CN218629676U - Detection is with entrapment equipment that sweeps - Google Patents

Detection is with entrapment equipment that sweeps Download PDF

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CN218629676U
CN218629676U CN202221737006.3U CN202221737006U CN218629676U CN 218629676 U CN218629676 U CN 218629676U CN 202221737006 U CN202221737006 U CN 202221737006U CN 218629676 U CN218629676 U CN 218629676U
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backup pad
pipe
gas storage
gas
liquid feeding
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崔贺坤
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Jiangsu Ningchen Beili Technology Co ltd
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Tianjin Zhongsheng Instrument Co ltd
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Abstract

The utility model discloses a detect with entrapment equipment that sweeps, including support frame, backup pad one, backup pad two, backup pad three, add the liquid storehouse, liquid feeding pipe, add liquid valve, lift cylinder, link, sealing plug and gas storage storehouse, backup pad one, backup pad two and backup pad three are located on the support frame, it locates on the backup pad three to add the liquid storehouse, the gas storage storehouse is located on backup pad one and the backup pad two, liquid feeding pipe one end is connected in adding the liquid storehouse, the liquid feeding pipe other end is connected in the gas storage storehouse. The utility model belongs to the technical field of the entrapment equipment that sweeps, specifically indicate that a structure is compacter, and convenient to use can be to the detection of water sample ration usefulness with the entrapment equipment that sweeps.

Description

一种检测用吹扫捕集设备A purge and trap device for detection

技术领域technical field

本实用新型属于吹扫捕集设备技术领域,具体是指一种检测用吹扫捕集设备。The utility model belongs to the technical field of purge and trap equipment, in particular to a purge and trap equipment for detection.

背景技术Background technique

现有生活中,吹扫捕集方法一般是用高纯氮气或者氦气作为载气吹扫室内的水样或土壤样品,将溶解在土壤或者水中的挥发性有机气体吹扫出来并富集至捕集管中,可常温进行捕集,吹扫结束后,捕集管瞬间加热,使捕集的待分析气体进入色谱仪内进行测定,如今吹扫捕集技术运用非常广泛。In the existing life, the purge and trap method is generally to use high-purity nitrogen or helium as the carrier gas to purge the water or soil samples in the chamber, and the volatile organic gases dissolved in the soil or water are purged out and enriched in the In the trapping tube, trapping can be carried out at room temperature. After the purge is completed, the trapping tube is heated instantaneously, so that the trapped gas to be analyzed enters the chromatograph for measurement. Nowadays, purge and trap technology is widely used.

公开号为CN209640303U的专利公开了一种挥发性有机物吹扫捕集装置,待测水样通过水泵由进液管进入到样品管内,惰性载气通过载气分散结构吹入样品管的底部,因载气分散结构由两个或多个带有排气孔的环形玻璃管组成,当惰性载气进入到环形玻璃管时会通过排气孔进入到待测水样,使得惰性载气与待测水样充分接触并产生许多微小气泡,待测水样中的挥发性有机物变成气态存在于惰性载气中,从而将待测水样中的挥发性有机物带出,对待测水样中的挥发性有机物吹扫更加均匀有效,而后经过三通阀二进入到气体干燥管进行水分吸收,再通过气体流通管道二进入到捕集管内,此过程不便于对水样进行定量取用,整体体积较大,使用不够便捷。The patent with the publication number CN209640303U discloses a volatile organic compound purging and trapping device. The water sample to be tested enters the sample tube from the liquid inlet pipe through the water pump, and the inert carrier gas is blown into the bottom of the sample tube through the carrier gas dispersion structure. The carrier gas dispersion structure is composed of two or more annular glass tubes with exhaust holes. When the inert carrier gas enters the annular glass tube, it will enter the water sample to be tested through the exhaust holes, so that the inert carrier gas and the sample to be tested The water sample is fully contacted and produces many tiny bubbles, and the volatile organic compounds in the water sample to be tested become gaseous and exist in the inert carrier gas, thereby taking out the volatile organic compounds in the water sample to be tested, and the volatile organic compounds in the water sample to be tested The purging of sexual organic matter is more uniform and effective, and then enters the gas drying pipe through the three-way valve 2 for moisture absorption, and then enters the trapping pipe through the gas circulation pipe 2. This process is not convenient for quantitatively taking water samples, and the overall volume is relatively small Big, not easy to use.

