CN218654475U - Synthesizer of isomeric mellow wine polyoxyethylene ether - Google Patents
Synthesizer of isomeric mellow wine polyoxyethylene ether Download PDFInfo
- Publication number
- CN218654475U CN218654475U CN202223142690.3U CN202223142690U CN218654475U CN 218654475 U CN218654475 U CN 218654475U CN 202223142690 U CN202223142690 U CN 202223142690U CN 218654475 U CN218654475 U CN 218654475U
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- Prior art keywords
- stirring
- premixing
- sliding
- polyoxyethylene ether
- feed inlet
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- 229940051841 polyoxyethylene ether Drugs 0.000 title claims abstract description 32
- 229920000056 polyoxyethylene ether Polymers 0.000 title claims abstract description 32
- 238000003756 stirring Methods 0.000 claims abstract description 87
- 238000007789 sealing Methods 0.000 claims abstract description 46
- 230000007246 mechanism Effects 0.000 claims abstract description 43
- 230000015572 biosynthetic process Effects 0.000 claims abstract description 15
- 238000003786 synthesis reaction Methods 0.000 claims abstract description 15
- 238000006243 chemical reaction Methods 0.000 claims description 51
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 23
- 230000000149 penetrating effect Effects 0.000 claims description 2
- 230000002194 synthesizing effect Effects 0.000 claims 1
- 239000000463 material Substances 0.000 abstract description 23
- 239000000126 substance Substances 0.000 abstract description 4
- 230000006835 compression Effects 0.000 abstract description 2
- 238000007906 compression Methods 0.000 abstract description 2
- 230000009471 action Effects 0.000 description 5
- 239000003054 catalyst Substances 0.000 description 3
- 238000007599 discharging Methods 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 230000005540 biological transmission Effects 0.000 description 2
- LQZZUXJYWNFBMV-UHFFFAOYSA-N dodecan-1-ol Chemical compound CCCCCCCCCCCCO LQZZUXJYWNFBMV-UHFFFAOYSA-N 0.000 description 2
- 230000005389 magnetism Effects 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- KJIOQYGWTQBHNH-UHFFFAOYSA-N undecanol Chemical compound CCCCCCCCCCCO KJIOQYGWTQBHNH-UHFFFAOYSA-N 0.000 description 2
- XFRVVPUIAFSTFO-UHFFFAOYSA-N 1-Tridecanol Chemical compound CCCCCCCCCCCCCO XFRVVPUIAFSTFO-UHFFFAOYSA-N 0.000 description 1
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 150000002191 fatty alcohols Chemical class 0.000 description 1
- 239000010985 leather Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 238000001308 synthesis method Methods 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 229940087291 tridecyl alcohol Drugs 0.000 description 1
- 229940057402 undecyl alcohol Drugs 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
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Abstract
The utility model discloses a synthesizer of heterogeneous mellow wine polyoxyethylene ether belongs to chemical industry equipment technical field, including premixing mechanism and rabbling mechanism, premixing mechanism sets up the top at rabbling mechanism, premixing mechanism is including premixing the jar, be provided with first stirring subassembly on premixing the jar, rabbling mechanism includes that retort and lid establish the sealed lid on the retort, be provided with the slip sealing member in the lid of sealed lid slidable, the feed inlet has been seted up on the lid, the feed inlet all communicates with the inner chamber of premixing jar and retort, the one end of slip sealing member is supported and is held on the oral wall of feed inlet, the inside of lid is provided with the electro-magnet, be provided with the spring between electro-magnet and the slip sealing member, the spring is in compression state, the switch of the break-make electric control feed inlet of accessible electro-magnet, thereby the material stirring premix time in the control premixing mechanism, efficiency and the synthesis efficiency that the stirring is mixed are improved.
Description
Technical Field
The utility model belongs to the technical field of chemical industry equipment, concretely relates to synthesizer of isomeric mellow wine polyoxyethylene ether.
