CN218609390U

CN218609390U - Formula chemical industry reation kettle breaks up in advance

Info

Publication number: CN218609390U
Application number: CN202222968549.2U
Authority: CN
Inventors: 刘建贵; 赵德斌; 吴其安; 钱云建; 崔平
Original assignee: Anhui Delongtai Chemical Co ltd
Current assignee: Anhui Delongtai Chemical Co ltd
Priority date: 2022-11-08
Filing date: 2022-11-08
Publication date: 2023-03-14
Anticipated expiration: 2032-11-08

Abstract

The utility model provides a pre-scattering chemical reaction kettle, which comprises a stirring tank; the upper end face of the stirring tank is fixedly connected with a double-shaft motor, one end of an output shaft of the double-shaft motor is provided with a stirring device, the other end of the output shaft of the double-shaft motor is provided with a feeding device, the upper end of the stirring tank is fixedly connected with a crushing tank, the upper end face of the crushing tank is rotatably connected with a sealing plate through a hinge, the lower end face of the crushing tank is fixedly connected with a discharging pipe, and the middle part of the inner cavity of the crushing tank is fixedly connected with a filter plate; the feeding device comprises a T-shaped rod and a transmission rod, a transmission rod is fixedly connected with an output shaft of the double-shaft motor, a rotary rod is rotatably connected to the upper portion of the outer surface of the transmission rod through a chain wheel matched with a chain, the T-shaped rod is fixedly connected to the upper end face of the stirring tank, and the transmission rod and the rotary rod are respectively rotatably connected to the two ends of the inner cavity of the T-shaped rod. The utility model discloses a crushing unit has realized the crushing to the material that adds to and the material after smashing carries out even unloading.

Description

Formula chemical industry reation kettle breaks up in advance

Technical Field

The utility model relates to a reation kettle technical field, concretely relates to formula chemical industry reation kettle breaks up in advance.

Background

Aluminum trichloride (also known as aluminum chloride) is an inorganic compound having the chemical formula AlCl3, which is a compound of chlorine and aluminum. Aluminum chloride has a low melting point and a low boiling point, and sublimes to form a covalent compound. Molten aluminum chloride is not readily conductive and is distinguished from most salts containing halogen ions, such as sodium chloride.

At present, when 2,4,6-trimethylbenzoyl chloride is produced, 368g of aluminum trichloride and 1100g of mesitylene are added into a reaction kettle, the mixture of 150g of hydrochloric acid and 900g of water is added into the reaction kettle after stirring and reaction, trimethylbenzene is obtained after the reaction, 2,4,6-trimethylbenzoic acid is obtained after freeze dehydration and filtration, and finally the acyl chlorination reaction is carried out, because most of the existing aluminum trichloride is powdery, if the existing aluminum trichloride is not placed in a dry place, the existing aluminum trichloride is easy to be corroded by moisture in the air when being stored, so that the powdery aluminum trichloride forms hardening, and if the existing aluminum trichloride is directly added into raw materials for stirring reaction, the following problems are easy to exist;

because most of the existing aluminum trichloride are powdery, if the aluminum trichloride is directly placed in a reaction kettle for stirring after hardening is formed, the aluminum trichloride is not easy to fully react with raw materials in the reaction kettle, and the reaction efficiency is also reduced.

In summary, there is a need for a reactor that can break up materials.

SUMMERY OF THE UTILITY MODEL

Not enough to prior art, the utility model provides a formula chemical industry reation kettle breaks up in advance has solved the problem of mentioning in the background art.

In order to achieve the above purpose, the utility model discloses a following technical scheme realizes:

a pre-scattering chemical reaction kettle comprises a stirring tank; the upper end face of the stirring tank is fixedly connected with a double-shaft motor, one end of an output shaft of the double-shaft motor is provided with a stirring device, the other end of the output shaft of the double-shaft motor is provided with a feeding device, the upper end of the stirring tank is fixedly connected with a crushing tank, the upper end face of the crushing tank is rotatably connected with a sealing plate through a hinge, the lower end face of the crushing tank is fixedly connected with a discharging pipe, and the middle part of the inner cavity of the crushing tank is fixedly connected with a filter plate; feeding device includes T type pole and transfer line, double-shaft motor output shaft end fixedly connected with transfer line, transfer line surface upper portion is rotated through sprocket cooperation chain and is connected with the rotary rod, agitator tank up end fixedly connected with T type pole, the both ends of T type pole inner chamber are rotated respectively and are connected with transfer line and rotary rod, rotary rod one end is run through the filter plate and is rotated with the filter plate and be connected, crushing unit is installed on rotary rod surface upper portion, unloading subassembly is installed to rotary rod surface lower part.

