CN218608142U - Quick layering device of reaction liquid extraction - Google Patents
Quick layering device of reaction liquid extraction Download PDFInfo
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- CN218608142U CN218608142U CN202222318500.2U CN202222318500U CN218608142U CN 218608142 U CN218608142 U CN 218608142U CN 202222318500 U CN202222318500 U CN 202222318500U CN 218608142 U CN218608142 U CN 218608142U
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- extraction
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- reaction liquid
- stirring rod
- extraction tank
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
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Abstract
The utility model relates to a solution extraction technical field just discloses a quick decker of reaction liquid extraction, including the extraction jar that has inlet and liquid outlet, extraction tank deck portion is provided with top cap, its characterized in that: the extraction tank is internally provided with a stirring device, the stirring device comprises a stirring rod rotatably installed in the extraction tank, the top end of the stirring rod penetrates through the top cover and is fixedly connected with a rotating shaft of the driving motor, and the stirring rod is connected with a plurality of stirring blades through an adjusting device. This quick decker of reaction liquid extraction through addding agitating unit and adjusting device in extraction jar inside, adjusting device's setting makes agitating unit when the reaction liquid after the stirring is accomplished need to stew, can calm down the pivoted reaction liquid fast, and owing to the stirring paddle leaf that is arranged in stopping the baffle of reaction liquid and is out of shape by agitating unit comes, the baffle is to its resistance that produces when can greatly reduce the reaction liquid and rotate, improves the mixing efficiency of solvent solution.
Description
Technical Field
The utility model relates to a solution extraction technical field specifically is a quick decker of reaction liquid extraction.
Background
The extraction is an operation method for extracting the solute from a solution consisting of another solvent by using the different solubilities of the solute in the solvents which are not mutually soluble, and in the synthesis of a medical intermediate, after the reaction is finished and quenched, an organic solvent is usually adopted for extraction, so that the product can be extracted from a water layer as far as possible.
The patent number CN217067766U granted in China is a reaction liquid extraction rapid layering device which comprises a support and an extraction tank, wherein the extraction tank is arranged on the support through a support rod, and the device also comprises: the motor is arranged at the upper end of the extraction tank; the output rod is rotatably connected in the extraction tank, and the upper end of the output rod is fixedly connected with the output end of the motor; the stirring blades are uniformly distributed on the output rod; the rotating rods are symmetrically and rotatably connected to two sides of the interior of the extraction tank through the fixed blocks; the adjusting plate is fixedly connected to the rotating rod; the sleeve is symmetrically and rotatably connected to two sides of the extraction tank close to the adjusting plate; the moving block is connected with the moving rod in the sleeve in a sliding mode, fixedly connected to the moving block, and one end, far away from the moving block, of the moving block is rotatably connected with the adjusting plate; the magnetic block is fixedly connected to one end, far away from the moving rod, of the moving block; circular telegram magnet, fixed connection are in the inside one end of keeping away from the carriage release lever of sleeve, and with external power electric connection ", through the setting of sleeve, carriage release lever, movable block, circular telegram magnet, magnetic path, after accomplishing the stirring, two regulating plates just can be in on same straight line under the effect of circular telegram magnet, magnetic path to be in the state of tightening, thereby alright stop the reaction liquid of pairing rotation, make its quick calm get off.
However, the sleeve, the moving rod and the adjusting plate which are arranged on the inner wall of the extraction tank still generate certain resistance to the rotation of the reaction liquid even if the energized magnet is not energized, and the mixing efficiency of the solvent and the solution is influenced.
We therefore propose a device for rapid stratification of the reaction solution extraction in order to solve the problems set forth above.
SUMMERY OF THE UTILITY MODEL
Technical problem to be solved
The utility model aims to provide a quick decker of reaction liquid extraction to the not enough of prior art in the above-mentioned background is provided to solve the problem that proposes in the above-mentioned background.
(II) technical scheme
In order to achieve the above purpose, the utility model discloses a following technical scheme realizes:
a reaction liquid extraction rapid layering device comprises an extraction tank with a liquid inlet and a liquid outlet, wherein a top cover is arranged at the top of the extraction tank, a stirring device is arranged in the extraction tank, the stirring device comprises a stirring rod rotatably arranged in the extraction tank, the top end of the stirring rod penetrates through the top cover and is fixedly connected with a rotating shaft of a driving motor, and the stirring rod is connected with a plurality of stirring blades through an adjusting device;
the adjusting device comprises a plurality of sector gears which are rotatably connected in a mounting groove arranged in the extraction tank, the sector gears are connected with paddle clamps for fixing stirring paddles through connecting rods which are connected to the side wall of the stirring rod in a sliding manner, the paddle clamps are hinged with the side wall of the extraction tank through hinge rods, and racks meshed with the sector gears are connected in the mounting groove in a sliding manner;
the top of the rack is provided with a magnetic block, and the top cover is provided with an electromagnet matched with the magnetic block for use.
Preferably, the cross section of the stirring rod is rectangular, the stirring blades and the sector gear are divided into two groups which are respectively arranged on two opposite sides of the stirring rod, and each group of stirring blades are longitudinally arranged.
Further, the spacing distance between every two sector gears in the same group is smaller than or equal to the width of the stirring paddle.
Preferably, the connecting rod is equipped with a plurality ofly along the length direction of paddle clamping, the arc spout with paddle clamping looks adaptation is seted up to the puddler lateral wall.
Furthermore, a clamping ring for fixing the magnetic block is fixed at the top end of the rack.
Further, the driving motor is a servo motor.
Preferably, the top cover is provided with a handle, the bottom end of the extraction tank is provided with supporting legs, and valves are arranged on the liquid inlet and the liquid outlet.
(III) advantageous effects
Compared with the prior art, the beneficial effects of the utility model are that: this quick layering device of reaction liquid extraction:
through addding agitating unit and adjusting device inside the extraction jar, agitating unit during operation can stir the solvent solution of extraction jar and mix, reaction effect with higher speed, adjusting device's setting makes agitating unit when the reaction liquid after the stirring is accomplished need stewing, can calm down pivoted reaction liquid fast, and because the baffle that is used for blockking the reaction liquid is out of shape by the stirring paddle leaf among the agitating unit and comes, the resistance of baffle to its production when can greatly reduce the reaction liquid and rotate, improve solvent solution's mixing efficiency.
Drawings
FIG. 1 is a schematic view of the cross-sectional structure of the reaction solution extraction rapid layering device of the present invention;
FIG. 2 is a schematic view of the structure of a stirring rod of the reaction solution extraction rapid layering device of the present invention;
FIG. 3 is a schematic structural view of an adjusting device of the reaction solution extraction rapid layering device of the present invention;
FIG. 4 is an enlarged view of the point A of the reaction solution extraction rapid layering device of the present invention;
FIG. 5 is an enlarged view of the position B of the reaction solution extraction rapid layering device of the present invention;
FIG. 6 is a magnetic block diagram of the reaction solution extraction rapid layering device of the present invention;
FIG. 7 is a schematic view of a partial structure of an adjusting device of the rapid reaction liquid extraction layering device of the present invention;
FIG. 8 is a schematic structural view of the stirring blade of the rapid reaction liquid extraction layering device of the present invention during stirring;
fig. 9 is a schematic structural diagram of the reaction liquid extraction rapid layering device of the present invention when the stirring blade blocks the reaction liquid.
In the figure: extraction jar 1, inlet 11, liquid outlet 12, top cap 2, agitating unit 3, puddler 31, driving motor 32, stirring paddle blade 33, mounting groove 34, arc spout 35, adjusting device 4, sector gear 41, connecting rod 42, paddle clamping 43, hinge bar 44, rack 45, electro-magnet 46, magnet 47, snap ring 48, handle 5, supporting leg 6.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
Referring to fig. 1-9, the present invention provides a reaction solution extraction rapid layering device; the extraction tank comprises an extraction tank 1 with a liquid inlet 11 and a liquid outlet 12, wherein valves are arranged on the liquid inlet 11 and the liquid outlet 12, a top cover 2 is arranged at the top of the extraction tank 1, a handle 5 is arranged on the top cover 2, supporting legs 6 are arranged at the bottom end of the extraction tank 1, a stirring device 3 is arranged in the extraction tank 1, the stirring device 3 comprises a stirring rod 31 which is rotatably arranged at the axis of the extraction tank 1, the stirring rod 31 is prism-shaped, the top end of the stirring rod 31 penetrates through the top cover 2 and is fixedly connected with a rotating shaft of a driving motor 32, the driving motor 32 is preferably a servo motor, the stirring rod 31 is connected with a plurality of connecting rods 42 and stirring blades 33 through an adjusting device 4;
as shown in fig. 3, a mounting groove 34 is vertically formed at the top of the stirring rod 31, a plurality of sector gears 41 are longitudinally and equidistantly mounted in the mounting groove 34, as shown in fig. 4, the axes of the sector gears 41 are hinged to two side walls of the mounting groove 34 through a connecting rod, which is not shown in the figure, the end surfaces of the sector gears 41 are fixed with a plurality of connecting rods 42, an arc chute 35 matched with the connecting rods 42 is formed on the side wall of the stirring rod 31, one end of each connecting rod 42, which is far away from the sector gear 41, penetrates through the arc chute 35 and is fixedly connected with a blade clamp 43 for fixing the stirring blade 33, one end of the blade clamp 43 is hinged to the side wall of the stirring rod 31 through a hinged rod 44, a rack 45 meshed with the sector gears 41 is slidably connected to the side wall of the mounting groove 34, a snap ring 48 for fixing a magnetic block 47 is arranged at the top of the rack 45, the magnetic block 47 is fixed in an annular groove formed at the top of the snap ring 48, the top cover 2 is provided with an electromagnet 46 matched with a magnet 47 for use, the electromagnet 46 is a circular electromagnet with the model WAXU-100-52-40, when solute solvent to be mixed is stirred, the electromagnet 46 is positively electrified to generate repulsive force to the magnet 47, so that a rack 45 moves downwards to drive a sector gear 41 to rotate downwards, the stirring blades 33 are driven to rotate and incline through a connecting rod 42 and blade clips 43, a certain interval is formed between adjacent stirring blades 3, at the moment, when a driving motor 32 rotates, the stirring blades 33 play a role in stirring and mixing the solvent solution, when stirring is completed and needs to stand, the electromagnet 46 is reversely electrified to generate suction to the magnet 47, so that the rack 45 moves upwards to drive the sector gear 41 to rotate upwards, and the stirring blades 33 are driven to rotate and incline through the connecting rod 42 and the blade clips 43, make adjacent stirring paddle 3 be close or be vertical form, play certain effect of blockking to pivoted reaction liquid, make it can calm down fast, compare in the baffle of setting at an extraction section of thick bamboo inner wall can greatly reduce the resistance to reaction liquid when mixing, can effectively improve mixing efficiency.
As a preferred technical solution of the utility model: a plurality of stirring paddle 33 and sector gear 41 divide into two sets ofly to be central symmetry form and set up respectively in the relative both sides of puddler 31, and every stirring paddle 33 of group is longitudinal arrangement, and two sets of stirring paddle 33 that the symmetry set up are more steady when making the motor rotate.
As an optimal technical solution of the utility model: the spacing distance between every two sector gears 41 in the same group is smaller than or equal to the width of the stirring blades 33, so that the two adjacent stirring blades 33 can be attached together when the stirring blades 33 deform, and the blocking efficiency is improved.
As a preferred technical solution of the utility model: the connecting rod 42 is provided with a plurality of connecting rods along the length direction of the blade clamp 43, and the side wall of the stirring rod 31 is provided with an arc-shaped sliding groove 35 matched with the blade clamp 43.
The above is the operation of the whole device, and the details which are not described in detail in this specification are well known to those skilled in the art.
The electrical components presented therein may be electrically connected to an external controller, and the controller may be electrically connected to an external 220V commercial power, and the controller may be a conventional known device for controlling a computer or the like.
Although the present invention has been described in detail with reference to the foregoing embodiments, it should be noted that, in the present invention, unless otherwise explicitly specified or limited, the terms "set", "mounted", "connected", "fixed", and the like are to be interpreted broadly, and may be, for example, either fixedly connected or detachably connected; or indirectly through an intermediary.
In the description of the present invention, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. As used herein, "plurality" means two or more unless specifically limited otherwise.
The specific meaning of the above terms in the present invention can be understood according to specific situations by those of ordinary skill in the art; it will be appreciated by those skilled in the art that modifications may be made to the above-described embodiments, or equivalents may be substituted for elements thereof, and any modifications, equivalents, improvements and the like which fall within the spirit and scope of the present invention may be resorted to.
Claims (7)
1. The utility model provides a quick decker of reaction liquid extraction, is including extraction jar (1) that has inlet (11) and liquid outlet (12), extraction jar (1) top is provided with top cap (2), its characterized in that: a stirring device (3) is arranged in the extraction tank (1), the stirring device (3) comprises a stirring rod (31) rotatably mounted in the extraction tank (1), the top end of the stirring rod (31) penetrates through the top cover (2) and is fixedly connected with a rotating shaft of a driving motor (32), and the stirring rod (31) is connected with a plurality of stirring blades (33) through a regulating device (4);
the adjusting device (4) comprises a plurality of sector gears (41) which are rotatably connected in a mounting groove (34) formed in the extraction tank (1), the sector gears (41) are connected with blade clamps (43) used for fixing stirring blades (33) through connecting rods (42) which are connected to the side wall of the stirring rod (31) in a sliding mode, the blade clamps (43) are hinged to the side wall of the extraction tank (1) through hinge rods (44), and racks (45) meshed with the sector gears (41) are connected in the mounting groove (34) in a sliding mode;
the top of the rack (45) is provided with a magnetic block (47), and the top cover (2) is provided with an electromagnet (46) matched with the magnetic block (47) for use.
2. The reaction solution extraction rapid delamination apparatus as defined in claim 1, wherein: the cross section of the stirring rod (31) is rectangular, the stirring blades (33) and the sector gear (41) are divided into two groups which are respectively arranged on two opposite sides of the stirring rod (31), and each group of stirring blades (33) is longitudinally arranged.
3. The reaction liquid extraction rapid layering device according to claim 2, characterized in that: the spacing distance between two adjacent sector gears (41) in the same group is smaller than or equal to the width of the stirring blade (33).
4. The reaction solution extraction rapid delamination apparatus as defined in claim 1, wherein: the length direction of connecting rod (42) edge paddle clamping (43) is equipped with a plurality ofly, arc spout (35) with paddle clamping (43) looks adaptation are seted up to puddler (31) lateral wall.
5. The reaction solution extraction rapid delamination apparatus as defined in claim 1, wherein: a snap ring (48) used for fixing the magnetic block (47) is fixed at the top end of the rack (45).
6. The reaction solution extraction rapid delamination apparatus as defined in claim 1, wherein: the driving motor (32) is a servo motor.
7. The reaction solution extraction rapid delamination apparatus as defined in claim 1, wherein: be provided with handle (5) on top cap (2), extraction jar (1) bottom is provided with supporting leg (6), all be provided with the valve on inlet (11) and liquid outlet (12).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202222318500.2U CN218608142U (en) | 2022-09-01 | 2022-09-01 | Quick layering device of reaction liquid extraction |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202222318500.2U CN218608142U (en) | 2022-09-01 | 2022-09-01 | Quick layering device of reaction liquid extraction |
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| Publication Number | Publication Date |
|---|---|
| CN218608142U true CN218608142U (en) | 2023-03-14 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN202222318500.2U Active CN218608142U (en) | 2022-09-01 | 2022-09-01 | Quick layering device of reaction liquid extraction |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN117920000A (en) * | 2024-03-21 | 2024-04-26 | 太原师范学院 | Chemical analysis is with accelerating dissolving instrument |
| CN117920000B (en) * | 2024-03-21 | 2024-06-11 | 太原师范学院 | Chemical analysis is with accelerating dissolving instrument |
-
2022
- 2022-09-01 CN CN202222318500.2U patent/CN218608142U/en active Active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN117920000A (en) * | 2024-03-21 | 2024-04-26 | 太原师范学院 | Chemical analysis is with accelerating dissolving instrument |
| CN117920000B (en) * | 2024-03-21 | 2024-06-11 | 太原师范学院 | Chemical analysis is with accelerating dissolving instrument |
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