Background
The isomeric alcohol polyoxyethylene ether is a chemical product of a surfactant, and is mainly divided into isomeric dodecyl alcohol polyoxyethylene ether, isomeric undecyl alcohol polyoxyethylene ether, isomeric tridecyl alcohol polyoxyethylene ether and the like. The isomeric alcohol polyoxyethylene ether has a molecular structure with a branched chain, and the unique structure enables the isomeric alcohol polyoxyethylene ether to have the excellent performance of alkylphenol polyoxyethylene ether and the high degradability of fatty alcohol polyoxyethylene ether, so that the isomeric alcohol polyoxyethylene ether is widely applied to textile industry, leather, daily chemical washing and the like. At present, the synthesis method of isomeric alcohol polyoxyethylene ether in industry is to adopt isomeric alcohol and ethylene oxide to catalyze and synthesize isomeric alcohol polyoxyethylene ether under the action of an alkaline catalyst. Under the action of an alkaline catalyst, a chain begins to grow before starting agent raw material alcohol is often not converted into alcohol ether with single or low EO addition number, so that the product has raw material residues, the molecular weight distribution of the synthesized product is wide, meanwhile, the reaction process of the method is accompanied by longer dehydration time, in order to relieve the phenomenon, the catalyst needs to be added after all the raw materials are uniformly mixed before preparation, the existing synthesis device has large tank body and more capacity, all the materials are added into the tank body at one time and need to be stirred for a long time to be uniformly stirred, the stirring and mixing efficiency is slower, and the synthesis efficiency is influenced.
Disclosure of Invention
The utility model provides a synthesizer of isomeric mellow wine polyoxyethylene ether has solved the problem of stirring inefficiency among the above-mentioned prior art.
In order to achieve the above purpose, the utility model adopts the following technical scheme:
a synthesis device of isomeric alcohol polyoxyethylene ether comprises a premixing mechanism, a stirring mechanism and a sealing cover, wherein the sealing cover is arranged at the top of the stirring mechanism, the premixing mechanism is arranged above the sealing cover, a feeding hole and a sliding sealing piece are arranged on the sealing cover, the sliding sealing piece controls the opening and closing of the feeding hole, and the feeding hole is communicated with the inner cavities of the premixing mechanism and the stirring mechanism;
in the structure, the top of the premixing tank is connected with a feeding pipe, and the feeding pipe is communicated with the inner cavity of the premixing tank;
a fixing frame is arranged on the inner side wall of the premixing tank, a bearing is mounted on the fixing frame, one end, relatively far away from the driving motor, of the stirring shaft is arranged in the bearing in a penetrating mode, and helical blades are arranged on the periphery of the side wall of the stirring shaft in a surrounding mode;
the premixing mechanism comprises a premixing tank, a first stirring assembly is arranged on the premixing tank, the first stirring assembly comprises a driving motor and a stirring shaft, the driving motor is mounted at the top of the premixing tank, the stirring shaft is rotatably arranged in the premixing tank, the driving motor is arranged on one side of the feeding pipe, and a driving shaft of the driving motor is in driving connection with one end of the stirring shaft;
the stirring mechanism comprises a reaction tank and a sealing cover covered on the reaction tank,
the reaction tank is provided with a second stirring assembly, the second stirring assembly comprises a mounting frame fixedly arranged at the bottom of the reaction tank, a motor arranged on the mounting frame, a stirring rod rotatably arranged in the reaction tank and a plurality of stirring blades arranged at one end of the stirring rod, the stirring blades are all positioned in the reaction tank, and one end of the stirring rod 3, opposite to the stirring blades, is in transmission connection with an output shaft of the motor; the bottom of the reaction tank is provided with a plurality of support frames, the reaction tank and the support frames are fixedly connected or integrally formed, the bottom of the side wall of the reaction tank is connected with a discharge pipe, and the discharge pipe is communicated with the inner cavity of the reaction tank;
a sliding sealing element is slidably arranged in a cover body of the sealing cover, a feed inlet is formed in the cover body, the feed inlet is communicated with inner cavities of the premixing tank and the reaction tank, one end of the sliding sealing element is abutted against the wall of the feed inlet, an electromagnet is arranged in the cover body, a spring is arranged between the electromagnet and the sliding sealing element, and the spring is in a compressed state;
a groove is formed in the wall of the opening of the feeding hole, a sliding groove is formed in one side, opposite to the groove, of the cover body, and a sliding hole communicated with the feeding hole is formed in one end of the wall of the sliding groove;
the sliding sealing piece is slidably arranged between the sliding groove and the feeding hole, the sliding sealing piece comprises a sliding plate which is slidably arranged in the sliding hole, and a sealing head and a sliding block which are arranged at two ends of the sliding plate, one end of the sliding plate, provided with the sealing head, penetrates through the sliding hole and extends into the feeding hole, the sealing head is matched with the groove, one end of the sliding plate, provided with the sliding block, penetrates through the sliding hole and extends to the sliding groove, and the sliding block is slidably arranged in the sliding groove;
the electromagnet is arranged in the sliding chute and is arranged at one end of the sliding chute, which is relatively far away from the sliding hole; two ends of the spring are respectively abutted against the sliding block and the electromagnet.