实用新型内容Utility model content

为了解决上述难题,本实用新型提供了一种结构更加紧凑,使用方便,可对水样定量取用的检测用吹扫捕集设备。In order to solve the above-mentioned problems, the utility model provides a more compact structure, easy to use, and a detection purge and trapping device that can quantitatively take water samples.

为了实现上述功能,本实用新型采取的技术方案如下:一种检测用吹扫捕集设备,包括支撑架、支撑板一、支撑板二、支撑板三、加液仓、加液管、加液阀门、升降气缸、连接架、密封塞和储气仓,所述支撑板一、支撑板二和支撑板三设于支撑架上,所述加液仓设于支撑板三上,所述储气仓设于支撑板一和支撑板二上,所述加液管一端连接于加液仓,所述加液管另一端连接于储气仓,所述加液阀门设于加液管上,所述密封塞设于储气仓内,所述连接架设于密封塞上,所述升降气缸一端设于储气仓顶壁下,所述升降气缸另一端设于连接架顶壁上,事先将惰性气体注于储气仓内,将定量的水置于加液仓内,打开加液阀门,将加液仓内的水从加液管流入到储气仓内,升降气缸带动连接架和密封塞上升,此时惰性气体在水中向上漂浮,将水样中挥发性的有机物带出。In order to achieve the above functions, the technical scheme adopted by the utility model is as follows: a detection purge and trapping device, including a support frame, support plate 1, support plate 2, support plate 3, liquid addition chamber, liquid addition pipe, liquid addition Valves, lifting cylinders, connecting frames, sealing plugs and gas storage bins, the first support plate, the second support plate and the third support plate are arranged on the support frame, the liquid adding bin is arranged on the third support plate, and the gas storage The warehouse is arranged on the support plate 1 and the support plate 2, one end of the liquid feeding pipe is connected to the liquid feeding chamber, the other end of the liquid feeding pipe is connected to the gas storage chamber, and the liquid feeding valve is arranged on the liquid feeding pipe. The sealing plug is set in the gas storage bin, the connection is erected on the sealing plug, one end of the lifting cylinder is set under the top wall of the gas storage bin, and the other end of the lifting cylinder is set on the top wall of the connecting frame. The gas is injected into the gas storage chamber, a certain amount of water is placed in the liquid filling chamber, the liquid filling valve is opened, the water in the liquid filling chamber flows into the gas storage chamber from the liquid filling pipe, and the lifting cylinder drives the connecting frame and the sealing plug Ascent, the inert gas floats upward in the water at this time, taking out the volatile organic compounds in the water sample.

优选地,所述支撑架外侧壁上设有支撑托架,所述支撑托架上设有捕集管,所述捕集管一端连接有连接管二,所述捕集管另一端连接有出气管,所述连接管二一端上连接有气体干燥管,所述气体干燥管和储气仓顶壁的连接处设有连接管一,所述连接管一贯穿支撑架侧壁设置,所述气体干燥管上固定套接有支撑套板,所述支撑套板套接于气体干燥管的同时设于支撑托架上,增加稳定性,将水样中挥发性的有机物带出,通过连接管一进入气体干燥管的内部,通过干燥剂颗粒对气体进行干燥,然后通过连接管二进入捕集管的内部,捕集管将挥发性有机物全部解析出来,并通过惰性载气的流动进入到色谱仪内进行检测。Preferably, a support bracket is provided on the outer wall of the support frame, and a collection tube is provided on the support bracket, one end of the collection tube is connected to a connecting pipe 2, and the other end of the collection tube is connected to an outlet A gas pipe, one end of the connecting pipe 2 is connected with a gas drying pipe, the connection between the gas drying pipe and the top wall of the gas storage bin is provided with a connecting pipe 1, and the connecting pipe 1 is arranged through the side wall of the support frame, and the The gas drying tube is fixedly sleeved with a support sleeve, and the support sleeve is sleeved on the gas drying tube and set on the support bracket at the same time to increase stability, take out the volatile organic matter in the water sample, and pass through the connecting tube One enters the inside of the gas drying tube, dries the gas through the desiccant particles, and then enters the inside of the trapping tube through the connecting tube two, and the trapping tube resolves all volatile organic compounds, and enters the chromatographic through the flow of inert carrier gas In-device testing.

