CN218188014U

CN218188014U - Agitating unit of crystallizer is used in zirconium oxychloride production

Info

Publication number: CN218188014U
Application number: CN202222384643.3U
Authority: CN
Inventors: 刘福来; 刘振明; 杨新利
Original assignee: Shandong Hongyuan New Material Technology Co ltd
Current assignee: Shandong Hongyuan New Material Technology Co ltd
Priority date: 2022-09-08
Filing date: 2022-09-08
Publication date: 2023-01-03
Anticipated expiration: 2032-09-08

Abstract

The utility model discloses a stirring device of a crystallizing tank for producing zirconium oxychloride, which relates to the technical field of zirconium oxychloride production, and comprises a tank body and a supporting frame, wherein a stirring rod and stirring blades are arranged in the tank body; this agitating unit of crystallizer is used in zirconium oxychloride production rotates through two motors and drives the worm and rotate and drive the worm wheel and rotate and drive the dwang and rotate to drive the thread bush and rotate, make the thread bush rebound and drive the bracing piece and rotate, make the stirring leaf remove and stop motor two to rotate after stirring leaf one side laminating jar internal wall on one side of the internal wall, connect the restart motor one to rotate and drive the stirring leaf and rotate and strike off the crystallization on the internal wall of jar.

Description

Agitating unit of crystallizer is used in zirconium oxychloride production

Technical Field

The utility model relates to a zirconium oxychloride production technology, concretely relates to zirconium oxychloride production is with agitating unit of crystallizer.

Background

After zircon sand powder and carbon powder are mixed, the mixture is added into a fluidized bed chlorination furnace according to a certain proportion, chlorine is introduced to react to generate zirconium tetrachloride and crude silicon tetrachloride, the crude zirconium tetrachloride is hydrolyzed, filtered, evaporated and concentrated, cooled and crystallized, washed and dried to produce the commodity zirconium oxychloride, the zirconium tetrachloride is dissolved in water to generate zirconium oxychloride solution and hydrochloric acid, and the zirconium oxychloride crystal is separated out from mother liquor by utilizing the characteristics that the solubility of the zirconium oxychloride in the hydrochloric acid is reduced along with the increase of acidity and is increased along with the increase of temperature and adjusting the acidity and the temperature of the solution by means of evaporation and concentration.

In the existing production zirconium oxychloride process, the mother liquor is heated for transferring and stirring when directly heating the crystallizer, the stirring mother liquor can ensure that the mother liquor is heated uniformly, the zirconium oxychloride crystal generally can grow along the inner wall of the tank body after the evaporation is finished and the mother liquor is cooled, the crystal can adhere to the inner wall and can not fall to the bottom of the tank body, manual scraping is needed when the crystal is collected, and the collection efficiency of zirconium oxychloride crystallization products is influenced.

SUMMERY OF THE UTILITY MODEL

The utility model aims at providing a zirconium oxychloride production is with agitating unit of crystallizer to solve the above-mentioned weak point among the prior art.

In order to achieve the above object, the present invention provides the following technical solutions: the utility model provides a stirring apparatus of crystallizer for production of zirconium oxychloride, includes a jar body and a support frame, the internal puddler that is equipped with of jar, puddler one side is equipped with the stirring leaf, actuating mechanism installs in jar body one side, and actuating mechanism is connected with puddler one side, actuating mechanism drive puddler rotates and rotates in order to drive the stirring leaf, actuating mechanism installs in support frame one side, drive mechanism installs in drive mechanism one side, supporting mechanism installs in drive mechanism one side, and supporting mechanism one side is connected with the stirring leaf, actuating mechanism drive mechanism rotates and drives supporting mechanism and remove and carry out the translation in order to drive the stirring leaf.

Further, actuating mechanism includes motor one, motor one side and jar body one side fixed connection, motor one output shaft one end fixedly connected with gear one, gear one side meshing is connected with gear two, gear two one side and puddler one end fixed connection, puddler one end run through jar body and with jar internal wall rotation connection.

Furthermore, the driving mechanism comprises a second motor, and one side of the second motor is fixedly connected with one side of the support frame.

