CN218107679U - KCl evaporating salt production device - Google Patents

KCl evaporating salt production device Download PDF

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CN218107679U
CN218107679U CN202222426342.2U CN202222426342U CN218107679U CN 218107679 U CN218107679 U CN 218107679U CN 202222426342 U CN202222426342 U CN 202222426342U CN 218107679 U CN218107679 U CN 218107679U
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heating
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吴保清
张明峰
尤玉豹
薛学勇
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Inner Mongolia Kunpeng New Material Co ltd
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Abstract

本实用新型提供一种KCl蒸发析盐生产装置,包括进料泵、进料预热器、加热室、蒸发结晶室、循环泵和集盐罐;进料泵、进料预热器和加热室依次连接,加热室的物料出口与蒸发结晶室的进料口连接;蒸发结晶室的蒸汽出口与进料预热器的加热介质入口连接,蒸发结晶室的结晶体出口与集盐罐连接,蒸发结晶室的循环料出口与循环泵的入口连接;循环泵的出口与加热室的进料口连接;加热室的加热管的外壁间隙中设置有振动除垢机构,振动除垢机构包括多根振动杆和设置在多根振动杆的两端的振动电机。本实用新型的装置解决了现有蒸发结晶装置中,因溶液蒸发析晶导致加热管内壁结垢,以及装置换热效率降低、处理量减少、堵塞加热管和停运疏通清洗频率高的问题。

Figure 202222426342

The utility model provides a KCl evaporation and salt production device, comprising a feed pump, a feed preheater, a heating chamber, an evaporation crystallization chamber, a circulation pump and a salt collection tank; a feed pump, a feed preheater and a heating chamber Connect in sequence, the material outlet of the heating chamber is connected to the feed port of the evaporation crystallization chamber; the steam outlet of the evaporation crystallization chamber is connected to the heating medium inlet of the feed preheater, the crystal outlet of the evaporation crystallization chamber is connected to the salt collection tank, and the evaporation crystallization The outlet of the circulating material in the chamber is connected to the inlet of the circulating pump; the outlet of the circulating pump is connected to the feeding port of the heating chamber; a vibration descaling mechanism is arranged in the gap between the outer wall of the heating tube of the heating chamber, and the vibration descaling mechanism includes multiple vibrating rods and vibrating motors arranged at both ends of a plurality of vibrating rods. The device of the utility model solves the problems of scaling on the inner wall of the heating tube due to evaporation and crystallization of the solution in the existing evaporation crystallization device, as well as reduced heat exchange efficiency of the device, reduced processing capacity, blockage of the heating tube and high frequency of dredging and cleaning during shutdown.

Figure 202222426342

Description

KCl蒸发析盐生产装置KCl evaporating salt production device

技术领域technical field

本实用新型涉及氯化钾生产技术领域,尤其涉及一种KCl蒸发析盐生产装置。The utility model relates to the technical field of potassium chloride production, in particular to a KCl evaporation salt production device.

背景技术Background technique

由于矿产资源丰富、生产方法简单、含钾量高而成本低等原因,至今氯化钾仍为世界上最主要的钾肥品种,约占全球钾肥销售总量的90%以上,其中50%能直接施用,其余主要用来制造复合肥料。氯化钾为植物生长所需的重要肥料,肥效快,并能被土壤吸收,不易流失,施用适量钾肥,能使作物茎杆长得坚实,防止倒伏,促进开花结果,增强抗旱、抗寒、抗病虫害的能力,因此对农业高产具有十分重要的意义。氯化钾化肥中,氯化钾含量一般达90-95%以上,其中K2O含量约为60-63%,含氯(Cl)约47.6%,此外还含有少量的钠、钙、镁、溴和硫酸根等,它具有吸湿性,易结块,易溶于水。纯品氯化钾为白色或淡黄色立方形结晶。Due to rich mineral resources, simple production methods, high potassium content and low cost, potassium chloride is still the most important potash fertilizer in the world, accounting for more than 90% of the global potash fertilizer sales, of which 50% can be directly The rest is mainly used to make compound fertilizers. Potassium chloride is an important fertilizer needed for plant growth. It has fast fertilizer efficiency and can be absorbed by the soil, so it is not easy to lose. Applying appropriate amount of potassium fertilizer can make the crop stems grow firm, prevent lodging, promote flowering and fruiting, and enhance drought resistance, cold resistance, The ability to resist diseases and insect pests is of great significance to high agricultural yield. In potassium chloride fertilizer, the content of potassium chloride is generally more than 90-95%, of which K 2 O content is about 60-63%, and chlorine (Cl) is about 47.6%. In addition, it also contains a small amount of sodium, calcium, magnesium, Bromine and sulfate, etc., it is hygroscopic, easy to agglomerate, and soluble in water. Pure potassium chloride is white or light yellow cubic crystal.