优选地,所述储气仓内侧壁上设有内支架,所述连接架外侧壁上设有套接块,所述套接块贯穿内支架滑动设置,增加连接架移动时的稳定性。Preferably, an inner support is provided on the inner side wall of the gas storage chamber, and a socket block is provided on the outer wall of the connecting frame, and the socket block is slidably arranged through the inner frame to increase the stability of the connecting frame when moving.

优选地,所述密封塞上设有导流板,所述导流板侧壁倾斜设置,水流顺着导流板侧壁流下。Preferably, the sealing plug is provided with a deflector, the side wall of the deflector is inclined, and the water flows down along the side wall of the deflector.

优选地,所述加液仓为U形结构,所述加液仓外侧壁上设有刻度尺,辅助观察,对加液仓内的水定量加入。Preferably, the liquid addition chamber has a U-shaped structure, and a scale is provided on the outer wall of the liquid addition chamber to assist observation and quantitatively add water in the liquid addition chamber.

优选地,所述储气仓底部为U形结构,所述储气仓底壁下设有进气口,所述进气口上设有进气阀,便于箱储气仓内注入惰性气体。Preferably, the bottom of the gas storage bin has a U-shaped structure, an air inlet is provided under the bottom wall of the gas storage bin, and an air inlet valve is provided on the air inlet to facilitate the injection of inert gas into the gas storage bin.

本实用新型采取上述结构取得有益效果如下:本实用新型提供的一种检测用吹扫捕集设备,整体结构紧凑,使用方便,通过储气仓事先将惰性气体注于储气仓内,将定量的水置于加液仓内,打开加液阀门,将加液仓内的水从加液管流入到储气仓内,升降气缸带动连接架和密封塞上升,此时惰性气体在水中向上漂浮,将水样中挥发性的有机物带出,通过连接管一进入气体干燥管的内部,通过干燥剂颗粒对气体进行干燥,然后通过连接管二进入捕集管的内部,捕集管将挥发性有机物全部解析出来,并通过惰性载气的流动进入到色谱仪内进行检测,通过刻度尺辅助观察,对加液仓内的水定量加入。The utility model adopts the above-mentioned structure to obtain the following beneficial effects: a detection purge and trapping device provided by the utility model has a compact overall structure and is easy to use. Put the water in the liquid filling chamber, open the liquid filling valve, and let the water in the liquid filling chamber flow into the gas storage chamber from the liquid filling pipe. The lifting cylinder drives the connecting frame and the sealing plug to rise, and the inert gas floats upward in the water , take out the volatile organic matter in the water sample, enter the gas drying tube through the connecting tube one, dry the gas through the desiccant particles, and then enter the trapping tube through the connecting tube two, the trapping tube will volatile All the organic matters are resolved, and enter the chromatograph through the flow of inert carrier gas for detection, and use the scale to assist in observation, and quantitatively add the water in the liquid addition chamber.

附图说明Description of drawings

图1为本实用新型一种检测用吹扫捕集设备的整体结构图;Fig. 1 is the overall structural diagram of a kind of detection purge and trapping equipment of the present invention;

图2为图1中A处的局部放大图。FIG. 2 is a partial enlarged view of A in FIG. 1 .