Further, crushing unit includes crushing pole and solid fixed ring, the crushing pole of rotary rod surface upper portion fixedly connected with, the rotary rod surface just is located the solid fixed ring of crushing pole lower part fixedly connected with, gu fixed ring surface rotates and is connected with crushing roller, crushing roller surface and filter plate up end contact each other, gu fixed ring surface fixedly connected with scraper blade, terminal surface and filter plate up end contact each other under the scraper blade.

Further, the unloading subassembly includes unloading pole, slant pole and flood dragon blade, the rotary rod surface just is located filter plate lower part fixedly connected with unloading pole, the rotary rod surface just is located unloading pole lower part fixedly connected with slant pole, slant pole one side and crushing jar inner chamber wall in contact with each other, rotary rod surface lower part fixedly connected with flood dragon blade, the flood dragon blade is located the unloading pipe inner chamber.

Further, agitating unit includes the (mixing) shaft, biax motor output shaft end fixedly connected with (mixing) shaft, (mixing) shaft one end runs through the agitator tank and rotates with the agitator tank to be connected, the circular screen cloth of (mixing) shaft up end fixedly connected with, equidistant fixedly connected with puddler in (mixing) shaft middle part, terminal surface fixedly connected with U type pole under the (mixing) shaft, terminal surface in contact with each other under U type pole and the agitator tank, U type pole both sides respectively with agitator tank inner chamber wall in contact with each other, unloading pipe one end runs through the agitator tank and extends to circular screen cloth upper portion.

Further, agitator tank up end fixedly connected with inlet pipe, the row's of terminal surface middle part fixedly connected with material pipe under the agitator tank, the valve is installed respectively to inlet pipe and row's material intraductal chamber, agitator tank inner chamber wall top fixedly connected with L type pole, L type pole one side fixedly connected with brush, terminal surface contaction under brush one end and the circular screen cloth.

The utility model provides a formula chemical industry reation kettle breaks up in advance. Compared with the prior art, the method has the following beneficial effects:

1. realized smashing the powder material of balling through the crushing unit among the feeding device, prevented that the powder material of balling from entering into the agitator tank to be not convenient for the even mixture in later stage, and after smashing, filter the powder material, prevent that impurity from entering into the agitator tank, lead to raw materials quality to descend.

2. Through mutually supporting of the circular screen cloth in unloading subassembly and the agitating unit among the feeding device, realized carrying out even unloading to the powder after smashing to and carry out even scattering in the agitator tank with it and carry out even mixture with the powder after smashing.

Drawings

In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings used in the description of the embodiments or the prior art will be briefly described below, it is obvious that the drawings in the following description are only some embodiments of the present invention, and for those skilled in the art, other drawings can be obtained according to these drawings without creative efforts.

Fig. 1 shows the overall structure of the present invention;

FIG. 2 is a schematic view of the overall structure of the present invention;

FIG. 3 is a schematic view of the structure of the present invention with another view angle;

fig. 4 is an enlarged schematic view of the area a in fig. 2 according to the present invention;

FIG. 5 is a schematic view of the structure of the crushing tank and the blanking pipe of the present invention;

FIG. 6 shows a schematic view of a sectional structure of the crushing tank and the blanking pipe of the present invention;

shown in the figure: 1. a stirring tank; 2. a dual-axis motor; 3. a stirring device; 31. a stirring shaft; 32. a circular screen; 33. a stirring rod; 34. a U-shaped rod; 4. a feeding device; 41. a T-shaped rod; 42. a transmission rod; 43. rotating the rod; 44. a size reduction assembly; 441. crushing the stems; 442. a fixing ring; 443. a crushing roller; 444. a squeegee; 45. a blanking assembly; 451. a blanking rod; 452. an oblique rod; 453. flood dragon leaves; 5. a grinding tank; 6. a sealing plate; 7. a discharging pipe; 8. filtering the plate; 9. a feeding pipe; 10. a discharge pipe; 11. an L-shaped rod; 12. and a brush.