同时,氯化钾也是工业中一种重要的无机复合盐,工业需求量日益增大,因此出现了较大的氯化钾盐结晶缺口,急需大型化、连续化的生产方法来缓解。考虑到氯化钾的处理量及蒸发量,以及氯化钾的溶解度随温度变化不大的情况,通过降温冷却结晶的方式分离氯化钾,存在晶体析出不明显、产品纯度较低、生产效率低、无法进行连续化生产的问题,而蒸发结晶是通过蒸发溶剂来析盐的,溶剂被蒸发后残留的溶质即氯化钾晶体了,因此氯化钾采用蒸发结晶工艺比较适合。Simultaneously, potassium chloride is also a kind of important inorganic compound salt in the industry, and the industrial demand is increasing day by day, so there has been a larger crystallization gap of potassium chloride salt, which needs to be alleviated by large-scale and continuous production methods. Considering the amount of processing and evaporation of potassium chloride, and the fact that the solubility of potassium chloride does not change much with temperature, potassium chloride is separated by cooling and crystallization, but crystal precipitation is not obvious, product purity is low, and production efficiency is low. The problem of low cost and inability to carry out continuous production, while evaporative crystallization is to precipitate salt by evaporating the solvent, and the residual solute after the solvent is evaporated is potassium chloride crystal, so the evaporative crystallization process for potassium chloride is more suitable.

蒸发结晶工艺是通过溶剂的散失(即蒸发)使溶液达到饱和状态,继而达到过饱和状态,在一定的温度下,一定量的水(或溶剂)所能溶解的某一溶质的质量是有限的,那么多余的溶质就会随着溶剂的减少而析出,即结晶。但是,现有的蒸发结晶装置中,无论是自然循环还是强制循环,都存在由于溶液蒸发析晶导致装置的加热室的加热管内壁结垢的情况,加热管内壁上的盐垢不但会影响加热管的换热效率和蒸发效果,长时间结垢还会堵塞加热管,而加热管内壁上的盐垢并不容易清理,疏通及清洗频率较高,且疏通及清洗都会导致装置停运、生产处理量减少的问题。The evaporation crystallization process is to make the solution reach saturation through the loss of the solvent (ie evaporation), and then reach the supersaturated state. At a certain temperature, the quality of a certain solute that can be dissolved by a certain amount of water (or solvent) is limited. , then the excess solute will precipitate out with the reduction of the solvent, that is, crystallization. However, in existing evaporative crystallization devices, no matter whether it is natural circulation or forced circulation, there is a situation that the inner wall of the heating tube of the heating chamber of the device is fouled due to the evaporation and crystallization of the solution. The heat exchange efficiency and evaporation effect of the tube, the scaling for a long time will block the heating tube, and the salt scale on the inner wall of the heating tube is not easy to clean, the frequency of dredging and cleaning is high, and dredging and cleaning will lead to the shutdown of the device and the production Handle volume reduction issues.

实用新型内容Utility model content

本实用新型提供一种KCl蒸发析盐生产装置,用以解决现有的蒸发结晶装置中,由于溶液蒸发析晶导致加热管内壁结垢,进而导致装置的换热效率降低、处理量减少、堵塞加热管和停运疏通清洗的频率高的问题。The utility model provides a KCl evaporative salt production device, which is used to solve the problem that in the existing evaporative crystallization device, the scaling on the inner wall of the heating tube is caused by the evaporation and crystallization of the solution, which further leads to the reduction of the heat exchange efficiency of the device, the reduction of the processing capacity, and the blockage. The problem of high frequency of cleaning of heating pipes and outage dredging.

