CN218741936U - High-efficient synthetic reation kettle of acetanilide - Google Patents
High-efficient synthetic reation kettle of acetanilide Download PDFInfo
- Publication number
- CN218741936U CN218741936U CN202222618492.3U CN202222618492U CN218741936U CN 218741936 U CN218741936 U CN 218741936U CN 202222618492 U CN202222618492 U CN 202222618492U CN 218741936 U CN218741936 U CN 218741936U
- Authority
- CN
- China
- Prior art keywords
- wall
- fixedly connected
- acetanilide
- bull stick
- cauldron jar
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- FZERHIULMFGESH-UHFFFAOYSA-N N-phenylacetamide Chemical compound CC(=O)NC1=CC=CC=C1 FZERHIULMFGESH-UHFFFAOYSA-N 0.000 title claims abstract description 66
- 229960001413 acetanilide Drugs 0.000 title claims abstract description 33
- 244000309464 bull Species 0.000 claims abstract description 21
- 230000005540 biological transmission Effects 0.000 claims abstract description 8
- 238000003786 synthesis reaction Methods 0.000 claims description 8
- 238000003756 stirring Methods 0.000 abstract description 37
- 239000002994 raw material Substances 0.000 abstract description 27
- 238000006243 chemical reaction Methods 0.000 abstract description 24
- 238000007599 discharging Methods 0.000 description 10
- 238000003466 welding Methods 0.000 description 5
- 239000000203 mixture Substances 0.000 description 4
- 238000007790 scraping Methods 0.000 description 4
- 239000000376 reactant Substances 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 230000000202 analgesic effect Effects 0.000 description 1
- 230000001754 anti-pyretic effect Effects 0.000 description 1
- 230000002421 anti-septic effect Effects 0.000 description 1
- 239000002221 antipyretic Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 229940124530 sulfonamide Drugs 0.000 description 1
- 150000003456 sulfonamides Chemical class 0.000 description 1
- -1 support 1 Chemical compound 0.000 description 1
Images
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The utility model discloses a high-efficient synthetic reation kettle of acetanilide, including the support, it is connected with the cauldron jar to rotate between the inner wall of support, the bottom outer wall fixedly connected with extension board of cauldron jar, the frame is propped up to the top outer wall fixedly connected with of support, it is connected with the curved bar to rotate between the inner wall of frame, the outer wall of curved bar rotates and has cup jointed the transfer line, and the one end of transfer line rotates the back outer wall of connection at the extension board, the top outer wall fixed mounting of cauldron jar has agitator motor, agitator motor's output shaft transmission is connected with the bull stick, the outer wall fixedly connected with a plurality of horizontal puddler of bull stick. The utility model discloses a circular motion is done to the one end that the curved bar rotated drive transfer line, and the other end of transfer line then drives the bottom swing of cauldron jar through the extension board, and the inside reaction raw materials of cauldron jar can mix along with the swing of cauldron jar, and no longer only lean on the puddler to stir and mix for the inside reaction raw materials of cauldron jar can the intensive mixing, and the reaction is more abundant.
Description
Technical Field
The utility model relates to an acetanilide production facility technical field, concretely relates to high-efficient synthetic reation kettle of acetanilide.
Background
Acetanilide is an organic compound, is colorless and glittering lobular solid or white crystalline powder, is a raw material of sulfonamides, and can be used as an analgesic, an antipyretic, an antiseptic and a dye intermediate.
However, in the prior art, the chemical reaction kettle tightly abuts against the stirring paddle to stir the reactants, so that the reactants cannot be efficiently and fully mixed, incomplete reaction is easily caused, and the reactants are easily accumulated at the bottom of the reaction kettle to influence the reaction efficiency. Therefore, it is necessary to design an efficient acetanilide synthesis reaction kettle to solve the above problems.
SUMMERY OF THE UTILITY MODEL
The utility model aims at providing a high-efficient synthetic reation kettle of acetanilide to solve the above-mentioned weak point among the prior art.