Detailed Description

To make the objects, technical solutions and advantages of the embodiments of the present invention clearer, the technical solutions in the embodiments of the present invention are clearly and completely described, and it is obvious that the described embodiments are some, but not all embodiments of the present invention. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative efforts belong to the protection scope of the present invention.

Example one

In order to solve the technical problems in the background art, the following pre-scattering chemical reaction kettle is provided:

referring to fig. 1-6, the utility model provides a pre-dispersing chemical reaction kettle, which comprises a stirring tank 1; the upper end face of the stirring tank 1 is fixedly connected with a double-shaft motor 2, one end of an output shaft of the double-shaft motor 2 is provided with a stirring device 3, the other end of the output shaft of the double-shaft motor 2 is provided with a feeding device 4, the upper end of the stirring tank 1 is fixedly connected with a crushing tank 5, the upper end face of the crushing tank 5 is rotatably connected with a sealing plate 6 through a hinge, the lower end face of the crushing tank 5 is fixedly connected with a discharging pipe 7, and the middle part of an inner cavity of the crushing tank 5 is fixedly connected with a filter plate 8; the feeding device 4 comprises a T-shaped rod 41 and a transmission rod 42, the output shaft end of the double-shaft motor 2 is fixedly connected with the transmission rod 42, the upper part of the outer surface of the transmission rod 42 is rotatably connected with a rotating rod 43 through a chain wheel matched with a chain, the upper end surface of the stirring tank 1 is fixedly connected with the T-shaped rod 41, two ends of the inner cavity of the T-shaped rod 41 are respectively rotatably connected with the transmission rod 42 and the rotating rod 43, one end of the rotating rod 43 penetrates through the filter plate 8 and is rotatably connected with the filter plate 8, the upper part of the outer surface of the rotating rod 43 is provided with a crushing assembly 44, and the lower part of the outer surface of the rotating rod 43 is provided with a blanking assembly 45.

Through closing plate 6, can reduce when smashing powdered material, lead to a large amount of dusts in the material to spill over to the polluted environment influences personnel's healthy.

As an improvement of the above technical solution, the crushing assembly 44 includes a crushing rod 441 and a fixing ring 442, the upper portion of the outer surface of the rotating rod 43 is fixedly connected with the crushing rod 441, the outer surface of the rotating rod 43 and the lower portion of the crushing rod 441 are fixedly connected with the fixing ring 442, the outer surface of the fixing ring 442 is rotatably connected with a crushing roller 443, the outer surface of the crushing roller 443 contacts with the upper end surface of the filter plate 8, the outer surface of the fixing ring 442 is fixedly connected with a scraper 444, and the lower end surface of the scraper 444 contacts with the upper end surface of the filter plate 8. The blanking assembly 45 comprises a blanking rod 451, an inclined rod 452 and a dragon blade 453, the blanking rod 451 is fixedly connected to the outer surface of the rotating rod 43 and is located on the lower portion of the filter plate 8, the inclined rod 452 is fixedly connected to the outer surface of the rotating rod 43 and is located on the lower portion of the blanking rod 451, one side of the inclined rod 452 is in contact with the wall of the inner cavity of the crushing tank 5, the dragon blade 453 is fixedly connected to the lower portion of the outer surface of the rotating rod 43, and the dragon blade 453 is located in the inner cavity of the blanking pipe 7.

Through crushing unit 44, realized smashing the powder material that becomes the group form to filtering the powder material that smashes, the powder material after the filtration will be through the flood dragon blade 453 in unloading subassembly 45, carry out even conveying circular screen 32 with it in, make things convenient for the later stage to carry out even scattering with the powder material after smashing and fall in agitator tank 1, make things convenient for the even stirring in later stage.