本实用新型提供一种KCl蒸发析盐生产装置,包括:进料泵、进料预热器、加热室、蒸发结晶室、循环泵和集盐罐;进料泵、进料预热器和加热室的下部的进料口通过进料管道依次连接,加热室的顶部的物料出口与蒸发结晶室的进料口连接。The utility model provides a KCl evaporation and salt production device, comprising: a feed pump, a feed preheater, a heating chamber, an evaporation crystallization chamber, a circulation pump and a salt collection tank; a feed pump, a feed preheater and a heating The feed inlet at the lower part of the chamber is connected sequentially through feed pipes, and the material outlet at the top of the heating chamber is connected with the feed inlet of the evaporation crystallization chamber.

具体的,蒸发结晶室的顶部的蒸汽出口与进料预热器的加热介质入口连接,蒸发结晶室的底部的结晶体出口与集盐罐连接,蒸发结晶室的下部的循环料出口与循环泵的入口连接;循环泵的出口与加热室的进料口连接;进料预热器的加热介质出口通过冷水管道排往回收池。Specifically, the steam outlet at the top of the evaporation crystallization chamber is connected to the heating medium inlet of the feed preheater, the crystal outlet at the bottom of the evaporation crystallization chamber is connected to the salt collection tank, and the circulation material outlet at the bottom of the evaporation crystallization chamber is connected to the circulation pump. The inlet is connected; the outlet of the circulation pump is connected with the feed inlet of the heating chamber; the outlet of the heating medium of the feed preheater is discharged to the recovery pool through the cold water pipe.

具体的,加热室的加热管的外壁间隙中设置有振动除垢机构,振动除垢机构包括多根贯穿加热室的振动杆,和,设置在多根振动杆的两端的振动电机;振动电机设置在加热室的外部。Specifically, a vibration descaling mechanism is provided in the outer wall gap of the heating tube of the heating chamber, and the vibration descaling mechanism includes a plurality of vibration rods penetrating the heating chamber, and vibration motors arranged at both ends of the plurality of vibration rods; the vibration motor is set outside the heating chamber.

具体的,蒸发结晶室的进料口设置在蒸发结晶室的筒体的切线方向上,加热室的顶部的物料出口通过管道与蒸发结晶室形成切向连接。Specifically, the feed port of the evaporative crystallization chamber is arranged in the tangential direction of the cylinder of the evaporative crystallization chamber, and the material outlet at the top of the heating chamber forms a tangential connection with the evaporative crystallization chamber through a pipe.

具体的,蒸发结晶室与集盐罐之间还设置有压滤机;压滤机的进料口与蒸发结晶室的底部的结晶体出口连接,压滤机的母液出口与进料预热器的物料入口连接,压滤机的结晶出管与集盐罐连接。Specifically, a filter press is also arranged between the evaporation crystallization chamber and the salt collection tank; the feed inlet of the filter press is connected to the crystal outlet at the bottom of the evaporation crystallization chamber, and the mother liquor outlet of the filter press is connected to the outlet of the feed preheater. The material inlet is connected, and the crystallization outlet pipe of the filter press is connected with the salt collection tank.

具体的,蒸发结晶室的蒸汽出口的下方还设置有除沫网板,除沫网板的上方还设置有防堵喷淋管。Specifically, a defoaming screen is provided below the steam outlet of the evaporation and crystallization chamber, and an anti-blocking spray pipe is provided above the defoaming screen.

具体的,蒸发结晶室的下部为倒锥形结构,锥度为45°-60°。Specifically, the lower part of the evaporation and crystallization chamber is an inverted cone structure with a taper of 45°-60°.

