CN218455655U

CN218455655U - Analysis device based on total carbon content in high-purity argon

Info

Publication number: CN218455655U
Application number: CN202221087068.4U
Authority: CN
Inventors: 秦辉辉; 杨利; 倪华松; 何国芳
Original assignee: Zhejiang Xite Electronic Materials Co ltd
Current assignee: Zhejiang Xite Electronic Materials Co ltd
Priority date: 2022-05-06
Filing date: 2022-05-06
Publication date: 2023-02-07
Anticipated expiration: 2032-05-06

Abstract

The utility model provides an analytical equipment based on total carbon content in high-purity argon gas, including the total carbon content analysis receiving mechanism of argon gas, the total carbon content analysis receiving mechanism of argon gas mainly comprises the triplex main structure: the gas analysis pipe fitting, the visual piece of high pressure and one-way shutoff piece, the visual piece of high pressure is installed in the inboard both sides of gas analysis pipe fitting, and the one-way shutoff piece is installed in the inside one end of the visual piece of high pressure. The utility model discloses total carbon content analysis receiving mechanism's of argon gas high pressure visual piece, pour into the back into liquefied argon gas, because the inside high pressure that will slowly form of admission analysis pipe, this moment, the outer contact electricity body of high pressure visual piece will be because the external pressure is sunken in the shape, the faint lamp of visual banks is opened after outer contact electricity body and contact, after whole outer contact electricity bodies all contact with contact, the strong light alright of visual banks is opened, learn the concrete capacity of inside liquefied argon gas through the conduction of light and pressure.

Description

Analysis device based on total carbon content in high-purity argon

Technical Field

The utility model belongs to the technical field of total carbon content, especially, relate to an analytical equipment based on total carbon content in high-purity argon gas.

Background

The total organic carbon analyzer is used for measuring Total Organic Carbon (TOC) in a solution. The determination principle is that organic carbon in the solution is converted into carbon dioxide through oxidation, and the content of the carbon dioxide is measured by a detector after interference substances are eliminated. And quantitatively determining the total organic carbon in the solution by utilizing the corresponding relation of the carbon content between the carbon dioxide and the total organic carbon. There are three main types of measuring methods of the total organic carbon analyzer. The method comprises the following steps of treating a sample to be detected by phosphoric acid before the sample is oxidized by acidic potassium persulfate, removing inorganic carbon, and then determining the TOC concentration, wherein the existing analysis device for the total carbon content has the following defects: when total organic carbon analysis appearance was injected into to liquefied argon gas, the specific capacity of the argon gas of unable visual liquefaction causes the consumption that can't effectual learn to inject into, and secondly, the liquefied argon gas of injecting has the probability to discharge the condition emergence outside.

Therefore, it is necessary to develop an analysis device based on the total carbon content in high purity argon.

SUMMERY OF THE UTILITY MODEL

In order to solve the technical problem, the utility model provides an analytical equipment based on total carbon content in high-purity argon gas, including the total carbon content analysis receiving mechanism of argon gas, the total carbon content analysis receiving mechanism of argon gas mainly comprises the triplex main structure: the gas analysis pipe fitting, the visual piece of high pressure and one-way shutoff piece are all installed in the inside of gas analysis pipe fitting, and the visual piece of high pressure is installed in the inboard both sides of gas analysis pipe fitting, and one-way shutoff piece is installed in the inside one end of the visual piece of high pressure.

The gas analysis pipe fitting is composed of four structures: the device comprises a receiving analysis tube, an analysis contact end, a collecting adapter tube and an injection port, wherein the analysis contact end is arranged inside and outside the receiving analysis tube, the analysis contact end is connected with a total organic carbon analysis instrument through a column tube, one end of the receiving analysis tube is provided with the conical collecting adapter tube, the collecting adapter tube is connected with the injection port, and a one-way blocking piece is arranged in the joint area of the collecting adapter tube and the injection port.

The high-pressure visual piece consists of four parts of structures: high pressure depressed area, outer convex electricity body, contact wire and visual banks, high pressure depressed area set up and accept the analysis pipe inboard at gas analysis pipe fitting, and high pressure depressed area adopts the depressed area that the arc was made, and contact wire has been embedded to high pressure depressed area's inboard, and contact wire mainly inlays in the inside of accepting the analysis pipe.

The installation has the evagination electricity body on the region in high pressure depressed area, the evagination electricity body is the lamellar body that adopts the evagination arc to make, the evagination electricity body is the electric conductor of visual banks, visual banks is the banks that adopts two kinds of red lights to make, two groups of lamps of visual banks are weak light and strong light, visual banks is provided with a plurality ofly, it is adjacent with it through the evagination electricity body between the visual banks, the evagination electricity body is the conductive convex body, the contact wire then is the electricity generation electric wire, the visual banks will be opened to the evagination electricity body and contact wire, visual banks further learns its specific capacity through the colour of red eye, the lamp of two different intensity of visual banks also can be effectual whether inject into the argon gas that accomplishes liquefaction (only can just can be in order to open when the strong light of the visual banks of argon gas complete injection completion back).

The one-way blocking piece is composed of six parts: restriction carrier pole, restriction wire pole, restriction recess, valve ball, reset spring and sunken arc region, restriction carrier pole are the dead lever that adopts the rectangle to make, and the both ends ann of restriction carrier pole is inlayed and is connect the intraduct in conical collection, and restriction wire pole on the restriction carrier pole is worn into the restriction recess, and the restriction recess is the cavity that adopts the T type to make.

The limiting groove is formed in the valve ball, one end of the reset spring is connected with the surface of the valve ball, the other end of the reset spring is connected with the surface of one side of the limiting carrier rod, the concave arc-shaped area is formed in the connection area of the collecting connection pipe and the injection port, the valve ball is clamped in the concave arc-shaped area of the collecting connection pipe and the injection port, the valve ball is matched with the external reset spring to realize unidirectional injection, when liquefied argon is injected into the receiving analysis pipe to be completed, the valve ball is tightly fixed and sealed by the aid of high pressure in the valve ball, and leakage is avoided during inspection.

Compared with the prior art, the utility model discloses following beneficial effect has:

1. the utility model discloses the high-pressure visual piece of total carbon content analysis receiving mechanism of argon gas, pour into the back with liquefied argon gas into, because it will slowly form the high pressure to accept the inside analysis pipe, at this moment, the outer contact electricity body of high-pressure visual piece will be because the internal caving in of external pressure shape, the faint lamp of visual banks is opened after outer contact electricity body and contact, after whole outer contact electricity bodies all contact with the contact, the strong light alright of visual banks opens, learn the concrete capacity of inside liquefied argon gas through the conduction of light and pressure.

2. The utility model discloses total carbon content analysis receiving mechanism's of argon gas one-way plug member sets up, then is the valve ball through one-way plug member and blocks up, and the outside reset spring of valve ball cooperation realizes one-way pouring into, when accepting the inside injection of analysis pipe and accomplishing liquefied argon gas, and the inside high pressure can be inseparable lets valve ball fixed seal, avoids appearing the condition emergence of leaking in the inspection.

3. The utility model discloses the visual banks setting of high pressure visual piece, then the observation of visual colourless liquefied argon gas that can be better, visual banks further learns its concrete capacity through red colour that shows the eye, and the lamp of two different intensity of visual banks also can effectually learn whether to pour into the argon gas of accomplishing the liquefaction (only can just can get open when the strong light lamp of the visual banks of argon gas complete injection completion back).

Drawings

Fig. 1 is a schematic view of the structure of the present invention.

Fig. 2 is a schematic view of the structure of fig. 1 in a partial cross section according to the present invention.

Fig. 3 is a schematic view of a partial enlarged assembly of fig. 2 according to the present invention.

In the figure:

the device comprises an argon total carbon content analysis receiving mechanism 1, a gas analysis pipe fitting 2, a high-voltage visual part 3, a one-way plugging part 4, an acceptance analysis pipe 5, an analysis contact end 6, a collection connection pipe 7, an injection port 8, a high-voltage concave area 9, a concave electric connector 10, a contact wire 11, a visual lamp set 12, a limiting carrier rod 13, a limiting lead rod 14, a limiting groove 15, a valve ball 16, a reset spring 17 and a concave arc area 18.

Detailed Description

In order to make the technical solution of the present invention better understood, the technical solution of the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments of the present invention, all other embodiments obtained by a person skilled in the art without creative efforts shall fall within the protection scope of the present invention.

In the description of the embodiments, it should be noted that the terms "upper", "lower", "inner", "outer", "front", "rear", "both ends", "one end", "the other end", and the like indicate orientations or positional relationships based on the orientations or positional relationships shown in the drawings, and are only for convenience of description and simplification of description, but do not indicate or imply that the device or element referred to must have a specific orientation, be constructed in a specific orientation, and be operated, and thus, should not be construed as limiting the present invention. Furthermore, the terms "first" and "second" are used for descriptive purposes only and are not to be construed as indicating or implying relative importance. In the description of the present invention, it should be noted that, unless otherwise explicitly specified or limited, the terms "mounted," "provided," "connected," and the like are to be construed broadly, such as "connected," which may be fixedly connected, detachably connected, or integrally connected; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meaning of the above terms in the present invention can be understood in specific cases to those skilled in the art.

As shown in figures 1 to 3:

the utility model provides a pair of analytical equipment based on total carbon content in high-purity argon gas, including total carbon content analysis receiving mechanism 1 of argon gas, gas analysis pipe fitting 2, high-pressure visual piece 3, one-way stifled plug member 4, accept analysis pipe 5, analysis contact jaw 6 collects linking pipe 7, injection port 8, high-pressure depressed area 9, the indent electricity body 10 that connects, contact wire 11, visual banks 12, restriction carrier pole 13, restriction wire pole 14, restriction recess 15, valve ball 16, reset spring 17 and sunken arc region 18, wherein: the argon total carbon content analysis receiving mechanism 1 mainly comprises three main structures: gaseous analysis pipe fitting 2, high-pressure visual piece 3 and one-way stifled plug member 4, the inside at gaseous analysis pipe fitting 2 is all installed to high-pressure visual piece 3 and one-way stifled plug member 4, and the inboard both sides at gaseous analysis pipe fitting 2 are installed to high-pressure visual piece 3, and one-way stifled plug member 4 is installed in the inside one end of high-pressure visual piece 3, and gaseous analysis pipe fitting 2 comprises four structures: the device comprises a receiving analysis tube 5, an analysis contact end 6, a collecting adapter tube 7 and an injection port 8, wherein the analysis contact end 6 is arranged inside and outside the receiving analysis tube 5, the analysis contact end 6 is connected with a total organic carbon analysis instrument through a string tube, one end of the receiving analysis tube 5 is provided with the conical collecting adapter tube 7, the collecting adapter tube 7 is connected with the injection port 8, and a one-way blocking piece 4 is arranged in the joint area of the collecting adapter tube 7 and the injection port 8.

Example (b):

an inner concave contact electric body 10 is embedded in the area of the high-voltage concave area 9, the inner concave contact electric body 10 is a sheet body made of an outer convex arc, the inner concave contact electric body 10 is a conductor of a visual light group 12, the visual light group 12 is a light group made of two red lights, two groups of lights of the visual light group 12 are weak lights and strong lights, a limiting carrier rod 13 is a fixing rod made of a rectangle, two ends of the limiting carrier rod 13 are embedded in a conical collecting connection pipe 7, a limiting lead rod 14 on the limiting carrier rod 13 penetrates into a limiting groove 15, a high-voltage visual part 3 of the argon total carbon content analysis receiving mechanism 1 is used for injecting liquefied argon, high voltage is slowly formed in an accommodating analysis pipe 4, at the moment, the outer convex contact electric body 10 of the high-voltage visual part 3 is sunken due to the shape of external pressure, the weak lights of the inner concave contact electric body 12 are turned on after the outer convex contact electric body 10 is contacted with a contact electric wire 11, when all outer convex contact electric bodies 11 are contacted with the contact electric wire 12, the visual light group 12 can be turned on, and the specific capacity of the inner concave light and the internal argon can be known through the specific transmission capacity of the liquefied argon; the one-way plugging piece 4 of the argon total carbon content analysis receiving mechanism 1 is plugged by the valve ball 16 of the one-way plugging piece 4, the valve ball is matched with an external reset spring 17 to realize one-way injection, and when liquefied argon is injected into the receiving analysis tube 4, the valve ball 16 is tightly fixed and sealed by internal high pressure, so that the leakage condition is avoided during inspection; the visual banks 12 of high-pressure visual piece 3 sets up, then the observation of visual colourless liquefied argon gas that can be better, and visual banks 12 further learns its specific capacity through red obvious colour, and the lamp of two different intensity of visual banks 12 also can effectually learn whether to inject into the argon gas that accomplishes the liquefaction (only can the strong light lamp of visual banks just can open when the argon gas is injected completely and is accomplished back).

Utilize technical scheme, or technical personnel in the field are in the utility model discloses under technical scheme's the inspiration, design similar technical scheme, and reach above-mentioned technological effect, all fall into the utility model discloses a protection scope.

Claims

1. The analysis device based on the total carbon content in the high-purity argon comprises an argon total carbon content analysis receiving mechanism (1), and is characterized in that the argon total carbon content analysis receiving mechanism (1) mainly comprises three main structures: the gas analysis pipe fitting comprises a gas analysis pipe fitting (2), a high-pressure visual piece (3) and a one-way blocking piece (4), wherein the high-pressure visual piece (3) and the one-way blocking piece (4) are installed inside the gas analysis pipe fitting (2), the high-pressure visual piece (3) is installed on two sides of the inner side of the gas analysis pipe fitting (2), and the one-way blocking piece (4) is installed at one end of the inner side of the high-pressure visual piece (3).

2. The analysis apparatus according to claim 1, wherein the analysis apparatus comprises: the gas analysis pipe fitting (2) is composed of four parts: the device comprises a receiving analysis tube (5), an analysis contact end (6), a collecting adapter tube (7) and an injection port (8), wherein the analysis contact end (6) is arranged in the receiving analysis tube (5) and outside the receiving analysis tube (5), the analysis contact end (6) is connected with a total organic carbon analysis instrument through a string tube, the conical collecting adapter tube (7) is arranged at one end of the receiving analysis tube (5), the collecting adapter tube (7) is connected with the injection port (8), and a one-way blocking piece (4) is arranged in the joint area of the collecting adapter tube (7) and the injection port (8).

3. The analysis apparatus according to claim 1, wherein the analysis apparatus comprises: the high-pressure visual piece (3) is composed of four parts: high pressure depressed area (9), outer convex electricity body (10), contact wire (11) and visual banks (12), high pressure depressed area (9) are seted up and are being accepted analysis pipe (5) inboard at gas analysis pipe fitting (2), and high pressure depressed area (9) are the depressed area that adopts the arc to make, and contact wire (11) have been inlayed to the inboard ann of high pressure depressed area (9), and contact wire (11) mainly are inlayed in the inside of accepting analysis pipe (5).

4. The analysis apparatus according to claim 3, wherein the analysis apparatus comprises: the installation has outer convex electricity body (10) on the region of high pressure depressed area (9), and outer convex electricity body (10) are the slice body that adopts outer convex arc to make, and outer convex electricity body (10) are the electric conductor of visual banks (12), and visual banks (12) are the banks that adopt two kinds of red lights to make, and two groups of lamps of visual banks (12) are weak light and strong light.

5. The analysis apparatus based on total carbon content in high purity argon as claimed in claim 1, wherein: the one-way blocking piece (4) is composed of six parts: the limiting device comprises a limiting carrier rod (13), a limiting wire rod (14), a limiting groove (15), a valve ball (16), a return spring (17) and a concave arc-shaped area (18), wherein the limiting carrier rod (13) is a fixing rod made of a rectangle, two ends of the limiting carrier rod (13) are embedded in a conical collecting connecting pipe (7), the limiting wire rod (14) on the limiting carrier rod (13) penetrates into the limiting groove (15), and the limiting groove (15) is a cavity made of a T shape.

6. The analysis apparatus according to claim 5, wherein the analysis apparatus comprises: the limiting groove (15) is formed in the valve ball (16), one end of a return spring (17) is connected with the surface of the valve ball (16), the other end of the return spring (17) is connected with the surface of one side of the limiting carrier rod (13), a concave arc-shaped area (18) is formed in the connection area of the collecting connection pipe (7) and the injection port (8), and the valve ball (16) is clamped in the concave arc-shaped area (18) of the collecting connection pipe (7) and the injection port (8).