In order to achieve the above object, the present invention provides the following technical solutions: the utility model provides a high-efficient synthetic reation kettle of acetanilide, includes the support, it is connected with the cauldron jar to rotate between the inner wall of support, the bottom outer wall fixedly connected with extension board of cauldron jar, the top outer wall fixedly connected with of support props up the frame, it is connected with the curved bar to prop up to rotate between the inner wall of frame, the outer wall of curved bar rotates and has cup jointed the transfer line, and the one end of transfer line rotates the back outer wall of connecting at the extension board, the top outer wall fixed mounting of cauldron jar has agitator motor, agitator motor's output shaft transmission is connected with the bull stick, the outer wall fixedly connected with a plurality of horizontal stirring rod of bull stick, the lateral wall fixedly connected with a plurality of vertical stirring rod of horizontal stirring rod, the bottom lateral wall fixedly connected with spiral leaf of bull stick.
Furthermore, the top outer wall of support is fixedly connected with the backing plate, the top outer wall fixed mounting of backing plate has swing motor, and swing motor's output shaft is connected with the one end transmission of curved bar.
Further, the top outer wall fixedly connected with inlet pipe of cauldron jar, the lateral wall of inlet pipe is provided with the feed valve.
Further, the bottom outer wall fixedly connected with discharging pipe of cauldron jar, the lateral wall of discharging pipe sets up the bleeder valve.
Furthermore, the side wall of the rotating rod is fixedly connected with a plurality of transverse connecting rods, and one ends of the transverse connecting rods are fixedly connected with side scraping plates.
Furthermore, the side wall of the rotating rod is fixedly connected with a plurality of inclined connecting rods, and one end of each inclined connecting rod is fixedly connected with a bottom scraping plate.
In the technical scheme, the utility model provides an acetanilide high efficiency synthesis reation kettle, rotate through the curved bar that sets up and drive one end of transfer line and do the circular motion, the other end of transfer line then drives the bottom swing of cauldron jar through the extension board, the reaction raw materials inside the cauldron jar can be mixed along with the swing of cauldron jar, no longer only lean on the puddler to stir and mix, make the reaction raw materials inside the cauldron jar can fully mix, the reaction is more abundant; the raw materials at the bottom are turned upwards through the rotation of the arranged spiral blades, so that the reaction raw materials cannot be accumulated at the bottom, and the reaction raw materials are matched with the transverse stirring rod to drive the vertical stirring rod to stir, so that the stirring range is larger, and the reaction efficiency is improved; the side scraping plates are driven to rotate through the arranged transverse connecting rods, and the side scraping plates rotate to scrape the acetanilide synthetic raw materials adhered to the inner wall of the kettle tank, so that workers can clean the interior of the kettle tank conveniently; the inclined connecting rod through setting up drives the end scraper blade and rotates, and the side scraper blade rotates and scrapes the synthetic raw materials of acetanilide who bonds at cauldron bottom inner wall and gets, avoids acetanilide synthetic raw materials to pile up at cauldron bottom inner wall and bonds to make things convenient for the staff to wash cauldron jar inside.
Drawings
In order to more clearly illustrate the embodiments of the present application or the technical solutions in the prior art, the drawings needed to be used in the embodiments will be briefly described below, and it is obvious that the drawings in the following description are only some embodiments described in the present invention, and other drawings can be obtained by those skilled in the art according to these drawings.
Fig. 1 is a schematic front structural diagram of a high-efficient synthetic reation kettle of acetanilide that the utility model provides.
Fig. 2 is a back structural schematic diagram of the high-efficient synthetic reation kettle of acetanilide that the utility model provides.
Fig. 3 is a schematic front sectional structural view of the acetanilide high-efficiency synthesis reactor provided by the utility model.
Fig. 4 is a schematic side sectional view of the acetanilide high-efficiency synthesis reaction kettle provided by the utility model.