Further, drive mechanism includes worm, worm wheel and dwang, two output shaft one end fixed connection of worm one end and motor, the worm other end rotates with support frame one side and is connected, the worm is connected with worm wheel one side meshing, worm wheel one side and dwang one end fixed connection, dwang one end run through the puddler and rotate with the puddler inner wall and be connected, dwang one end is rotated with jar body bottom and is connected.

Further, supporting mechanism includes thread bush and three bracing piece, wherein two bracing piece one end rotates with the puddler both ends respectively and is connected, and wherein two bracing piece other ends rotate with same stirring leaf one side respectively and be connected, another bracing piece one end rotates with stirring leaf one side and is connected, another the bracing piece other end rotates and is connected with the bearing, bearing inner wall and thread bush outside fixed connection, thread bush inner wall and dwang one end threaded connection.

Further, jar body top is equipped with the inlet, jar body bottom is equipped with the discharge gate, support frame one side and jar body top fixed connection.

Compared with the prior art, the utility model provides a pair of agitating unit of crystallizer is used in zirconium oxychloride production has following beneficial effect: 1. this agitating unit of crystallizer is used in zirconium oxychloride production rotates drive gear one through a motor and rotates and drive two rotations of gear and rotate in order to drive the puddler to bracing piece through among the supporting mechanism drives the stirring leaf and rotates, stirs the internal mother liquor of jar through the stirring leaf, makes the mother liquor be heated evenly, rapid heating up and accelerate mother liquor evaporation rate.

2. This agitating unit of crystallizer is used in zirconium oxychloride production rotates through two motors and drives the worm and rotate and drive worm wheel rotation and drive the dwang and rotate to drive the thread bush and rotate, make the thread bush rebound and drive the bracing piece and rotate, make the stirring leaf remove and stop motor two rotations behind stirring leaf one side laminating jar internal wall to jar internal wall one side, thereby connect restart motor one to rotate and drive the stirring leaf and rotate and strike off the crystallization on the internal wall of jar, practiced thrift the cost of labor.

Drawings

In order to more clearly illustrate the embodiments of the present application or the technical solutions in the prior art, the drawings needed to be used in the embodiments will be briefly described below, and it is obvious that the drawings in the following description are only some embodiments described in the present invention, and other drawings can be obtained by those skilled in the art according to these drawings.

Fig. 1 is a perspective view of the overall structure provided by the embodiment of the present invention;

fig. 2 is a cross-sectional perspective view of the overall structure provided by the embodiment of the present invention;

fig. 3 is a perspective view of a threaded sleeve structure provided by the embodiment of the present invention.

Description of reference numerals:

1. a tank body; 11. a stirring rod; 12. stirring blades; 2. a support frame; 3. a starting mechanism; 31. a first motor; 32. a first gear; 33. a second gear; 4. a drive mechanism; 41. a second motor; 5. a transmission mechanism; 51. a worm; 52. a worm gear; 53. rotating the rod; 6. a support mechanism; 61. a threaded sleeve; 62. a support rod.

Detailed Description

In order to make those skilled in the art better understand the technical solution of the present invention, the present invention will be further described in detail with reference to the attached drawings.

The first embodiment is as follows:

referring to fig. 1-3, a stirring device of a crystallizing tank for producing zirconium oxychloride comprises a tank body 1 and a support frame 2, wherein a stirring rod 11 is arranged in the tank body 1, a stirring blade 12 is arranged on one side of the stirring rod 11, a heating device is arranged outside the tank body 1, the heating device heats mother liquor in the tank body through the tank body 1 to evaporate a solvent in the mother liquor, a liquid inlet is arranged on the top of the tank body 1, a discharge port is arranged at the bottom of the tank body 1, a valve is arranged on the discharge port, one side of the support frame 2 is fixedly connected with the top of the tank body 1, a starting mechanism 3 is arranged on one side of the tank body 1 and is connected with one side of the stirring rod 11, the starting mechanism 3 drives the stirring rod 11 to rotate so as to drive the stirring blade 12 to rotate, the starting mechanism 3 comprises a motor one 31, one side of the motor one 31 is fixedly connected with one side of the tank body 1, one end of an output shaft of the motor one 31 is fixedly connected with a gear one 32, one side of the first gear 32 is engaged with the second gear 33, one side of the second gear 33 is fixedly connected with one end of the stirring rod 11, the first motor 31 rotates to drive the first gear 32 to rotate and drive the second gear 33 to rotate so as to drive the stirring rod 11 to rotate, so that the supporting rod 62 in the supporting mechanism 6 drives the stirring blade 12 to rotate, one end of the stirring rod 11 penetrates through the tank body 1 and is rotatably connected with the inner wall of the tank body 1, the driving mechanism 4 is installed on one side of the supporting frame 2, the driving mechanism 4 comprises a second motor 41, one side of the second motor 41 is fixedly connected with one side of the supporting frame 2, the transmission mechanism 5 is installed on one side of the driving mechanism 4, the transmission mechanism 5 comprises a worm 51, a worm wheel 52 and a rotating rod 53, one end of the worm 51 is fixedly connected with one end of an output shaft of the second motor 41, the other end of the worm 51 is rotatably connected with one side of the supporting frame 2, the worm 51 is engaged with one side of the worm wheel 52, one side of the worm wheel 52 is fixedly connected with one end of the rotating rod 53, one end of a rotating rod 53 penetrates through the stirring rod 11 and is rotatably connected with the inner wall of the stirring rod 11, one end of the rotating rod 53 is rotatably connected with the bottom of the tank body 1, a second motor 41 rotates to drive a worm 51 to rotate to drive a worm gear 52 to rotate and drive the rotating rod 53 to rotate, a supporting mechanism 6 is installed on one side of a transmission mechanism 5, one side of the supporting mechanism 6 is connected with the stirring blade 12, a driving mechanism 4 drives the transmission mechanism 5 to rotate to drive the supporting mechanism 6 to move so as to drive the stirring blade 12 to translate, the supporting mechanism 6 comprises a threaded sleeve 61 and three supporting rods 62, one ends of the two supporting rods 62 are respectively rotatably connected with two ends of the stirring rod 11, the other ends of the two supporting rods 62 are respectively rotatably connected with one side of the same stirring blade 12, one end of the other supporting rod 62 is rotatably connected with one side of the stirring blade 12, the other end of the other supporting rod 62 is rotatably connected with a bearing, the inner wall of the bearing is fixedly connected with the outer side of the threaded sleeve 61, the inner wall of the threaded sleeve 61 is in threaded sleeve 53, the threaded sleeve 61 moves upwards and drives the supporting rod 62 to rotate, so that the stirring blade 12 moves towards one side of the tank body 1 and is attached to the inner wall of the stirring blade 12, and the inner wall of the stirring blade is scraped off after the inner wall of the tank body 31 of the stirring blade 12 is attached to be attached to the inner wall of the tank body, and the stirring blade 12.

The working principle is as follows: when the mother liquor heating device is used, firstly, a worker pours mother liquor into the tank body 1 from a feed port, then, a heating device on the tank body 1 is started, a first motor 31 is started to rotate, the first motor 31 rotates to drive a first gear 32 to rotate and drive a second gear 33 to rotate so as to drive a stirring rod 11 to rotate, so that a supporting rod 62 in a supporting mechanism 6 drives a stirring blade 12 to rotate, the mother liquor in the tank body 1 is stirred through the stirring blade 12, the mother liquor is heated uniformly, the temperature is rapidly raised, the evaporation speed of the mother liquor is accelerated, after the mother liquor is evaporated, the first motor 31 stops rotating, the mother liquor starts to crystallize after standing and radiating, after the crystallization is finished, a second motor 41 starts to rotate, a worm 51 rotates to drive a worm gear 52 to rotate and drive a rotating rod 53 to rotate, so as to drive a threaded sleeve 61 to rotate, the threaded sleeve 61 moves upwards and drives the supporting rod 62 to rotate, so that the stirring blade 12 moves towards one side of the inner wall of the tank body 1 and adheres to the inner wall of the tank body 1 on one side of the stirring blade 12, the inner wall of the tank body 1, the second motor 41 stops rotating, the rotating is started again to drive the first motor 31 to rotate so as to drive the stirring blade 12 to rotate, so as to scrape crystals on the inner wall of the tank body 1, finally, a discharge port of the mother liquor, and collect a product of the mother liquor flowing out of the mother liquor of the tank body 1, and then the mother liquor flowing out of the mother liquor.

While certain exemplary embodiments of the present invention have been described above by way of illustration only, it will be apparent to those of ordinary skill in the art that the described embodiments may be modified in various different ways without departing from the spirit and scope of the present invention. Accordingly, the drawings and description are to be regarded as illustrative in nature and not as restrictive on the scope of the appended claims.

Claims

1. The utility model provides a zirconium oxychloride production is with agitating unit of crystallizer, includes a jar body (1) and support frame (2), be equipped with puddler (11) in jar body (1), puddler (11) one side is equipped with stirring leaf (12), its characterized in that:

the starting mechanism (3) is arranged on one side of the tank body (1), the starting mechanism (3) is connected with one side of the stirring rod (11), and the starting mechanism (3) drives the stirring rod (11) to rotate so as to drive the stirring blades (12) to rotate;

the driving mechanism (4), the said driving mechanism (4) is installed on one side of the supporting arm (2);

the transmission mechanism (5), the said transmission mechanism (5) is installed on one side of driving mechanism (4);

the supporting mechanism (6) is installed on one side of the transmission mechanism (5), one side of the supporting mechanism (6) is connected with the stirring blade (12), and the driving mechanism (4) drives the transmission mechanism (5) to rotate to drive the supporting mechanism (6) to move so as to drive the stirring blade (12) to move horizontally.

2. The stirring device of the crystallizing tank for producing the zirconium oxychloride as claimed in claim 1, wherein the starting mechanism (3) comprises a first motor (31), one side of the first motor (31) is fixedly connected with one side of the tank body (1), one end of an output shaft of the first motor (31) is fixedly connected with a first gear (32), one side of the first gear (32) is engaged with a second gear (33), one side of the second gear (33) is fixedly connected with one end of the stirring rod (11), and one end of the stirring rod (11) penetrates through the tank body (1) and is rotatably connected with the inner wall of the tank body (1).

3. The stirring device of the crystallization tank for producing zirconium oxychloride as claimed in claim 1, wherein the driving mechanism (4) comprises a second motor (41), and one side of the second motor (41) is fixedly connected with one side of the support frame (2).

4. The stirring device of the crystallization tank for producing zirconium oxychloride as claimed in claim 3, wherein the transmission mechanism (5) comprises a worm (51), a worm wheel (52) and a rotating rod (53), one end of the worm (51) is fixedly connected with one end of an output shaft of the motor II (41), the other end of the worm (51) is rotatably connected with one side of the support frame (2), the worm (51) is meshed with one side of the worm wheel (52), one side of the worm wheel (52) is fixedly connected with one end of the rotating rod (53), one end of the rotating rod (53) penetrates through the stirring rod (11) and is rotatably connected with the inner wall of the stirring rod (11), and one end of the rotating rod (53) is rotatably connected with the bottom of the tank body (1).

5. The stirring device of the crystallization tank for producing zirconium oxychloride as claimed in claim 4, wherein the supporting mechanism (6) comprises a threaded sleeve (61) and three supporting rods (62), wherein two of the supporting rods (62) are rotatably connected with two ends of the stirring rod (11) at one end respectively, and wherein the other ends of the two supporting rods (62) are rotatably connected with one side of the same stirring blade (12), one end of the other supporting rod (62) is rotatably connected with one side of the stirring blade (12), the other end of the other supporting rod (62) is rotatably connected with a bearing, the inner wall of the bearing is fixedly connected with the outer side of the threaded sleeve (61), and the inner wall of the threaded sleeve (61) is in threaded connection with one end of the rotating rod (53).

6. The stirring device of the crystallizing tank for producing zirconium oxychloride as claimed in claim 1, wherein a liquid inlet is arranged at the top of the tank body (1), a discharge outlet is arranged at the bottom of the tank body (1), and one side of the support frame (2) is fixedly connected with the top of the tank body (1).