Example two

As shown in fig. 1 to fig. 6, on the basis of the above embodiments, the present embodiment further provides the following:

agitating unit 3 includes (mixing)

shaft

31, 2 output shaft end fixedly connected with (mixing) shaft 31 of biax motor, 31 one end of (mixing) shaft runs through agitator tank 1 and rotates with agitator tank 1 and be connected, 31 up end fixedly connected with circular screen cloth 32 of (mixing) shaft, 31 equidistant fixedly connected with puddler 33 in the middle part of (mixing) shaft, 31 end fixedly connected with U type pole 34 under the (mixing) shaft, end face and agitator tank 1 end face contact each other under U type pole 34, U type pole 34 both sides respectively with 1 inner chamber wall of agitator tank contact each other, 7 one ends of unloading pipe run through agitator tank 1 and extend to circular screen cloth 32 upper portion.

Through the rotation of circular screen 32, realized scattering evenly the material after smashing in agitator tank 1, then puddler 33 and U type pole 34 carry out abundant stirring with the raw materials in agitator tank 1 with it.

EXAMPLE III

the upper end face of the stirring tank 1 is fixedly connected with a feeding pipe 9, the middle part of the lower end face of the stirring tank 1 is fixedly connected with a discharging pipe 10, the inner cavities of the feeding pipe 9 and the discharging pipe 10 are respectively provided with a valve, the top of the inner cavity wall of the stirring tank 1 is fixedly connected with an L-shaped rod 11, one side of the L-shaped rod 11 is fixedly connected with a brush 12, and one end of the brush 12 is in mutual contact with the lower end face of the circular screen 32.

Can clear up circular screen 32 lower part through brush 12, prevent that circular screen 32 from appearing blockking up, and then the interpolation of the later stage material of being not convenient for to and the stirring in later stage.

The utility model discloses a theory of operation and use flow:

in the use state:

firstly, raw materials to be made are placed in a stirring tank 1 for reaction, when the materials are required to be added in later period, the materials are added into a crushing tank 5, after the materials are added, a sealing plate 6 is rotated to the crushing tank 5, so that dust prevention is prevented from floating out of the upper part of the crushing tank 5 when the powdery materials in the crushing tank 5 are crushed in later period, after the materials are placed, a double-shaft motor 2 is started, the double-shaft motor 2 drives a transmission rod 42 to rotate, when the transmission rod 42 rotates, a rotating rod 43 is driven to rotate through a chain wheel matched with a chain, when the rotating rod 43 rotates, the rotating rod 43 respectively drives a crushing assembly 44 and a blanking assembly 45 to rotate, when the crushing assembly 44 rotates, the crushing rod 441, the crushing roller 443 and a scraper 444 are respectively driven to rotate, and when the crushing rod 441 rotates, at this time, the agglomerated powder can be scattered through the pulverizing rod 441, when the pulverizing roller 443 rotates, the filter plates 8 are matched with each other, and the smaller agglomerated powder is crushed, so that the crushed powder falls into the lower portion of the pulverizing tank 5 from the filter plates 8, when the scraper 444 rotates, the powder adhered to the filter plates 8 can be scraped through the scraper 444, the filter holes on the filter plates 8 are prevented from being blocked by the powder, when the crushed powder enters the lower portion of the pulverizing tank 5, the powder can be stirred and scattered again through the rotation of the blanking rod 451 and the diagonal rod 452 in the blanking assembly 45, finally, the pulverized powder is uniformly conveyed into the circular screen 32 through the blanking tube 7 by the rotation of the auger blade 453 in the blanking assembly 45, and when the dual-shaft motor 2 operates, the dual-shaft motor 2 drives the stirring shaft 31 to rotate, will drive circular screen 32 respectively when (mixing) shaft 31 rotates, puddler 33, U type pole 34 rotates, when circular screen 32 rotates, at this moment can carry out even scattering in agitator tank 1 through the material after circular screen 32 will smash, then carry out intensive mixing through puddler 33 and U type pole 34, make the material carry out the more even that mixes with the raw materials, during the stirring, scrape through U type pole 34 and get agitator tank 1 inner wall and bottom, prevent that the material from adhering on the inner wall, lead to the loss of material.

And (2) totaling: the aforesaid has realized smashing the material of bulk through agitating unit and feeding device, smashes the back to filter it, filter the back, carry out even pay-off, then carry out even spilling the material and fall in the agitator tank, thereby make things convenient for the later stage faster carry out even stirring to it.

It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus. Without further limitation, an element defined by the phrase "comprising a … …" does not exclude the presence of another identical element in a process, method, article, or apparatus that comprises the element.