Description of reference numerals:
the device comprises a support 1, a kettle tank 2, a support plate 3, a support frame 4, a curved rod 5, a transmission rod 6, a stirring motor 7, a rotating rod 8, a transverse stirring rod 9, a vertical stirring rod 10, a spiral blade 11, a base plate 12, a swing motor 13, a feeding pipe 14, a feeding valve 15, a discharging pipe 16, a discharging valve 17, a transverse connecting rod 18, a side scraper 19, an inclined connecting rod 20 and a bottom scraper 21.
Detailed Description
In order to make the technical solution of the present invention better understood by those skilled in the art, the present invention will be further described in detail with reference to the accompanying drawings.
As shown in fig. 1-4, the embodiment of the utility model provides a high-efficient synthetic reation kettle of acetanilide, including support 1, it is connected with cauldron jar 2 to rotate between the inner wall of support 1, cauldron jar 2's bottom outer wall welding has extension board 3, support 1's top outer wall welding has a frame 4, it is connected with bent lever 5 to rotate between the inner wall of frame 4, bent lever 5's outer wall rotates and has cup jointed transfer line 6, and transfer line 6's one end rotates the back outer wall of connecting at extension board 3, circular motion is done to bent lever 5 rotation drive transfer line 6's one end, transfer line 6's the other end then drives the bottom swing of cauldron jar 2 through extension board 3, cauldron jar 2 inside reaction raw materials can be mixed along with cauldron jar 2's swing, the equidistance only leans on the puddler to stir the mixture again, make cauldron jar 2 inside reaction materials can the intensive mixing, the reaction is more abundant, there is agitator motor 7 at the top outer wall of cauldron jar 2 through bolt fixed mounting, agitator motor 7's transmission output shaft has a bull stick 8, the outer wall of bull stick 8, the outer wall welding has a plurality of bull stick 8, make the propeller shaft stir pole 8 to stir the pole to stir the top and carry out the top of 10 rotation and stir the propeller blade and carry out the stirring and carry out the cooperation of propeller blade and carry out the stirring blade and carry out the stirring efficiency improvement in the propeller stirring blade 10, stir blade and stir blade 10, stir blade and carry out the stirring blade rotation range on the stirring blade and stir blade and carry out the stirring blade rotation range 10.
The utility model provides a pair of high-efficient synthetic reation kettle of acetanilide adopts curved bar 5 to rotate the one end that drives transfer line 6 and is circular motion, and transfer line 6's the other end then drives the bottom swing of cauldron jar 2 through extension board 3, and the inside reaction raw materials of cauldron jar 2 can be mixed along with the swing of cauldron jar 2, and no longer only lean on the puddler to stir and mix for the reaction raw materials of cauldron jar 2 inside can intensive mixing, and the reaction is more abundant.
In another embodiment, as shown in fig. 1-3, the top outer wall of the support 1 is welded with a backing plate 12, the top outer wall of the backing plate 12 is fixed with a swing motor 13 through a bolt, the output shaft of the swing motor 13 is connected with the one end of the curved bar 5 in a transmission manner, and the swing motor 13 drives the curved bar 5 to rotate.
In another embodiment, as shown in fig. 1-3, the feeding pipe 14 is fixedly connected to the outer wall of the top of the autoclave 2, the acetanilide raw material enters the autoclave 2 through the feeding pipe 14, the side wall of the feeding pipe 14 is provided with a feeding valve 15, and the feeding valve 15 controls the opening and closing of the feeding pipe 14.
In another embodiment, as shown in fig. 1 and fig. 2-4, the discharging pipe 16 is fixedly connected to the outer wall of the bottom of the autoclave 2, the synthesized acetanilide is discharged through the discharging pipe 16, the discharging valve 17 is disposed on the side wall of the discharging pipe 16, and the discharging valve 17 controls the opening and closing of the discharging pipe 16.