Has the advantages that: the utility model provides a synthesizer of heterogeneous mellow wine polyoxyethylene ether, including premixing mechanism and rabbling mechanism, premixing mechanism sets up the top at rabbling mechanism, premixing mechanism is including premixing the jar, be provided with first stirring subassembly on premixing the jar, rabbling mechanism includes that retort and lid establish the sealed lid on the retort, be provided with the slip sealing member in the lid of sealed lid slidable, the feed inlet has been seted up on the lid, the feed inlet all communicates with the inner chamber of premixing jar and retort, the one end of slip sealing member is supported and is held on the oral wall of feed inlet, the inside of lid is provided with the electro-magnet, be provided with the spring between electro-magnet and the slip sealing member, the both ends of spring are supported respectively and are held on slip sealing member and electro-magnet and the spring is in compression state, produce magnetism and adsorb the slip sealing member and slide to the direction that is close to the electro-magnet when the electro-magnet circular telegram, the feed inlet is opened, the electro-magnet is when outage, the slip sealing member resets under the effect of spring, the feed inlet is sealed, the switch of feed inlet of staff's accessible electro-magnet, thereby control premixing time is mixed in the material stirring of control, the efficiency and the synthetic efficiency of stirring are mixed are improved.
Drawings
FIG. 1 is a schematic structural diagram of a synthesis apparatus for isomeric alcohol polyoxyethylene ether in an embodiment of the present invention;
FIG. 2 is a sectional view of a synthesis device for isomeric alcohol polyoxyethylene ether in an embodiment of the present invention;
FIG. 3 is a cross-sectional view of a sealing cover in a synthesis device of isomeric alcohol polyoxyethylene ether in an embodiment of the present invention;
FIG. 4 is a schematic view of a sliding seal in a seal cap according to an embodiment of the present invention;
in the figure: 1-premixing mechanism, 11-premixing tank, 111-feeding pipe, 12-first stirring component, 121-driving motor, 122-stirring shaft, 123-helical blade, 124-fixing frame, 2-stirring mechanism, 21-reaction tank, 211-discharging pipe, 22-sealing cover, 221-cover body, 2211-feeding hole, 2212-groove, 2213-sliding groove, 2214-sliding hole, 222-sliding sealing piece, 2221-separating plate, 2222-sealing head, 2223-sliding block, 223-electromagnet, 224-spring, 23-second stirring component, 231-mounting frame, 232-motor, 233-stirring rod, 234-stirring blade and 24-supporting frame.
Detailed Description
The invention will be described in detail with reference to the following drawings and specific embodiments:
as shown in fig. 1, a synthesis apparatus for isomeric alcohol polyoxyethylene ether comprises a premixing mechanism 1 for stirring and premixing materials, and a stirring mechanism 2 for stirring and reacting to synthesize isomeric alcohol polyoxyethylene ether, wherein the premixing mechanism 1 is arranged at the top of the stirring mechanism 2, and the materials are conveyed into the premixing mechanism 1 for stirring and premixing, and then conveyed to the stirring mechanism 2 for reacting;
as shown in fig. 2, the premixing mechanism 1 includes a premixing tank 11 for containing the respective materials, and a first stirring assembly 1 mounted on the premixing tank 11 for stirring and premixing the respective materials; the top of the premixing tank 11 is connected with a feeding pipe 111 for conveying materials, and the feeding pipe 111 is communicated with the inner cavity of the premixing tank 11; the first stirring group comprises a driving motor 121 arranged at the top of the premixing tank 11 and a stirring shaft 122 rotatably arranged in the premixing tank 11, the driving motor 121 is arranged at one side of the feeding pipe 111, a driving shaft of the driving motor 121 is in driving connection with one end of the stirring shaft 122, helical blades 123 for stirring materials are arranged around the periphery of the side wall of the stirring shaft 122, a fixing frame 124 matched with the stirring shaft 122 is arranged on the inner side wall of the premixing tank 11, a bearing is arranged on the fixing frame 124, one end, relatively far away from the driving motor 121, of the stirring shaft 122 penetrates through the bearing, and the driving motor 121 drives the stirring shaft 122 to drive the helical blades 123 to rotate, so that the materials in the premixing tank 11 are stirred and premixed;