The above embodiments are only used to illustrate the technical solution of the present invention, and not to limit it; although the present invention has been described in detail with reference to the foregoing embodiments, it should be understood by those skilled in the art that: the technical solutions described in the foregoing embodiments may still be modified, or some technical features may be equivalently replaced; such modifications and substitutions do not depart from the spirit and scope of the present invention in its corresponding aspects.

Claims

1. The utility model provides a formula chemical industry reation kettle breaks up in advance which characterized in that: comprises a stirring tank (1); the upper end face of the stirring tank (1) is fixedly connected with a double-shaft motor (2), one end of an output shaft of the double-shaft motor (2) is provided with a stirring device (3), the other end of the output shaft of the double-shaft motor (2) is provided with a feeding device (4), the upper end of the stirring tank (1) is fixedly connected with a crushing tank (5), the upper end face of the crushing tank (5) is rotatably connected with a sealing plate (6) through a hinge, the lower end face of the crushing tank (5) is fixedly connected with a discharging pipe (7), and the middle part of an inner cavity of the crushing tank (5) is fixedly connected with a filter plate (8);

feeding device (4) are including T type pole (41) and transfer line (42), double-shaft motor (2) output shaft end fixedly connected with transfer line (42), transfer line (42) surface upper portion is rotated through sprocket cooperation chain and is connected with rotary rod (43), terminal surface fixedly connected with T type pole (41) on agitator tank (1), the both ends of T type pole (41) inner chamber are rotated respectively and are connected with transfer line (42) and rotary rod (43), rotary rod (43) one end is run through filter plate (8) and is rotated with filter plate (8) and be connected, crushing unit (44) are installed on rotary rod (43) surface upper portion, unloading subassembly (45) are installed to rotary rod (43) surface lower part.

2. The pre-dispersing chemical reaction kettle according to claim 1, wherein: crushing unit (44) are including smashing pole (441) and solid fixed ring (442), pole (441) are smashed to rotary rod (43) surface upper portion fixedly connected with, rotary rod (43) surface just is located smash pole (441) lower part fixedly connected with solid fixed ring (442), gu fixed ring (442) surface rotates and is connected with crushing roller (443), crushing roller (443) surface and filter plate (8) up end be in contact with each other, gu fixed ring (442) surface fixedly connected with scraper blade (444), under scraper blade (444) terminal surface and filter plate (8) up end be in contact with each other.

3. The pre-dispersing chemical reaction kettle according to claim 2, wherein: unloading subassembly (45) are including unloading pole (451), slant pole (452) and flood dragon blade (453), rotary rod (43) surface just is located filter plate (8) lower part fixedly connected with unloading pole (451), rotary rod (43) surface just is located unloading pole (451) lower part fixedly connected with slant pole (452), slant pole (452) one side and crushing jar (5) inner chamber wall contact each other, rotary rod (43) surface lower part fixedly connected with flood dragon blade (453), flood dragon blade (453) are located unloading pipe (7) inner chamber.

4. The pre-dispersing chemical reaction kettle according to claim 1, wherein: agitating unit (3) are including (mixing) shaft (31), double-shaft motor (2) output shaft end fixedly connected with (mixing) shaft (31), (mixing) shaft (31) one end runs through agitator tank (1) and rotates with agitator tank (1) and is connected, end fixedly connected with circular screen cloth (32) on (mixing) shaft (31), equidistant fixedly connected with puddler (33) in (mixing) shaft (31) middle part, end fixedly connected with U type pole (34) under (mixing) shaft (31), terminal surface in contact with each other under U type pole (34) and agitator tank (1), U type pole (34) both sides respectively with agitator tank (1) inner chamber wall in contact with each other, unloading pipe (7) one end runs through agitator tank (1) and extends to circular screen cloth (32) upper portion.

5. The pre-dispersing chemical reaction kettle according to claim 4, wherein: agitator tank (1) up end fixedly connected with inlet pipe (9), terminal surface middle part fixedly connected with arranges material pipe (10) under agitator tank (1), valve is installed respectively to inlet pipe (9) and row material pipe (10) inner chamber, inner chamber wall top fixedly connected with L type pole (11) in agitator tank (1), L type pole (11) one side fixedly connected with brush (12), terminal surface contaction under brush (12) one end and circular screen cloth (32).