具体的,加热室内设置有自动清垢结构,自动清垢结构包括弹簧支架,弹簧,限位卡板和清洗螺旋钢丝;弹簧的一端与弹簧支架固定连接,弹簧的另一端与限位卡板的一端固定连接,限位卡板的另一端与清洗螺旋钢丝的一端连接;弹簧支架与加热室的下部固定连接,且弹簧支架设置在加热室的进料口的上方;弹簧和限位卡板设置在加热室的加热管的外部,清洗螺旋钢丝伸入加热管的内部;弹簧、限位卡板和清洗螺旋钢丝与加热管一一对应设置。Specifically, the heating chamber is equipped with an automatic scale cleaning structure, which includes a spring bracket, a spring, a limit clamp and a cleaning spiral steel wire; one end of the spring is fixedly connected to the spring support, and the other end of the spring is connected to the limit clamp. One end is fixedly connected, and the other end of the limit clamp is connected to one end of the cleaning spiral steel wire; the spring support is fixedly connected to the lower part of the heating chamber, and the spring support is arranged above the feeding port of the heating chamber; the spring and the limit clamp are set Outside the heating tube of the heating chamber, the cleaning spiral steel wire extends into the inside of the heating tube; the spring, the limit clamp and the cleaning spiral steel wire are arranged in correspondence with the heating tube.

具体的,限位卡板与弹簧相连的端部的宽度为加热管的外径的1.1-1.5倍,限位卡板的长度为50-100mm。Specifically, the width of the end of the limit clip connected to the spring is 1.1-1.5 times the outer diameter of the heating tube, and the length of the limit clip is 50-100 mm.

具体的,清洗螺旋钢丝的长度比加热管的长度短200-500mm,清洗螺旋钢丝的外径为加热管的内径的0.7-0.9倍。Specifically, the length of the cleaning spiral steel wire is 200-500mm shorter than the length of the heating tube, and the outer diameter of the cleaning spiral steel wire is 0.7-0.9 times the inner diameter of the heating tube.

本实用新型提供的KCl蒸发析盐生产装置能实现氯化钾的连续化生产,循环加热蒸发能提升蒸发结晶效率,使得处理量大幅度提高,装置运行稳定性高,解决氯化钾纯度低、产量低、生产成本高以及生产效率低的问题,提高经济效益。The KCl evaporative salt production device provided by the utility model can realize the continuous production of potassium chloride, and the circulation heating and evaporation can improve the evaporation crystallization efficiency, so that the processing capacity is greatly increased, the device has high operating stability, and solves the problem of low purity of potassium chloride, The problems of low output, high production cost and low production efficiency can improve economic benefits.

本实用新型提供的KCl蒸发析盐生产装置在生产运行中,利用振动除垢机构和自动清垢结构,能避免加热管内壁结垢和频繁堵塞,降低装置停运和疏通清洗的频率,提高换热效率,使得料液过饱和度均匀,结晶体粒度分布良好,装置能耗低,故障发生少,外源蒸汽用量少,实现了高效率连续性结晶。The KCl evaporative salt production device provided by the utility model uses a vibration descaling mechanism and an automatic descaling structure during production and operation, which can avoid scaling and frequent blockage on the inner wall of the heating tube, reduce the frequency of device shutdown and dredging and cleaning, and improve the efficiency of replacement. The thermal efficiency makes the supersaturation of the feed liquid uniform, the crystal particle size distribution is good, the energy consumption of the device is low, the failure occurs less, and the amount of external steam is small, realizing high-efficiency continuous crystallization.

附图说明Description of drawings

为了更清楚地说明本实用新型实施例或现有技术中的技术方案,下面将对实施例或现有技术描述中所需要使用的附图作一简单地介绍,显而易见地,下面描述中的附图是本实用新型的一些实施例,对于本领域普通技术人员来讲,在不付出创造性劳动的前提下,还可以根据这些附图获得其他的附图。In order to more clearly illustrate the technical solutions in the embodiments of the present invention or the prior art, the following will briefly introduce the accompanying drawings that need to be used in the description of the embodiments or the prior art. Obviously, the appended drawings in the following description The drawings show some embodiments of the utility model, and those skilled in the art can also obtain other drawings according to these drawings without creative work.

图1为本实用新型一实施例提供的KCl蒸发析盐生产装置的结构示意图;Fig. 1 is the structural representation of the KCl evaporative salt production device that an embodiment of the present invention provides;

图2为本实用新型一实施例提供的振动除垢机构的结构示意图;Fig. 2 is a structural schematic diagram of a vibration descaling mechanism provided by an embodiment of the present invention;

图3为本实用新型另一实施例提供的KCl蒸发析盐生产装置的结构示意图;Fig. 3 is the structural representation of the KCl evaporative salt production device that another embodiment of the present invention provides;

图4为本实用新型一实施例提供的自动清垢结构的结构示意图。Fig. 4 is a structural schematic diagram of an automatic cleaning structure provided by an embodiment of the present invention.

