) recovery tube (302) top sets up, the control with reaction tube (301) rotate to be connected, reaction tube (301) pass through the control with recovery tube (302) intercommunication or partition.
3. The water separator of claim 2, wherein: the control piece includes door (2), the one end of door (2) is run through reaction pipe (301), door (2) with reaction pipe (301) rotate to be connected, the through-hole has been seted up to the intermediate position of door (2), just the through-hole sets up in reaction pipe (301), reaction pipe (301) pass through door (2) with recovery pipe (302) intercommunication or partition.
4. The water separator of claim 2, wherein: divide liquid pipe (4) reaction tube (301) with recovery tube (302) is integrated into one piece mechanism, wherein, divide liquid pipe (4) to set up one side of reaction tube (301), divide the one end of liquid pipe (4) with the top intercommunication of reaction tube (301), divide the other end of liquid pipe (4) to stretch into in recovery tube (302), recovery tube (302) pass through divide liquid pipe (4) with the top intercommunication of reaction tube (301).
5. The water separator of claim 2, wherein: the quick-connection mounting seat comprises an outer side grinding opening (1) and an inner side grinding opening (5), the outer side grinding opening (1) is fixedly connected with the bottom outer wall of the recovery pipe (302), and the inner side grinding opening (5) is fixedly connected with the top end inner wall of the reaction pipe (301).
6. The water knockout vessel of claim 2, wherein: the side wall surface of the reaction tube (301) is provided with scales.
CN202223431540.4U 2022-12-20 2022-12-20 Water separator Active CN218853529U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202223431540.4U CN218853529U (en) 2022-12-20 2022-12-20 Water separator

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202223431540.4U CN218853529U (en) 2022-12-20 2022-12-20 Water separator

Publications (1)

Publication Number Publication Date
CN218853529U true CN218853529U (en) 2023-04-14

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ID=87350096

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202223431540.4U Active CN218853529U (en) 2022-12-20 2022-12-20 Water separator

Country Status (1)

Country Link
CN (1) CN218853529U (en)

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