其中,1、支撑架,2、支撑板一,3、支撑板二,4、支撑板三,5、加液仓,6、加液管,7、加液阀门,8、升降气缸,9、连接架,10、密封塞,11、储气仓,12、连接管一,13、连接管二,14、支撑套板,15、气体干燥管,16、出气管,17、捕集管,18、支撑托架,19、刻度尺,20、进气口,21、进气阀,22、导流板,23、套接块,24、内支架。Among them, 1. Support frame, 2. Support plate one, 3. Support plate two, 4. Support plate three, 5. Liquid filling chamber, 6. Liquid filling pipe, 7. Liquid filling valve, 8. Lifting cylinder, 9, Connecting frame, 10, sealing plug, 11, gas storage bin, 12, connecting pipe one, 13, connecting pipe two, 14, supporting sleeve plate, 15, gas drying pipe, 16, gas outlet pipe, 17, collecting pipe, 18 , support bracket, 19, scale, 20, air inlet, 21, air inlet valve, 22, deflector, 23, socket block, 24, inner bracket.

具体实施方式Detailed ways

下面将结合附图对本实用新型的技术方案进行清楚、完整地描述,显然,所描述的实施例是本实用新型一部分实施例,而不是全部的实施例。基于本实用新型中的实施例,本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例,都属于本实用新型保护的范围。The technical solutions of the utility model will be clearly and completely described below in conjunction with the accompanying drawings. Apparently, the described embodiments are part of the embodiments of the utility model, but not all of them. Based on the embodiments of the present utility model, all other embodiments obtained by persons of ordinary skill in the art without making creative efforts belong to the scope of protection of the present utility model.

在本实用新型的描述中,需要说明的是,术语“中心”、“上”、“下”、“左”、“右”、“竖直”、“水平”、“内”、“外”等指示的方位或位置关系为基于附图所示的方位或位置关系,仅是为了便于描述本实用新型和简化描述,而不是指示或暗示所指的装置或元件必须具有特定的方位、以特定的方位构造和操作,因此不能理解为对本实用新型的限制。此外,术语“第一”、“第二”、“第三”仅用于描述目的,而不能理解为指示或暗示相对重要性。以下结合附图,对本实用新型做进一步详细说明。In the description of the present utility model, it should be noted that the terms "center", "upper", "lower", "left", "right", "vertical", "horizontal", "inner", "outer" The orientation or positional relationship indicated by etc. is based on the orientation or positional relationship shown in the drawings, which is only for the convenience of describing the utility model and simplifying the description, rather than indicating or implying that the device or element referred to must have a specific orientation, use a specific The azimuth structure and operation, therefore can not be construed as the limitation of the present utility model. In addition, the terms "first", "second", and "third" are used for descriptive purposes only, and should not be construed as indicating or implying relative importance. Below in conjunction with accompanying drawing, the utility model is described in further detail.