附图标记说明:Explanation of reference signs:

1、进料泵,2、进料预热器,3、加热室,4、蒸发结晶室,5、循环泵,6、集盐罐,7、压滤机,31、振动杆,32、振动电机,33、弹簧支架,34、弹簧,35、限位卡板,36、清洗螺旋钢丝,41、除沫网板,42、防堵喷淋管。1. Feed pump, 2. Feed preheater, 3. Heating chamber, 4. Evaporation and crystallization chamber, 5. Circulation pump, 6. Salt collection tank, 7. Filter press, 31. Vibration rod, 32. Vibration Motor, 33, spring support, 34, spring, 35, limit clamp, 36, cleaning spiral steel wire, 41, defoaming mesh plate, 42, anti-blocking spray pipe.

具体实施方式detailed description

为使本实用新型实施例的目的、技术方案和优点更加清楚,下面对本实用新型实施例中的技术方案进行清楚、完整地描述,显然,所描述的实施例是本实用新型一部分实施例,而不是全部的实施例。基于本实用新型中的实施例,本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其它实施例,也属于本实用新型保护的范围。In order to make the purpose, technical solutions and advantages of the embodiments of the present invention clearer, the technical solutions in the embodiments of the present invention are clearly and completely described below. Obviously, the described embodiments are part of the embodiments of the present invention, and Not all examples. Based on the embodiments of the present invention, all other embodiments obtained by persons of ordinary skill in the art without making creative efforts also belong to the scope of protection of the present invention.

如图1所示,本实用新型提供一种KCl蒸发析盐生产装置,包括:进料泵1、进料预热器2、加热室3、蒸发结晶室4、循环泵5和集盐罐6;进料泵1、进料预热器2和加热室3的下部的进料口通过进料管道依次连接,加热室3的顶部的物料出口与蒸发结晶室4的进料口连接。As shown in Figure 1, the utility model provides a KCl evaporative salt production device, including: feed pump 1, feed preheater 2, heating chamber 3, evaporation crystallization chamber 4, circulation pump 5 and salt collection tank 6 ; Feed pump 1, feed preheater 2 and the lower feed port of heating chamber 3 are connected sequentially through feed pipelines, and the material outlet at the top of heating chamber 3 is connected with the feed port of evaporation crystallization chamber 4.

具体的,蒸发结晶室4的顶部的蒸汽出口与进料预热器2的加热介质入口连接,蒸发结晶室4的底部的结晶体出口与集盐罐6连接,蒸发结晶室4的下部的循环料出口与循环泵5的入口连接;循环泵5的出口与加热室3的进料口连接;进料预热器2的加热介质出口通过冷水管道排往回收池。Specifically, the steam outlet at the top of the evaporation crystallization chamber 4 is connected with the heating medium inlet of the feed preheater 2, the crystal outlet at the bottom of the evaporation crystallization chamber 4 is connected with the salt collection tank 6, and the circulating material at the bottom of the evaporation crystallization chamber 4 The outlet is connected to the inlet of the circulation pump 5; the outlet of the circulation pump 5 is connected to the feed port of the heating chamber 3; the outlet of the heating medium of the feed preheater 2 is discharged to the recovery pool through the cold water pipeline.

通过设置使用外源蒸汽的加热室3对含有KCl的料液进行蒸发处理,方便料液在蒸发结晶室4中进行结晶和分离;利用蒸发结晶室4排出的二次蒸汽对进料预热器2中的进料进行预热,既能回收利用余热,节约能源,避免热量损耗,又能对进料进行提前预热,能降低加热室3的热源需求量和外源蒸汽消耗量,降低生产成本。The feed liquid containing KCl is evaporated by setting the heating chamber 3 using external steam, so that the feed liquid is crystallized and separated in the evaporation crystallization chamber 4; The feed material in 2 is preheated, which can not only recycle waste heat, save energy, avoid heat loss, but also preheat the feed material in advance, which can reduce the heat source demand and external steam consumption of heating chamber 3, and reduce production cost.