the stirring mechanism 2 comprises a reaction tank 21 for containing reaction materials, a sealing cover 22 which is covered on the reaction tank 21 and is used for sealing the reaction tank 21, a second stirring component 23 which is arranged on the reaction tank 21 and is used for stirring the reaction materials, and a plurality of supporting frames 24 which are arranged at the bottom of the reaction tank 21 and are used for supporting the reaction tank 21, wherein the reaction tank 21 and the supporting frames 24 are fixedly connected or integrally formed; the bottom of the side wall of the reaction tank 21 is connected with a discharge pipe 211 for discharging reaction materials, and the discharge pipe 211 is communicated with the inner cavity of the reaction tank 21; the second stirring assembly 23 comprises a mounting frame 231 fixedly arranged at the bottom of the reaction tank 21, a motor 232 arranged on the mounting frame 231, a stirring rod 233 rotatably arranged in the reaction tank 21, and a plurality of stirring blades 234 arranged at one end of the stirring rod 233, wherein the stirring blades 234 are all positioned inside the reaction tank 21, one end of the stirring rod 233, opposite to the stirring blades 234, is in transmission connection with an output shaft of the motor 232, and the motor 232 drives the stirring rod 233 to drive the stirring blades 234 to rotate, so that reaction materials in the reaction tank 21 are stirred;
as shown in fig. 3 and 4, the sealing cover 22 includes a cover 221 covering the top of the reaction tank 21, and a sliding seal 222 slidably disposed on the cover 221, the cover 221 is provided with a feed port 2211 for conveying materials, the feed port 2211 is communicated with the inner cavities of the pre-mixing tank 11 and the reaction tank 21, one end of the sliding seal 222 abuts against the wall of the feed port 2211, the wall of the feed port 2211 is provided with a groove 2212 matched with the sliding seal 222, the inside of one side of the cover 221 opposite to the groove 2212 is provided with a sliding slot 2213, and one end of the slot wall of the sliding slot 2213 is provided with a sliding hole 2214 communicated with the feed port 2211; the sliding seal 222 is slidably disposed between the sliding slot 2213 and the feeding port 2211, the sliding seal 222 includes a sliding plate 2221 slidably disposed in the sliding hole 2214, and a sealing head 2222 and a sliding block 2223 disposed at two ends of the sliding plate, one end of the sliding plate 2221 having the sealing head 2222 extends into the feeding port 2211 through the sliding hole 2214, the sealing head 2222 at one end of the sliding plate 2221 is adapted to the groove 2212 on the wall of the feeding port 2211, one end of the sliding plate 2221 having the sliding block 2223 is extended into the sliding slot 2213 through the sliding hole 2214, the sliding block 2223 at one end of the sliding plate 2221 is slidably disposed in the sliding slot 2213, one end of the sliding slot 2213 opposite to the sliding hole 2214 is disposed with an electromagnet 223, a spring 224 is disposed between the electromagnet 223 and the sliding block 2223, two ends of the spring 224 respectively abut against the sliding block 2223 and the electromagnet 223, the spring 224 is in a compressed state, the sliding seal piece 222 abuts against the wall of the feeding hole 2211 under the action of the spring 224, at this time, the sealing head 2222 is embedded in the groove 2212, when the material in the premixing mechanism 1 is stirred and premixed, the electromagnet 224 is electrified to generate magnetism and adsorb the sliding block 2223 to slide towards the direction close to the electromagnet 224, the sliding block 2223 extrudes the spring 224 and drives the sliding seal piece 222 to move integrally, at this time, the sealing head 2222 is separated from the groove 2212, the feeding hole 2211 is opened, the material is conveyed into the inner reaction tank 21 through the feeding hole 2211, after the conveying is completed, the electromagnet 224 is powered off, and the sliding seal piece 222 is reset under the action of the spring 224, so that the reaction tank 21 is in a sealed state.
When the device is used, materials to be reacted are conveyed into the premixing tank 11 through the feeding pipe 111, the driving motor 121 is started, the driving motor 121 drives the stirring shaft 122 to drive the helical blade 123 to stir and premix the materials in the premixing tank 11, after premixing is completed, the electromagnet 224 is electrified, the electromagnet 224 adsorbs the sliding block 2223 to extrude the spring 224 and drives the sliding sealing piece 222 to integrally slide, the sealing head 2222 is separated from the groove 2212 to open the feeding port 2211, the premixed materials are conveyed into the inner reaction tank 21 through the feeding port 2211, after conveying is completed, the electromagnet 224 is powered off, the sliding sealing piece 222 is reset under the action of the spring 224, the feeding port 2211 is closed, the reaction tank 21 is in a sealed state, the motor 232 is started, the motor 232 drives the stirring rod 233 to drive the stirring blades 234 to stir the reaction materials in the reaction tank 21, and after reaction is completed, the materials are discharged and collected through the discharging pipe 211 at the bottom of the side wall of the reaction tank 21; the switch of feed inlet 2211 is controlled to the break-make electricity of staff's accessible electro-magnet to the material stirring in the control mixes the mechanism 1 in advance the time of mixing, improves the efficiency and the synthetic efficiency that stir and mix.