如图1-2所示,本实用新型一种检测用吹扫捕集设备,包括支撑架1、支撑板一2、支撑板二3、支撑板三4、加液仓5、加液管6、加液阀门7、升降气缸8、连接架9、密封塞10和储气仓11,支撑板一2、支撑板二3和支撑板三4设于支撑架1上,加液仓5设于支撑板三4上,加液仓5为U形结构,加液仓5外侧壁上设有刻度尺19,储气仓11设于支撑板一2和支撑板二3上,储气仓11底部为U形结构,储气仓11底壁下设有进气口20,进气口20上设有进气阀21,加液管6一端连接于加液仓5,加液管6另一端连接于储气仓11,加液阀门7设于加液管6上,密封塞10设于储气仓11内,连接架9设于密封塞10上,升降气缸8一端设于储气仓11顶壁下,升降气缸8另一端设于连接架9顶壁上。As shown in Figure 1-2, the utility model is a kind of purge and trapping equipment for detection, including a support frame 1, a support plate 2, a support plate 2 3, a support plate 3 4, a liquid addition chamber 5, and a liquid addition pipe 6 , liquid filling valve 7, lifting cylinder 8, connecting frame 9, sealing plug 10 and gas storage bin 11, supporting plate one 2, supporting plate two 3 and supporting plate three 4 are arranged on the supporting frame 1, and liquid adding bin 5 is located on On the support plate three 4, the liquid filling chamber 5 is a U-shaped structure, a scale 19 is arranged on the outer wall of the liquid adding chamber 5, the gas storage chamber 11 is arranged on the support plate one 2 and the support plate two 3, and the bottom of the gas storage chamber 11 It is a U-shaped structure, an air inlet 20 is provided under the bottom wall of the gas storage bin 11, an air inlet valve 21 is arranged on the air inlet 20, one end of the liquid feeding pipe 6 is connected to the liquid feeding chamber 5, and the other end of the liquid feeding pipe 6 is connected to In the gas storage bin 11, the liquid filling valve 7 is set on the liquid filling pipe 6, the sealing plug 10 is set in the gas storage bin 11, the connecting frame 9 is set on the sealing plug 10, and one end of the lifting cylinder 8 is set on the top of the gas storage bin 11 Under the wall, the lifting cylinder 8 other ends are located on the connecting frame 9 top walls.

如图1所示,支撑架1外侧壁上设有支撑托架18,支撑托架18上设有捕集管17,捕集管17一端连接有连接管二13,捕集管17另一端连接有出气管16,连接管二13一端上连接有气体干燥管15,气体干燥管15和储气仓11顶壁的连接处设有连接管一12,连接管一12贯穿支撑架1侧壁设置,气体干燥管15上固定套接有支撑套板14,支撑套板14套接于气体干燥管15的同时设于支撑托架18上。As shown in Figure 1, a support bracket 18 is provided on the outer wall of the support frame 1, and a catch tube 17 is provided on the support bracket 18, and one end of the catch tube 17 is connected with a connecting pipe 13, and the other end of the catch tube 17 is connected to There is a gas outlet pipe 16, one end of the connecting pipe 13 is connected with a gas drying pipe 15, the connection between the gas drying pipe 15 and the top wall of the gas storage bin 11 is provided with a connecting pipe 12, and the connecting pipe 12 is arranged through the side wall of the support frame 1 , the gas drying pipe 15 is fixedly sleeved with a supporting sleeve 14 , and the supporting sleeve 14 is sleeved on the gas drying pipe 15 and is set on the supporting bracket 18 at the same time.

如图2所示,储气仓11内侧壁上设有内支架24,连接架9外侧壁上设有套接块23,套接块23贯穿内支架24滑动设置,密封塞10上设有导流板22,导流板22侧壁倾斜设置。As shown in Figure 2, an inner bracket 24 is provided on the inner side wall of the gas storage bin 11, a socket block 23 is provided on the outer wall of the connecting frame 9, the socket block 23 slides through the inner bracket 24, and the sealing plug 10 is provided with a guide. The flow plate 22 and the side wall of the flow guide plate 22 are arranged obliquely.

具体使用时,事先将惰性气体注于储气仓11内,将定量的水置于加液仓5内,通过刻度尺19辅助观察,对加液仓5内的水定量加入,加入完成之后,打开加液阀门7,将加液仓5内的水从加液管6流入到储气仓11内,水将储气仓11顶部密封,升降气缸8带动连接架9和密封塞10上升,此时惰性气体在水中向上漂浮,将水样中挥发性的有机物带出,通过连接管一12进入气体干燥管15的内部,通过干燥剂颗粒对气体进行干燥,然后通过连接管二13进入捕集管17的内部,捕集管17将挥发性有机物全部解析出来,并通过惰性载气的流动进入到色谱仪内进行检测。During specific use, inert gas is injected into the gas storage bin 11 in advance, a certain amount of water is placed in the liquid addition bin 5, and the water in the liquid addition bin 5 is quantitatively added through the scale 19 for auxiliary observation. After the addition is completed, Open the liquid filling valve 7, and the water in the liquid filling chamber 5 will flow into the air storage chamber 11 from the liquid filling pipe 6, and the water will seal the top of the air storage chamber 11, and the lifting cylinder 8 will drive the connecting frame 9 and the sealing plug 10 to rise. When the inert gas floats upwards in the water, the volatile organic matter in the water sample is taken out, enters the inside of the gas drying pipe 15 through the connecting pipe 12, and dries the gas through the desiccant particles, and then enters the trapping pipe through the connecting pipe 2 13 Inside the tube 17, the trapping tube 17 resolves all the volatile organic compounds, and enters the chromatograph through the flow of the inert carrier gas for detection.