在蒸发结晶室4和加热室3之间设置循环加热,能对蒸发结晶室4中的含有微小晶体的料液进行重复蒸发,使得微小晶体能在循环过程中长成较大颗粒的晶体,方便回收,还能利用循环料液来调控整套KCl蒸发析盐生产装置的安全、稳定、高效的运行。Circular heating is set between the evaporation crystallization chamber 4 and the heating chamber 3, which can repeatedly evaporate the feed liquid containing tiny crystals in the evaporation crystallization chamber 4, so that the tiny crystals can grow into larger crystals during the circulation process, which is convenient Recycling can also use the circulating feed liquid to regulate the safe, stable and efficient operation of the entire KCl evaporation and salt production device.

如图2所示,具体的,加热室3的加热管的外壁间隙中设置有振动除垢机构,振动除垢机构包括多根贯穿加热室3的振动杆31,和,设置在多根振动杆31的两端的振动电机32;振动电机32设置在加热室3的外部。As shown in Figure 2, specifically, a vibration descaling mechanism is provided in the outer wall gap of the heating tube of the heating chamber 3, and the vibration descaling mechanism includes a plurality of vibrating rods 31 passing through the heating chamber 3, and is arranged on a plurality of vibrating rods Vibration motor 32 at two ends of 31; Vibration motor 32 is arranged on the outside of heating chamber 3.

需要说明的是,上述振动杆31的数量根据加热管的数量进行设置,本实用新型不做限制,可以在每列加热管的间隙中平行设置一根或多根振动杆31,也可以在几列加热管组成的加热管束的间隙中平行设置一根或多根振动杆31。It should be noted that the number of the above-mentioned vibrating rods 31 is set according to the number of heating tubes, the utility model is not limited, one or more vibrating rods 31 can be arranged in parallel in the gap of each row of heating tubes, or several One or more vibrating rods 31 are arranged in parallel in the gap of the heating tube bundle composed of rows of heating tubes.

在加热室3的加热管的间隙中设置振动除垢机构,其中振动电机32能控制振动杆31持续或间歇地进行振动,若加料量出现波动或加热室3温度控制过高而造成加热室3中料液过饱和并在加热管中析晶时,能及时将加热管内壁上的晶体进行振动驱除,提高加热管的洁净度,有效防止加热管内壁结垢堵塞,有利于提高加热室3的换热效率,延长加热管的使用时间,降低装置停运和疏通清洗加热管的频率,降低生产成本。A vibration descaling mechanism is set in the gap between the heating tubes of the heating chamber 3, wherein the vibration motor 32 can control the vibrating rod 31 to vibrate continuously or intermittently. When the medium feed liquid is supersaturated and crystallizes in the heating tube, the crystals on the inner wall of the heating tube can be vibrated and removed in time, the cleanliness of the heating tube can be improved, the scaling and blockage of the inner wall of the heating tube can be effectively prevented, and the efficiency of the heating chamber 3 can be improved. High heat exchange efficiency, prolonging the service time of the heating tube, reducing the frequency of device shutdown and dredging and cleaning the heating tube, and reducing production costs.

具体的,蒸发结晶室4的进料口设置在蒸发结晶室4的筒体的切线方向上,加热室3的顶部的物料出口通过管道与蒸发结晶室4形成切向连接。Specifically, the feed port of the evaporation crystallization chamber 4 is arranged in the tangential direction of the barrel of the evaporation crystallization chamber 4, and the material outlet at the top of the heating chamber 3 forms a tangential connection with the evaporation crystallization chamber 4 through a pipeline.