The above description is only a preferred embodiment of the present invention, and various changes and modifications can be made by those skilled in the art without departing from the scope of the present invention, and the changes and modifications also belong to the protection scope of the present invention.
Claims (9)
1. The utility model provides a synthesizer of heterogeneous mellow wine polyoxyethylene ether, its characterized in that, includes and mixes mechanism, stirring reaction mechanism, sealed lid in advance, stirring reaction mechanism top sets up sealed lid, mix the mechanism setting in advance in sealed lid top, sealed covering sets up feed inlet and sliding seal spare, opening and shutting of sliding seal spare control feed inlet, feed inlet intercommunication mixes mechanism and rabbling mechanism inner chamber in advance.
2. The synthesis device of isomeric alcohol polyoxyethylene ether according to claim 1, wherein the premixing mechanism comprises a premixing tank, a first stirring assembly; the first stirring assembly comprises a driving motor and a stirring shaft; the driving motor is installed at the top of the premixing tank, an output shaft of the driving motor is connected with the top end of the stirring shaft, the stirring shaft extends to the bottom in the premixing tank, and the part of the stirring shaft, which is positioned in the premixing tank, is provided with stirring blades in a surrounding manner.
3. The device for synthesizing isomeric alcohol polyoxyethylene ether according to claim 2, wherein a fixing frame is arranged on the inner side wall of the premixing tank, a bearing is mounted on the fixing frame, and the bottom end of the stirring shaft is arranged in the bearing in a penetrating manner.
4. The synthesis device of isomeric alcohol polyoxyethylene ether according to claim 2, wherein the feed inlet of the premixing mechanism is arranged at the top of the premixing tank.
5. The synthesis device of isomeric alcohol polyoxyethylene ether according to claim 1, wherein the stirring reaction mechanism comprises a reaction tank and a second stirring component; the second stirring assembly comprises a motor and a stirring rod, the motor is installed at the bottom end of the reaction tank, an output shaft of the motor is connected with the stirring rod, the stirring rod extends into the reaction tank, and stirring blades are installed on the part, located in the reaction tank, of the stirring rod.
6. The synthesis device of isomeric alcohol polyoxyethylene ether according to claim 5, wherein a mounting rack is arranged at the bottom of the reaction tank and used for mounting a motor; a plurality of support frames are arranged at the bottom of the reaction tank and used for supporting the whole device.
7. The synthesis device of isomeric alcohol polyoxyethylene ether according to claim 5, wherein the discharge port of the stirring reaction mechanism is arranged at the bottom of the side surface of the reaction tank.
8. The synthesis device of isomeric alcohol polyoxyethylene ether according to claim 1, wherein the sealing cover comprises a cover body and a sliding sealing piece; the feed inlet sets up on the lid, set up the recess that suits with sliding seal spare one end on the lateral wall of one side of feed inlet, set gradually on the lateral wall of opposite side with sliding seal spare other end suit the slide opening and with the spout, the one end of keeping away from the slide opening in the spout sets up the electro-magnet, sets up the spring between electro-magnet and the sliding seal spare.
9. The synthesis device of isomeric alcohol polyoxyethylene ether according to claim 8, wherein the sliding sealing element comprises a sliding plate, a sealing head and a sliding block; the sealing head and the sliding block are positioned on two sides of the sliding plate, the sealing head is matched with the groove, the sliding block is arranged in the sliding groove in a sliding mode, and two ends of the spring are respectively abutted to the sliding block and the electromagnet.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202223142690.3U CN218654475U (en) | 2022-11-25 | 2022-11-25 | Synthesizer of isomeric mellow wine polyoxyethylene ether |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202223142690.3U CN218654475U (en) | 2022-11-25 | 2022-11-25 | Synthesizer of isomeric mellow wine polyoxyethylene ether |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN218654475U true CN218654475U (en) | 2023-03-21 |
Family
ID=85540306
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202223142690.3U Active CN218654475U (en) | 2022-11-25 | 2022-11-25 | Synthesizer of isomeric mellow wine polyoxyethylene ether |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN218654475U (en) |
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2022
- 2022-11-25 CN CN202223142690.3U patent/CN218654475U/en active Active
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| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of utility model: A synthetic device for isomeric alcohol polyoxyethylene ether Granted publication date: 20230321 Pledgee: Bank of Jiangsu Co.,Ltd. Taixing sub branch Pledgor: TAIXING LINGFEI CHEMICAL TECHNOLOGY Co.,Ltd. Registration number: Y2024980029802 |
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| PE01 | Entry into force of the registration of the contract for pledge of patent right |