以上对本实用新型及其实施方式进行了描述,这种描述没有限制性,附图中所示的也只是本实用新型的实施方式之一,实际的结构并不局限于此。总而言之如果本领域的普通技术人员受其启示,在不脱离本实用新型创造宗旨的情况下,不经创造性的设计出与该技术方案相似的结构方式及实施例,均应属于本实用新型的保护范围。The utility model and its implementation have been described above. This description is not restrictive. What is shown in the drawings is only one implementation of the utility model, and the actual structure is not limited thereto. All in all, if a person of ordinary skill in the art is inspired by it, without departing from the purpose of the utility model, without creatively designing a structural method and embodiment similar to the technical solution, it shall be protected by the utility model scope.

Claims (6)

1. The utility model provides a detection is with sweeping entrapment equipment which characterized in that: including support frame, backup pad one, backup pad two, backup pad three, add liquid storehouse, liquid feeding pipe, liquid feeding valve, lift cylinder, link, sealing plug and gas storage storehouse, backup pad one, backup pad two and backup pad three are located on the support frame, add the liquid storehouse and locate on the backup pad three, the gas storage storehouse is located on backup pad one and the backup pad two, liquid feeding pipe one end is connected in adding the liquid storehouse, the liquid feeding pipe other end is connected in the gas storage storehouse, the liquid feeding valve is located on the liquid feeding pipe, the sealing plug is located in the gas storage storehouse, the link is located on the sealing plug, lift cylinder one end is located under the gas storage storehouse roof, the lift cylinder other end is located on the link roof.
2. A purge and trap apparatus for testing according to claim 1, wherein: the gas storage bin is characterized in that a supporting bracket is arranged on the outer side wall of the supporting frame, a collecting pipe is arranged on the supporting bracket, one end of the collecting pipe is connected with a second connecting pipe, the other end of the collecting pipe is connected with a gas outlet pipe, one end of the second connecting pipe is connected with a gas drying pipe, a first connecting pipe is arranged at the joint of the gas drying pipe and the top wall of the gas storage bin, a first connecting pipe penetrates through the side wall of the supporting frame, a supporting sleeve plate is fixedly sleeved on the gas drying pipe, and the supporting sleeve plate is sleeved on the supporting bracket when the gas drying pipe is arranged.
3. A purge and trap apparatus for testing according to claim 2, wherein: the inner side wall of the gas storage bin is provided with an inner support, the outer side wall of the connecting frame is provided with a sleeving block, and the sleeving block penetrates through the inner support to be arranged in a sliding mode.
4. A purge and trap apparatus for testing according to claim 3, wherein: and a guide plate is arranged on the sealing plug, and the side wall of the guide plate is obliquely arranged.
5. The purge and trap apparatus for testing according to claim 4, wherein: the liquid feeding bin is of a U-shaped structure, and a graduated scale is arranged on the outer side wall of the liquid feeding bin.
6. A purge and trap apparatus for testing according to claim 5, wherein: the bottom of the gas storage bin is of a U-shaped structure, an air inlet is formed in the bottom wall of the gas storage bin, and an air inlet valve is arranged on the air inlet.
CN202221737006.3U 2022-07-05 2022-07-05 Detection is with entrapment equipment that sweeps Active CN218629676U (en)

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