The utility model provides a further embodiment, as shown in fig. 4, a plurality of transverse connecting rod 18 of lateral wall fixedly connected with of bull stick 8, transverse connecting rod 18 is symmetrical arrangement, transverse connecting rod 18 rotates along with bull stick 8, transverse connecting rod 18's one end fixedly connected with side scraper 19, side scraper 19's lateral wall is laminated with the inner wall of cauldron jar 2 mutually, transverse connecting rod 18 drives side scraper 19 and rotates, side scraper 19 rotates and scrapes the synthetic raw materials of acetanilide who bonds on 2 inner walls of cauldron jar and take off, make things convenient for the staff to wash 2 insides of cauldron jar.
The utility model provides a further embodiment, as shown in FIG. 4, the lateral wall welding of bull stick 8 has a plurality of oblique connecting rod 20, oblique connecting rod 20 is the slope form, and symmetrical arrangement, oblique connecting rod 20 rotates along with the bull stick 8, the one end welding of oblique connecting rod 20 has end scraper 21, end scraper 21 is arc, and laminate mutually with the bottom inner wall of cauldron jar 2, oblique connecting rod 20 drives end scraper 21 and rotates, side scraper 19 rotates and scrapes the synthetic raw materials of acetanilide who bonds at 2 bottom inner walls of cauldron jar and get, avoid acetanilide synthetic raw materials to pile up the bonding at 2 bottom inner walls of cauldron jar, and make things convenient for the staff to wash 2 insides of cauldron jar.
The working principle is as follows: during the use, the staff opens feed valve 15, acetanilide synthetic raw materials enter into cauldron jar 2 through inlet pipe 14, agitator motor 7 drive bull stick 8 rotates, bull stick 8 drives violently stirring rod 9 and spiral leaf 11 and rotates, spiral leaf 11 rotates upwards the raw materials of bottom, make reaction raw materials can not pile up in the bottom, cooperation violently stir rod 9 drives perpendicular stirring rod 10 and stirs, make the stirring scope bigger, improve reaction efficiency, cross-connecting rod 18 rotates along with bull stick 8, cross-connecting rod 18 drives side scraper blade 19 and rotates, side scraper blade 19 rotates scrapes the acetanilide synthetic raw materials that bonds on cauldron jar 2 inner wall, oblique connecting rod 20 rotates along with bull stick 8, oblique connecting rod 20 drives end scraper 21 and rotates, side scraper blade 19 rotates and scrapes the acetanilide synthetic raw materials that bonds at cauldron jar 2 bottom inner wall, avoid acetanilide synthetic raw materials to pile up the bonding at cauldron jar 2 bottom inner wall, the staff starts swing motor 13, swing motor 13 drives curved rod 5 and rotates, curved rod 5 rotates and does the circular motion, the other end of transfer line 6 then passes through 3, the inside of cauldron jar 2 that drives, the reaction raw materials that the stirring kettle jar 2 is not leaned on the reaction raw materials can not carry out again, the reaction raw materials that the mixing kettle 2 is not enough again.
While certain exemplary embodiments of the present invention have been described above by way of illustration only, it will be apparent to those of ordinary skill in the art that the described embodiments may be modified in various different ways without departing from the spirit and scope of the present invention. Accordingly, the drawings and description are illustrative in nature and should not be construed as limiting the scope of the invention.
Claims (6)
1. The utility model provides a high-efficient synthetic reation kettle of acetanilide, includes support (1), its characterized in that, it is connected with cauldron jar (2) to rotate between the inner wall of support (1), bottom outer wall fixedly connected with extension board (3) of cauldron jar (2), the top outer wall fixedly connected with of support (1) props up frame (4), it is connected with curved bar (5) to rotate between the inner wall of frame (4), the outer wall of curved bar (5) rotates and has cup jointed transfer line (6), and the one end of transfer line (6) rotates the back outer wall of connecting at extension board (3), the top outer wall fixed mounting of cauldron jar (2) has agitator motor (7), the output shaft transmission of agitator motor (7) is connected with bull stick (8), the outer wall fixedly connected with a plurality of bull stick (9), the lateral wall fixedly connected with a plurality of bull stick (10) of bull stick (9) is violently stirred, the bottom lateral wall fixedly connected with spiral leaf (11) of bull stick (8).