现有的蒸发结晶室4的进料口都竖直地伸入蒸发结晶室4的内部,在氯化钾结晶下落的过程中,很容易在内置的进料管和进料口上发生沉积而形成盐垢,大块盐垢脱落后容易造成输出管道的堵塞,不利于装置的稳定生产。在本实用新型中,蒸发结晶室4采用切向进料的方式,使得加热室3排出的饱和氯化钾料液沿筒体旋转进料,由于蒸发结晶室4的内部无阻碍,筒体内壁又不断被进料冲刷,因而在蒸发结晶室4中不易形成盐垢,水分大量蒸发后,方便了过饱和溶液在蒸发结晶室4的下部进行结晶,延长了装置的生产周期。The feed ports of the existing evaporative crystallization chamber 4 all extend vertically into the inside of the evaporative crystallization chamber 4, and during the process of the potassium chloride crystals falling, it is easy to deposit on the built-in feed pipe and the feed port to form Salt scale, after large pieces of salt scale fall off, it is easy to cause blockage of the output pipeline, which is not conducive to the stable production of the device. In the utility model, the evaporation and crystallization chamber 4 adopts a tangential feeding method, so that the saturated potassium chloride feed liquid discharged from the heating chamber 3 rotates and feeds along the cylinder body. It is continuously washed by the feed, so it is not easy to form salt scale in the evaporation crystallization chamber 4. After a large amount of water evaporates, it is convenient for the supersaturated solution to crystallize in the lower part of the evaporation crystallization chamber 4, prolonging the production cycle of the device.

如图3所示,具体的,蒸发结晶室4与集盐罐6之间还设置有压滤机7;压滤机7的进料口与蒸发结晶室4的底部的结晶体出口连接,压滤机7的母液出口与进料预热器2的物料入口连接,压滤机7的结晶出管与集盐罐6连接。As shown in Figure 3, specifically, a filter press 7 is also arranged between the evaporation crystallization chamber 4 and the salt collection tank 6; The mother liquor outlet of the machine 7 is connected with the material inlet of the feed preheater 2, and the crystallization outlet pipe of the filter press 7 is connected with the salt collecting tank 6.

加热后的料液在蒸发结晶室4中进行蒸发、结晶和分离,蒸发结晶室4的底部能生长和沉积颗粒大且均匀的氯化钾晶体,将该部分氯化钾晶体送入压滤机7中进行固液分离,能得到纯度较高、含水量低的氯化钾结晶产品,经压滤机7分离的母液送入进料预热器2中循环进行蒸发,能使得母液中残留的氯化钾再一次结晶回收,能最大限度地回收氯化钾。The heated feed liquid is evaporated, crystallized and separated in the evaporation crystallization chamber 4, and the bottom of the evaporation crystallization chamber 4 can grow and deposit large and uniform potassium chloride crystals, and send this part of potassium chloride crystals into the filter press Carry out solid-liquid separation in 7, can obtain the potassium chloride crystalline product with higher purity, low water content, send the mother liquor that separates through filter press 7 into feed preheater 2 and circulate and evaporate, can make residual in the mother liquor Potassium chloride is recrystallized again, can reclaim potassium chloride to the greatest extent.

具体的,蒸发结晶室4的蒸汽出口的下方还设置有除沫网板41,除沫网板41的上方还设置有防堵喷淋管42。Specifically, a defoaming screen 41 is provided below the steam outlet of the evaporation and crystallization chamber 4 , and an anti-blocking spray pipe 42 is provided above the defoaming screen 41 .

本实用新型中,将蒸发结晶室4产生的二次蒸汽用于进料预热,这是二次蒸汽的回收利用的一个示例,该部分二次蒸汽还能用于给其他工段的设备或物料进行加热,当其他设备对二次蒸汽的除沫要求较高时,在蒸发结晶室4中设置除沫网板41能进一步对二次蒸汽进行除沫和洁净,有利于二次蒸汽的再利用。由于该部分二次蒸汽在上升过程中可能夹带氯化钾晶体,长时间运行后,会在除沫网板41上发生沉积,为避免除沫网板41堵塞,在其上方设置防堵喷淋管42能及时对除沫网板41进行清洗和疏通,有利于延长装置的运行周期。In this utility model, the secondary steam generated by the evaporation and crystallization chamber 4 is used for feed preheating, which is an example of secondary steam recovery and utilization, and this part of secondary steam can also be used for equipment or materials in other sections Heating, when other equipment has high requirements on the defoaming of the secondary steam, setting the defoaming screen 41 in the evaporation crystallization chamber 4 can further defoam and clean the secondary steam, which is beneficial to the reuse of the secondary steam . Since this part of the secondary steam may entrain potassium chloride crystals during the rising process, after a long time of operation, deposition will occur on the defoaming net plate 41. In order to avoid the clogging of the defoaming net plate 41, an anti-blocking spray is set above it The pipe 42 can clean and dredge the defoaming screen 41 in time, which is beneficial to prolong the operating period of the device.

