CN218421063U

CN218421063U - Distillation plant is used in nonane production

Info

Publication number: CN218421063U
Application number: CN202221938862.5U
Authority: CN
Inventors: 王成洪; 丁勇; 李斌; 张华锋; 李学龙
Original assignee: Shayang Qinjiang Chemical Co ltd
Current assignee: Shayang Qinjiang Chemical Co ltd
Priority date: 2022-07-26
Filing date: 2022-07-26
Publication date: 2023-02-03
Anticipated expiration: 2032-07-26

Abstract

The utility model relates to a nonane production technical field just discloses a distillation plant is used in nonane production, which comprises a housin, the bottom left and right sides of casing all is provided with quantity and is two supporting legss, the right side of casing is provided with the inlet pipe that one end extends to its inside, the outside of inlet pipe is provided with first solenoid valve, the interior diapire of casing is provided with the discharging pipe that one end extends to its bottom, the outside of discharging pipe is provided with the second solenoid valve, be provided with the heating pipe on the inner wall of casing. This distillation plant is used in nonane production drives the puddler through starting biax driving motor and rotates to this stirs the raw materials, and biax driving motor can also drive puddler reciprocating motion from top to bottom at the in-process of operation simultaneously, makes the puddler reciprocating motion from top to bottom in rotatory in-process cooperation, with this come to carry out even stirring to the raw materials, thereby makes the raw materials be heated evenly, and then improves the distillative effect.

Description

Distillation plant is used in nonane production

Technical Field

The utility model relates to a nonane production technical field specifically is a distillation plant is used in nonane production.

Background

The nonane is a colorless liquid, is insoluble in water, is miscible in ethanol, ether and the like, can replace original toxic products, namely solvent oil, white oil, aromatic hydrocarbon oil and the like, is non-toxic and non-corrosive, is a green and environment-friendly product, is a very popular research direction at present, is more and more favored by new drug research and development enterprises in new drug research and development, and in the process of producing the nonane, the mixed raw materials are generally heated through a distillation device, so that the solvent in the mixed raw materials is distilled off.

However, most of existing distillation devices for producing nonane do not have the stirring function, so that the mixed raw materials are easily heated unevenly in the distillation process of the mixed raw materials, and further the evaporation effect of a solvent is influenced, and therefore the distillation device for producing nonane is provided.

SUMMERY OF THE UTILITY MODEL

Technical problem to be solved

To prior art not enough, the utility model provides a distillation plant is used in nonane production possesses the advantage such as evenly being heated, has solved that current distillation plant is used in nonane production most and does not possess the function of stirring, leads to carrying out the in-process of distilling to mixing raw materials, the inhomogeneous condition of being heated appears easily in mixing raw materials, and then can remove the problem that the effect caused the influence to evaporating of solvent.

(II) technical scheme

In order to realize the above-mentioned even purpose of being heated, the utility model provides a following technical scheme: the utility model provides a distillation plant is used in nonane production, includes the casing, the bottom left and right sides of casing all is provided with the supporting legs that quantity is two, the right side of casing is provided with one end and extends to its inside inlet pipe, the outside of inlet pipe is provided with first solenoid valve, the interior diapire of casing is provided with the discharging pipe that one end extends to its bottom, the outside of discharging pipe is provided with the second solenoid valve, be provided with the heating pipe on the inner wall of casing, the right side of casing is provided with the controller that is located the inlet pipe below, the left side of casing is provided with the one end and extends to its inside condensation subassembly, the top left and right sides of casing all is provided with the riser, two be provided with the diaphragm between the riser, the bottom of diaphragm is provided with the (mixing) shaft that one end extends to its casing inside, the outside of (mixing) shaft is provided with the sleeve that is located the casing inside, the telescopic left and right sides all is provided with the puddler that quantity is four, the top of casing is provided with one end and extends to the drive assembly on right side outside fixed connection bearing, the top of connecting block is provided with the extension rod that the one end runs through the diaphragm and the right side and the extension rod and the top of riser is provided with the right side extrusion frame body and the one end and the right side extrusion subassembly.

Preferably, the condensation subassembly includes the cooler bin, the left side fixed mounting of casing has the cooler bin, the top fixed mounting of cooler bin has one end to run through and extend to the condenser pipe of its bottom, the top fixed mounting of condenser pipe has one end to extend to the inside connecting pipe of casing.

Preferably, the drive assembly includes biax driving motor, the top fixed mounting of casing has the biax driving motor that is located between (mixing) shaft and the right side riser and is located the diaphragm below, biax driving motor's left side output shaft fixed mounting has drive bevel gear, the outside fixed mounting of (mixing) shaft has the driven bevel gear who is located casing top and one end and drive bevel gear meshing, biax driving motor's right side output shaft extends to the right side and the fixed mounting of right side riser and has drive gear.

Preferably, the extruding component includes pivot, left side the right side movable mounting of riser has the pivot that is located diaphragm top and one end and passes the framework and extends to right side riser right side, the outside fixed mounting of pivot has the disc that is located the laminating of inside and one end of framework and bottom wall in the framework, the outside fixed mounting of pivot has the driven gear who is located right side riser right side and one end and drive gear meshing.

Preferably, the bottom fixed mounting of diaphragm has first bearing, the (mixing) shaft rotates through first bearing and diaphragm to be connected, the mounting hole with the stirring shaft adaptation is seted up at the top of casing.

Preferably, the first through-hole with two extension rod looks adaptations respectively is all seted up to both sides around the roof in the casing, the inside front and back both sides of diaphragm all seted up respectively with the second through-hole of two extension rod looks adaptations.

(III) advantageous effects

Compared with the prior art, the utility model provides a distillation plant is used in nonane production possesses following beneficial effect:

this distillation plant is used in nonane production, it is rotatory to drive bevel gear and drive gear through starting biax driving motor, wherein drive bevel gear then can drive the (mixing) shaft through driven bevel gear at rotatory in-process, sleeve and puddler are whole to be rotated, stir the raw materials with this, drive gear then can drive pivot and disc rotation through driven gear at rotatory in-process, the disc then can extrude through both sides about the inner wall to the framework at rotatory in-process, drive framework and extension rod reciprocating motion from top to bottom with this, and then drive sleeve and puddler reciprocating motion from top to bottom through connecting block and connecting bearing, make the puddler reciprocating motion from top to bottom in rotatory in-process cooperation, with this come to carry out even stirring to the raw materials, thereby make the raw materials be heated evenly, and then improve the effect of distillation.

Drawings

FIG. 1 is a schematic structural view of the present invention;

fig. 2 is a right side view sectional partial schematic view of the present invention.

In the figure: the device comprises a shell 1, supporting legs 2, a feeding pipe 3, a first electromagnetic valve 4, a discharging pipe 5, a second electromagnetic valve 6, a heating pipe 7, a controller 8, a condensation component 9, a cooling box 91, a condensation pipe 92, a connecting pipe 93, a vertical plate 10, a transverse plate 11, a stirring shaft 12, a sleeve 13, a stirring rod 14, a driving component 15, a double-shaft driving motor 151, a driving bevel gear 152, a driven bevel gear 153, a driving gear 154, a connecting bearing 16, a connecting block 17, an extending rod 18, a frame body 19, an extrusion component 20, a rotating shaft 201, a disc 202 and a driven gear 203.

Detailed Description

The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.

Referring to fig. 1-2, the present invention provides a technical solution: the utility model provides a distillation plant is used in nonane production, which comprises a housin 1, the equal fixed mounting in bottom left and right sides of casing 1 has quantity to be two supporting legs 2, the right side fixed mounting of casing 1 has one end to extend to its inside inlet pipe 3, the outside fixed mounting of inlet pipe 3 has first solenoid valve 4, the interior diapire fixed mounting of casing 1 has discharging pipe 5 that one end extends to its bottom, the outside fixed mounting of discharging pipe 5 has second solenoid valve 6, fixed mounting has heating pipe 7 on casing 1's the inner wall, casing 1's right side fixed mounting has controller 8 that is located the 3 below of inlet pipe.

The left side fixed mounting of casing 1 has one end to extend to its inside condensation subassembly 9, and condensation subassembly 9 includes cooler bin 91, and the left side fixed mounting of casing 1 has cooler bin 91, and the top fixed mounting of cooler bin 91 has one end to run through and extend to the condenser pipe 92 of its bottom, and the top fixed mounting of condenser pipe 92 has one end to extend to the inside connecting pipe 93 of casing 1.

The equal fixed mounting in top left and right sides of casing 1 has riser 10, fixed mounting has diaphragm 11 between two riser 10, the bottom movable mounting of diaphragm 11 has one end to extend to its casing 1 inside (mixing) shaft 12, the bottom fixed mounting of diaphragm 11 has first bearing, (mixing) shaft 12 rotates with diaphragm 11 through first bearing to be connected, the mounting hole with (mixing) shaft 12 looks adaptation is seted up at the top of casing 1, the outside sliding connection of (mixing) shaft 12 has sleeve 13 that is located casing 1 inside, the equal fixed mounting in the left and right sides of sleeve 13 has puddler 14 that quantity is four, four puddler 14 of unilateral are the equidistance and distribute.

The top fixed mounting of casing 1 has one end and the (mixing) shaft 12 outside fixed connection and the other end to extend to the drive assembly 15 on right side riser 10 right side, drive assembly 15 includes biax driving motor 151, the top fixed mounting of casing 1 has the biax driving motor 151 that is located between (mixing) shaft 12 and the right side riser 10 and is located diaphragm 11 below, the model of biax driving motor 151 is YSK78-4J, the left side output shaft fixed mounting of biax driving motor 151 has drive bevel gear 152, the outside fixed mounting of (mixing) shaft 12 has the driven bevel gear 153 that is located casing 1 top and one end and drive bevel gear 152 meshing, the right side output shaft of biax driving motor 151 extends to the right side of right side riser 10 and fixed mounting has drive gear 154.

The outside top fixed mounting of sleeve 13 has connecting bearing 16, connecting bearing 16's outside fixed mounting has connecting block 17, the equal fixed mounting in both sides has one end to run through casing 1 and extend to the extension rod 18 at diaphragm 11 top around the top of connecting block 17, the first through-hole with two extension rod 18 looks adaptations is all seted up to both sides around the roof in casing 1 respectively, the second through-hole with two extension rod 18 looks adaptations is all seted up to both sides around diaphragm 11 is inside respectively, the top fixed mounting of preceding side extension rod 18 has one end and 18 top fixed connection's of rear side extension rod framework 19.

The right side movable mounting of left side riser 10 has one end to pass framework 19 and extend to right side riser 10 right side and with the extrusion subassembly 20 of drive assembly 15 meshing, extrusion subassembly 20 includes pivot 201, the right side movable mounting of left side riser 10 has the pivot 201 that is located diaphragm 11 top and one end and passes framework 19 and extend to right side riser 10 right side, the right side fixed mounting of left side riser 10 has the second bearing that is located diaphragm 11 top, pivot 201 passes through the second bearing and is connected with left side riser 10 rotation, the perforation with pivot 201 looks adaptation is seted up to the inside of right side riser 10, the outside fixed mounting of pivot 201 has the disc 202 that is located framework 19 inside and one end and the laminating of framework 19 inner bottom wall, the outside fixed mounting of pivot 201 has the driven gear 203 that is located right side riser 10 right side and one end and drive gear 154 meshing, the diameter of driven gear 203 is greater than the diameter of drive gear 154.

When in use, the mixed raw material for nonane production is injected into the shell 1 through the feeding pipe 3, then the first electromagnetic valve 4 is closed, the heating pipe 7 is started to heat the mixed raw material, the double-shaft driving motor 151 is started to drive the driving bevel gear 152 and the driving gear 154 to rotate, the driving bevel gear 152 drives the stirring shaft 12, the sleeve 13 and the stirring rod 14 to integrally rotate through the driven bevel gear 153 in the rotating process, so as to stir the raw material, the driving gear 154 drives the rotating shaft 201 and the disc 202 to rotate through the driven gear 203 in the rotating process, the disc 202 extrudes the upper side and the lower side of the inner wall of the frame 19 in the rotating process, so as to drive the frame 19 and the extension rod 18 to reciprocate up and down, further drives the sleeve 13 and the stirring rod 14 to reciprocate up and down through the connecting block 17 and the connecting bearing 16, so that the stirring rod 14 cooperates with the reciprocating up and down in the rotating process to stir the raw material uniformly, so as to enable the raw material to be heated uniformly, the distilled solvent to be separated and enter the distillation discharging pipe 92, so as to be condensed, the distillation environment is discharged, and the second electromagnetic valve 93 is opened, so as to prevent the solvent from being liquefied and being discharged, so as to be condensed, and the second electromagnetic valve 6 to be condensed.

In summary, in the distillation apparatus for nonane production, the driving bevel gear 152 and the driving gear 154 are driven to rotate by starting the dual-shaft driving motor 151, wherein the driving bevel gear 152 drives the stirring shaft 12, the sleeve 13 and the stirring rod 14 to integrally rotate by the driven bevel gear 153 in the rotation process, so as to stir the raw materials, the driving gear 154 drives the rotating shaft 201 and the disc 202 to rotate by the driven gear 203 in the rotation process, the disc 202 extrudes the upper side and the lower side of the inner wall of the frame 19 in the rotation process, so as to drive the frame 19 and the extension rod 18 to vertically reciprocate, and further drives the sleeve 13 and the stirring rod 14 to vertically reciprocate by the connecting block 17 and the connecting bearing 16, so that the stirring rod 14 vertically reciprocates in the rotation process, so as to uniformly stir the raw materials, so as to uniformly heat the raw materials, further improve the distillation effect, and solve the problem that the conventional distillation apparatus for nonane production does not have the stirring function, so that the raw materials are easily mixed in the distillation process, and further the raw materials are easily heated unevenly, and the distillation effect of the solvent is greatly affected.

It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus. Without further limitation, an element defined by the phrases "comprising a," "8230," "8230," or "comprising" does not exclude the presence of additional like elements in a process, method, article, or apparatus that comprises the element.

Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims

1. The utility model provides a distillation plant is used in nonane production, includes casing (1), the bottom left and right sides of casing (1) all is provided with supporting legs (2) that quantity is two, the right side of casing (1) is provided with inlet pipe (3) that one end extends to its inside, the outside of inlet pipe (3) is provided with first solenoid valve (4), the interior diapire of casing (1) is provided with discharging pipe (5) that one end extends to its bottom, the outside of discharging pipe (5) is provided with second solenoid valve (6), be provided with heating pipe (7) on the inner wall of casing (1), the right side of casing (1) is provided with controller (8) that are located inlet pipe (3) below, the left side of casing (1) is provided with one end and extends to its inside condensation component (9), its characterized in that: the top left and right sides of casing (1) all is provided with riser (10), two be provided with between riser (10) diaphragm (11), the bottom of diaphragm (11) is provided with (mixing) shaft (12) that one end extends to its casing (1) inside, the outside of (mixing) shaft (12) is provided with and is located casing (1) inside sleeve (13), the left and right sides of sleeve (13) all is provided with puddler (14) that quantity is four, the top of casing (1) is provided with one end and (mixing) shaft (12) outside fixed connection and other end extend to drive assembly (15) on right side riser (10) right side, the outside top of sleeve (13) is provided with connecting bearing (16), the outside of connecting bearing (16) is provided with connecting block (17), both sides all are provided with one end around the top of connecting block (17) and run through casing (1) and extend to extension rod (18) at diaphragm (11) top, the front side the top of extension rod (18) is provided with one end and extends to frame (19) of frame (18) top fixed connection with rear side and rear side extension rod (10) top, and right side extension rod (10) and right side drive assembly (15) and extrusion drive assembly (20) meshing assembly (20).

2. The distillation device for nonane production according to claim 1, wherein: condensation subassembly (9) include cooler bin (91), the left side fixed mounting of casing (1) has cooler bin (91), the top fixed mounting of cooler bin (91) has condenser pipe (92) that one end runs through and extend to its bottom, the top fixed mounting of condenser pipe (92) has connecting pipe (93) that one end extends to casing (1) inside.

3. The distillation device for nonane production according to claim 1, wherein: drive assembly (15) include biax driving motor (151), the top fixed mounting of casing (1) has biax driving motor (151) that is located between (mixing) shaft (12) and right side riser (10) and is located diaphragm (11) below, the left side output shaft fixed mounting of biax driving motor (151) has drive bevel gear (152), the outside fixed mounting of (mixing) shaft (12) has driven bevel gear (153) that is located casing (1) top and one end and drive bevel gear (152) meshing, the right side output shaft of biax driving motor (151) extends to the right side of right side riser (10) and fixed mounting has drive gear (154).

4. The distillation device for nonane production according to claim 3, wherein: extrusion subassembly (20) are including pivot (201), left side the right side movable mounting of riser (10) has pivot (201) that is located diaphragm (11) top and one end and passes framework (19) and extend to right side riser (10) right side, the outside fixed mounting of pivot (201) has disc (202) that is located framework (19) inside and one end and framework (19) inner bottom wall laminating, the outside fixed mounting of pivot (201) has driven gear (203) that is located right side riser (10) right side and one end and drive gear (154) meshing.

5. The distillation device for nonane production according to claim 1, wherein: the stirring shaft (12) is rotatably connected with the transverse plate (11) through the first bearing, and a mounting hole matched with the stirring shaft (12) is formed in the top of the shell (1).

6. The distillation device for nonane production according to claim 1, wherein: first through-holes matched with the two extension rods (18) respectively are formed in the front side and the rear side of the inner top wall of the shell (1), and second through-holes matched with the two extension rods (18) respectively are formed in the front side and the rear side of the inner portion of the transverse plate (11).