2. The acetanilide high-efficiency synthesis reaction kettle according to claim 1, wherein a backing plate (12) is fixedly connected to the outer wall of the top of the support (1), a swing motor (13) is fixedly mounted on the outer wall of the top of the backing plate (12), and an output shaft of the swing motor (13) is in transmission connection with one end of the curved rod (5).
3. The high-efficiency acetanilide synthesis reaction kettle according to claim 1, wherein a feed pipe (14) is fixedly connected to the outer wall of the top of the kettle tank (2), and a feed valve (15) is arranged on the side wall of the feed pipe (14).
4. The high-efficiency acetanilide synthesis reaction kettle according to claim 1, wherein a discharge pipe (16) is fixedly connected to the outer wall of the bottom of the kettle tank (2), and a discharge valve (17) is arranged on the side wall of the discharge pipe (16).
5. The acetanilide high-efficiency synthesis reaction kettle according to claim 1, wherein a plurality of transverse connecting rods (18) are fixedly connected to the side wall of the rotating rod (8), and a side scraper (19) is fixedly connected to one end of each transverse connecting rod (18).
6. The reactor according to claim 1, wherein the side wall of the rotating rod (8) is fixedly connected with a plurality of inclined connecting rods (20), and one end of each inclined connecting rod (20) is fixedly connected with a bottom scraper (21).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202222618492.3U CN218741936U (en) | 2022-10-07 | 2022-10-07 | High-efficient synthetic reation kettle of acetanilide |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202222618492.3U CN218741936U (en) | 2022-10-07 | 2022-10-07 | High-efficient synthetic reation kettle of acetanilide |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN218741936U true CN218741936U (en) | 2023-03-28 |
Family
ID=85695891
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202222618492.3U Expired - Fee Related CN218741936U (en) | 2022-10-07 | 2022-10-07 | High-efficient synthetic reation kettle of acetanilide |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN218741936U (en) |
-
2022
- 2022-10-07 CN CN202222618492.3U patent/CN218741936U/en not_active Expired - Fee Related
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN213320889U (en) | High-efficient agitating unit is used in concrete production | |
| CN112454671A (en) | High efficiency concrete mixing jar convenient to it is clean | |
| CN207310249U (en) | Concrete production multistep agitating device | |
| CN218741936U (en) | High-efficient synthetic reation kettle of acetanilide | |
| CN210552138U (en) | High-efficient concrete mixer of building machinery | |
| CN210235938U (en) | A agitating unit for discharging material silo | |
| CN217802447U (en) | Closed integrated vertical mortar stirring tank | |
| CN110813146A (en) | Two-way agitating unit that wood industry glue was used | |
| CN211988156U (en) | Sodium carboxymethylcellulose mixing machine | |
| CN114177864A (en) | Solid-liquid mixing stirring type reaction kettle | |
| CN210473769U (en) | A batching mixing arrangement for flour processing | |
| CN219748486U (en) | Concrete stirring device | |
| CN217962128U (en) | Water quality modifier raw material mixing device for aquaculture | |
| CN219252580U (en) | Enamel neutralization kettle stirring device | |
| CN220878676U (en) | Anti-blocking mixing stirring device | |
| CN221774877U (en) | Stirring equipment for grouting of super-early-strength grouting material | |
| CN221889857U (en) | Three-dimensional agitating unit of hydrolysis reaction cauldron | |
| CN218962840U (en) | Preparation device of attapulgite passivation material | |
| CN221637807U (en) | Horizontal mixer for producing reinforced efficient water-soluble fertilizer | |
| CN218981565U (en) | Reation kettle is used in chitin production | |
| CN218422197U (en) | Biological adhesive stirring device for plate bonding | |
| CN218196000U (en) | Anti-bonding mortar storage tank | |
| CN220125942U (en) | Agitated vessel for electrical chemistry industry | |
| CN218422138U (en) | High-efficient horizontal mixer | |
| CN219291134U (en) | Raw material mixing device |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20230328 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |