CN218654393U - 8-hydroxyquinoline preparation is with heat preservation retort with filter effect - Google Patents

8-hydroxyquinoline preparation is with heat preservation retort with filter effect Download PDF

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Publication number
CN218654393U
CN218654393U CN202221751522.1U CN202221751522U CN218654393U CN 218654393 U CN218654393 U CN 218654393U CN 202221751522 U CN202221751522 U CN 202221751522U CN 218654393 U CN218654393 U CN 218654393U
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China
Prior art keywords
retort
filter
heat
reaction tank
water conservancy
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CN202221751522.1U
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Chinese (zh)
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李霞
周向阳
周敏华
李卫国
汤中平
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Pingdingshan Aipu Chemical Co ltd
Henan University of Urban Construction
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Pingdingshan Aipu Chemical Co ltd
Henan University of Urban Construction
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Abstract

The utility model relates to an 8-hydroxyquinoline prepares technical field, discloses a 8-hydroxyquinoline preparation is with heat preservation retort with filter effect, including the retort, the surface of retort is provided with close ring, close ring's surface rotates and is connected with the inlet pipe, the top of inlet pipe is provided with the expansion fill, the inner wall of retort is provided with the conveyer pipe, the inside of retort is provided with the filter funnel, the internal surface of filter funnel is provided with the water conservancy diversion sieve. The utility model has the advantages of it is following and effect: can carry out the water conservancy diversion to the bottom of filter hopper through the water conservancy diversion sieve when reaction material gets into the inside of filter hopper, the surface of water conservancy diversion sieve can block partly impurity, when the material was through the surface of filter layer upon layer, reaction material can be attached to the surface of filter, the material after having the filter to filter gets into the inside of water conservancy diversion mouth and will stay the filtration through the filter screen once more, alright reduce the impurity among the reaction material from this and remain.

Description

8-hydroxyquinoline preparation is with heat preservation retort with filter effect
Technical Field
The utility model relates to an 8-hydroxyquinoline preparation technical field, in particular to 8-hydroxyquinoline preparation is with heat preservation retort with filter effect.
Background
8-hydroxyquinoline is an organic compound having the formula C9H7NO, a white or pale yellow crystal or crystalline powder, insoluble in water and diethyl ether, soluble in ethanol, acetone, chloroform, benzene or dilute acids, sublimable, useful as a preservative, disinfectant and insecticide, useful as a transcription inhibitor.
In the prior art, chinese patent publication No. CN208320789U discloses a reaction tank for preventing material deposition in the reaction tank, the reaction tank includes a motor, a reaction tank body, a reaction tank inner cavity, a stirrer, and a discharge valve, the discharge valve includes a valve core, a valve core top and a discharge port, the stirrer includes stirrer leaflets, the valve core top and the reaction tank bottom form an inner cavity, and the stirrer leaflets are located in the inner cavity or at the upper edge of the inner cavity. When the reaction tank works, the motor drives the stirrer to stir materials uniformly and fully react, and the materials and reaction sediments deposited at the bottom of the reaction tank are stirred by the small blades of the stirrer on the stirrer to fully react.
Have fine effect that prevents the reaction material deposit in the above-mentioned patent, but its retort is not convenient for filter the reaction material when using, and the retort heat preservation effect is not good, is not convenient for heat up and cool down to the inside temperature of retort, consequently need make the improvement to the problem that exists at present.
SUMMERY OF THE UTILITY MODEL
The utility model aims at providing a 8-hydroxyquinoline preparation is with heat preservation retort with filter effect has and is convenient for filter reaction material, and retort heat preservation effect is good, the effect of being convenient for rise temperature and cooling.
The above technical purpose of the present invention can be achieved by the following technical solutions: the utility model provides an 8-hydroxyquinoline preparation is with heat preservation retort with filter effect, includes the retort, the surface of retort is provided with the close ring that connects, the surface of close ring rotates and is connected with the inlet pipe, the top of inlet pipe is provided with the expansion fill, the inner wall of retort is provided with the conveyer pipe, the inside of retort is provided with the filter hopper, the internal surface of filter hopper is provided with the water conservancy diversion sieve, the inside of filter hopper is provided with the filter, the bottom of filter hopper is provided with the water conservancy diversion mouth, the inside of water conservancy diversion mouth is provided with the filter screen, the inside of retort is provided with the reacting chamber.
Through adopting above-mentioned technical scheme, the staff carries reaction material to the inside of fighting to filter by the conveyer pipe through the inlet pipe, fight through the expansion and increase the import scope of feeding and prevent that the material from leaking and spilling, can carry out the water conservancy diversion to the bottom of fighting to filter through the water conservancy diversion sieve through mixing reaction when reaction material gets into the inside of fighting, the surface of water conservancy diversion sieve can block partly impurity, when the material is through the surface of filter layer upon layer, reaction material can attach to the surface of filter, the material after having the filter to filter gets into the inside of water conservancy diversion mouth and will stop the filtration through the filter screen once more, from this alright reduce the impurity residue in the reaction material, promote reaction material's mixed reaction quality.
The utility model discloses a further set up to: the top of retort is provided with the sealing port, the top of sealing port is provided with the activity sealed lid.
Through adopting above-mentioned technical scheme, be convenient for seal and open the retort through the cooperation of seal opening and activity sealed lid to play sealed heat preservation effect when the material carries out the reaction, increase the discharge port when carrying out the heat extraction to retort inside and handling.
The utility model discloses a further set up to: the inner surface of the reaction tank is provided with a heat preservation layer, the outer surface of the heat preservation layer is provided with a heat conduction layer, and an electric heating tube is arranged inside the heat conduction layer.
By adopting the technical scheme, the worker starts the electric heating tube to heat in the heat conducting layer, so that the temperature required by the reaction is conveniently provided for the reaction materials, and the heating and heat preservation effects of the reaction tank are better under the matching action of the electric heating tube and the heat preservation layer.
The utility model discloses a further set up to: the outer surface of the reaction tank is provided with a sealing interface, and the outer surface of the sealing interface is sleeved with a ventilation pipe.
Through adopting above-mentioned technical scheme, through being connected ventilation pipe and sealing interface after the material reaction is accomplished, be convenient for carry out circulation ventilation to the inside of retort.
The utility model discloses a further set up to: one end of the ventilation pipe is provided with an air box, a rotating fan is arranged inside the air box, and an exhaust pipe is arranged on the outer surface of the air box.
Through adopting above-mentioned technical scheme, rotate the inside of ventilating to the retort through the ventilation pipe by changeing the fan in the inside of bellows, with the mating reaction of exhaust pipe, make its inside to the retort circulate the air supply and exhaust to make the inside cooling rate of retort faster.
The utility model discloses a further set up to: the one end of changeing the fan is provided with the pivot, the one end of pivot is provided with the motor.
Through adopting above-mentioned technical scheme, make the pivot rotate through starter motor and be convenient for changeing the fan and provide mechanical power, improve the efficiency of the cooling operation of airing exhaust, reduce staff's working strength and safety risk.
The utility model has the advantages that:
1. the utility model discloses, through the retort, the close ring that connects, the inlet pipe, the expansion is fought, the conveyer pipe, the filtration fill, the water conservancy diversion sieve, the filter, the water conservancy diversion mouth, cooperation setting between filter screen and the reacting chamber, can make this device when using, the staff passes through the inlet pipe and carries reaction material to the inside of filtering the fill by the conveyer pipe, it prevents that the material from spilling to increase the feed inlet scope through the expansion fill, can carry out the water conservancy diversion to the bottom of filtering the fill through the water conservancy diversion sieve through the mixing reaction when reaction material gets into the inside of filtering the fill, the surface of water conservancy diversion sieve can block partly impurity, when material through the surface of filter layer upon layer, reaction material can attach to the surface of filter, the material after having the filter filtration gets into the inside of water conservancy diversion mouth and stops the filter through the filter screen once more, from this alright reduction impurity among the reaction material is remained, promote reaction material's mixed reaction quality.
2. The utility model discloses, through the seal, the activity is sealed, the heat preservation, cooperation setting between heat-conducting layer and the electrothermal tube, can make this device when using, be convenient for seal and open the retort through the seal with the cooperation of activity sealing cover, thereby play sealed heat preservation effect when the material carries out the reaction, increase the discharge port when carrying out the heat extraction to retort inside and handling, the staff makes its inside at the heat-conducting layer generate heat through starting the electrothermal tube, thereby be convenient for provide the required temperature of reaction for reaction material, and the intensification heat preservation effect through the mating reaction messenger retort with the heat preservation is better.
Drawings
In order to more clearly illustrate the technical solutions in the embodiments of the present invention, the drawings needed to be used in the description of the embodiments will be briefly described below, and it is obvious that the drawings in the following description are only some embodiments of the present invention, and it is obvious for those skilled in the art to obtain other drawings without creative efforts.
FIG. 1 is a schematic structural view of the present invention;
FIG. 2 is a schematic view of the structure of the reaction tank of the present invention;
FIG. 3 is a schematic view of the heat-conducting layer of the present invention;
FIG. 4 is a schematic view of the structure of the bellows of the present invention.
In the figure, 1, a reaction tank; 2. a close connection ring; 3. a feed pipe; 4. expanding the hopper; 5. a delivery pipe; 6. a filter hopper; 7. a flow guide sieve; 8. a filter plate; 9. a flow guide port; 10. filtering with a screen; 11. a reaction chamber; 12. sealing the opening; 13. a movable sealing cover; 14. a heat-insulating layer; 15. a heat conductive layer; 16. an electric heating tube; 17. sealing the interface; 18. a vent pipe; 19. an air box; 20. rotating the fan; 21. an exhaust duct; 22. a rotating shaft; 23. an electric motor.
Detailed Description
The technical solution of the present invention will be clearly and completely described below with reference to the specific embodiments. It is to be understood that the disclosed embodiments are merely exemplary of the invention, and are not intended to limit the invention to the precise embodiments disclosed. Based on the embodiments of the present invention, all other embodiments obtained by a person skilled in the art without making creative efforts belong to the protection scope of the present invention.
Referring to fig. 1-4, a heat preservation reaction tank with filtering effect for preparing 8-hydroxyquinoline comprises a reaction tank 1, a sealing ring 2 is arranged on the outer surface of the reaction tank 1, a feeding pipe 3 is rotatably connected to the outer surface of the sealing ring 2, an expansion hopper 4 is arranged on the top of the feeding pipe 3, a conveying pipe 5 is arranged on the inner wall of the reaction tank 1, a filtering hopper 6 is arranged inside the reaction tank 1, a diversion screen 7 is arranged on the inner surface of the filtering hopper 6, a filtering plate 8 is arranged inside the filtering hopper 6, a diversion port 9 is arranged at the bottom of the filtering hopper 6, a filtering screen 10 is arranged inside the diversion port 9, a reaction chamber 11 is arranged inside the reaction tank 1, a worker conveys reaction materials from the conveying pipe 5 to the inside of the filtering hopper 6 through the feeding pipe 3, the feeding inlet range is increased through the expansion hopper 4 to prevent the leakage of the materials, when the reaction materials enter the inside of the filtering hopper 6, the reaction materials are guided to the bottom of the filtering hopper 6 through the diversion screen 7 through mixing reaction, the surface of the flow guide sieve 7 can block part of impurities, when materials pass through the surface of the layer-by-layer filter plate 8, reaction materials can be attached to the surface of the filter plate 8, the materials filtered by the filter plate 8 enter the interior of the flow guide port 9 and are stopped and filtered by the filter screen 10 again, therefore, the impurity residue in the reaction materials can be reduced, the mixed reaction quality of the reaction materials is improved, the top of the reaction tank 1 is provided with a sealing port 12, the top of the sealing port 12 is provided with a movable sealing cover 13, the reaction tank 1 can be conveniently sealed and opened through the matching of the sealing port 12 and the movable sealing cover 13, thereby, the sealing and heat preservation effects are achieved when the materials are reacted, discharge ports are increased when heat extraction treatment is performed on the interior of the reaction tank 1, the inner surface of the reaction tank 1 is provided with a heat preservation layer 14, the outer surface of heat preservation 14 is provided with heat-conducting layer 15, the inside of heat-conducting layer 15 is provided with electrothermal tube 16, the staff makes it generate heat in the inside of heat-conducting layer 15 through starting electrothermal tube 16, thereby be convenient for provide the required temperature of reaction for the reaction material, and it is better to make the intensification heat preservation effect of retort 1 through the mating reaction with heat preservation 14, the surface of retort 1 is provided with sealed interface 17, ventilation pipe 18 has been cup jointed to sealed interface 17's surface, through being connected ventilation pipe 18 and sealed interface 17 after the material reaction is accomplished, be convenient for circulate the ventilation to the inside of retort 1, the one end of ventilation pipe 18 is provided with bellows 19, the inside of bellows 19 is provided with commentaries on classics fan 20, the surface of bellows 19 is provided with exhaust pipe 21, by changeing fan 20 and rotating to carry out the ventilation through ventilation pipe 18 in the inside of bellows 19, with the mating reaction of bellows 21, make it circulate the air supply and exhaust to the inside of retort 1, thereby make the inside cooling rate of retort 1 faster, the one end of commentaries on classics fan 20 is provided with pivot 22, the one end of pivot 22 is provided with motor 23, it is convenient to rotate to make the pivot 22 provide the power for commentaries on classics fan cooling efficiency and reduce the security work of the staff's work, and reduce the risk of the work.
In the utility model, through the matching arrangement of the reaction tank 1, the tight-joint ring 2, the feeding pipe 3, the expansion hopper 4, the conveying pipe 5, the filtering hopper 6, the flow guide sieve 7, the filtering plate 8, the flow guide port 9, the filtering net 10 and the reaction chamber 11, when the device is used, a worker conveys reaction materials from the conveying pipe 5 to the inside of the filtering hopper 6 through the feeding pipe 3, the feed inlet range is increased through the expansion hopper 4 to prevent the materials from leaking, the reaction materials can be guided to the bottom of the filtering hopper 6 through the flow guide sieve 7 after the mixing reaction when entering the inside of the filtering hopper 6, the surface of the flow guide sieve 7 can block part of impurities, when the materials pass through the surface of the filtering plate 8 layer by layer, the reaction materials can be attached to the surface of the filtering plate 8, the materials filtered by the filtering plate 8 enter the inside of the flow guide port 9 and are filtered by the filtering net 10 again, therefore, the impurity residue in the reaction materials can be reduced, the mixed reaction quality of the reaction materials is improved, the reaction tank 1 can be conveniently sealed and opened through the matching of the sealing port 12, the movable sealing cover 13, the heat-insulating layer 14, the heat-conducting layer 15 and the electric heating tube 16 when the device is used, so that the sealing and heat-insulating effects are realized when the materials are reacted, the discharge port is increased when the heat extraction treatment is performed on the inside of the reaction tank 1, a worker can heat the inside of the heat-conducting layer 15 by starting the electric heating tube 16, the temperature required by the reaction is conveniently provided for the reaction materials, and the heating and heat-insulating effects of the reaction tank 1 are better through the matching effect with the heat-insulating layer 14.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims (6)

1. The utility model provides an 8-hydroxyquinoline preparation is with heat preservation retort with filter effect, includes retort (1), its characterized in that: the surface of retort (1) is provided with close ring (2), the surface of close ring (2) rotates and is connected with inlet pipe (3), the top of inlet pipe (3) is provided with expansion fill (4), the inner wall of retort (1) is provided with conveyer pipe (5), the inside of retort (1) is provided with filter hopper (6), the internal surface of filter hopper (6) is provided with water conservancy diversion sieve (7), the inside of filter hopper (6) is provided with filter (8), the bottom of filter hopper (6) is provided with water conservancy diversion mouth (9), the inside of water conservancy diversion mouth (9) is provided with filter screen (10), the inside of retort (1) is provided with reacting chamber (11).
2. The heat-preservation reaction tank with the filtering effect for preparing 8-hydroxyquinoline according to claim 1, characterized in that: the top of the reaction tank (1) is provided with a sealing opening (12), and the top of the sealing opening (12) is provided with a movable sealing cover (13).
3. The heat-preservation reaction tank with the filtering effect for preparing 8-hydroxyquinoline according to claim 1, characterized in that: the inner surface of the reaction tank (1) is provided with a heat insulation layer (14), the outer surface of the heat insulation layer (14) is provided with a heat conduction layer (15), and an electric heating tube (16) is arranged inside the heat conduction layer (15).
4. The heat-preservation reaction tank with the filtering effect for preparing 8-hydroxyquinoline according to claim 1, is characterized in that: the outer surface of the reaction tank (1) is provided with a sealing interface (17), and the outer surface of the sealing interface (17) is sleeved with a ventilation pipe (18).
5. The heat-preservation reaction tank with the filtering effect for preparing 8-hydroxyquinoline according to claim 4 is characterized in that: one end of the ventilation pipe (18) is provided with an air box (19), the inside of the air box (19) is provided with a rotating fan (20), and the outer surface of the air box (19) is provided with an exhaust pipe (21).
6. The heat-preservation reaction tank with the filtering effect for preparing 8-hydroxyquinoline according to claim 5, is characterized in that: one end of the rotating fan (20) is provided with a rotating shaft (22), and one end of the rotating shaft (22) is provided with a motor (23).
CN202221751522.1U 2022-07-09 2022-07-09 8-hydroxyquinoline preparation is with heat preservation retort with filter effect Active CN218654393U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202221751522.1U CN218654393U (en) 2022-07-09 2022-07-09 8-hydroxyquinoline preparation is with heat preservation retort with filter effect

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202221751522.1U CN218654393U (en) 2022-07-09 2022-07-09 8-hydroxyquinoline preparation is with heat preservation retort with filter effect

Publications (1)

Publication Number Publication Date
CN218654393U true CN218654393U (en) 2023-03-21

Family

ID=85552234

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202221751522.1U Active CN218654393U (en) 2022-07-09 2022-07-09 8-hydroxyquinoline preparation is with heat preservation retort with filter effect

Country Status (1)

Country Link
CN (1) CN218654393U (en)

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