具体的,蒸发结晶室4的下部为倒锥形结构,锥度为45°-60°。将蒸发结晶室4的下部设置为倒锥形结构,与圆形结构相比,倒锥形结构能更好地利用重力作用将氯化钾结晶体进行粗细分层,大颗粒氯化钾结晶体沉积在底部,方便输往集盐罐6,微小颗粒的结晶体浮在上层,方便从循环料出口通过管道进行再循环,使得微小颗粒的结晶体能在再循环过程中长大,这样能获得晶体颗粒较大的氯化钾晶体产品。Specifically, the lower part of the evaporation and crystallization chamber 4 is an inverted cone structure with a taper of 45°-60°. The lower part of the evaporation crystallization chamber 4 is set as an inverted conical structure. Compared with the circular structure, the inverted conical structure can better use gravity to carry out coarse and subdivided potassium chloride crystals, and large grains of potassium chloride crystals are deposited on the The bottom is convenient to be transported to the salt collection tank 6, and the crystals of tiny particles float on the upper layer, which is convenient for recirculation from the outlet of the circulating material through the pipeline, so that the crystals of tiny particles can grow up during the recirculation process, so that larger crystal particles can be obtained Potassium chloride crystal product.

如图4所示,具体的,加热室3内设置有自动清垢结构,自动清垢结构包括弹簧支架33,弹簧34,限位卡板35和清洗螺旋钢丝36;弹簧34的一端与弹簧支架33固定连接,弹簧34的另一端与限位卡板35的一端固定连接,限位卡板35的另一端与清洗螺旋钢丝36的一端连接;弹簧支架33与加热室3的下部固定连接,且弹簧支架33设置在加热室3的进料口的上方;弹簧34和限位卡板35设置在加热室3的加热管的外部,清洗螺旋钢丝36伸入加热管的内部;弹簧34、限位卡板35和清洗螺旋钢丝36与加热管一一对应设置。As shown in Figure 4, specifically, the heating chamber 3 is provided with an automatic descaling structure, and the automatic descaling structure includes a spring support 33, a spring 34, a limit clamp 35 and a cleaning spiral steel wire 36; one end of the spring 34 is connected to the spring support 33 is fixedly connected, the other end of the spring 34 is fixedly connected with an end of the limit clamp 35, and the other end of the limit clamp 35 is connected with one end of the cleaning spiral steel wire 36; the spring support 33 is fixedly connected with the bottom of the heating chamber 3, and Spring support 33 is arranged on the top of the feeding port of heating chamber 3; Spring 34 and limit clip 35 are arranged on the outside of the heating pipe of heating chamber 3, and cleaning spiral steel wire 36 stretches into the inside of heating pipe; The clamping plate 35 and the cleaning spiral steel wire 36 are provided in one-to-one correspondence with the heating tubes.

自动清垢结构中的弹簧34能提供整个机构往复运动的动力,使得清洗螺旋钢丝36在加热管中做往复运动,限位卡板35则控制了清洗螺旋钢丝36的上升极限位置,清洗螺旋钢丝36在加热管中受料液流动影响向上运动,弹簧34自然伸长,当料液从加热管排出后,料液部分汽化泄压,清洗螺旋钢丝36会在弹簧34的拉力作用下向下复位,再循环往复运动。The spring 34 in the automatic cleaning structure can provide the power for the reciprocating movement of the whole mechanism, so that the cleaning spiral steel wire 36 reciprocates in the heating tube, and the limit clamp 35 controls the rising limit position of the cleaning spiral steel wire 36, and the cleaning spiral steel wire 36 moves upwards in the heating tube affected by the flow of the material liquid, and the spring 34 naturally elongates. When the material liquid is discharged from the heating tube, part of the material liquid vaporizes and releases pressure, and the cleaning spiral steel wire 36 will reset downward under the tension of the spring 34 , recirculating reciprocating motion.

清洗螺旋钢丝36的上下往复运动,在运动过程中,能将加热管内壁上沉积的盐垢剐蹭下来,避免盐垢沉积而堵塞加热管,除垢清洗能力强,延长了加热室3及整套装置的运行周期,在上下往复运动的过程中,还能加大加热管内料液的波动幅度,同时还能将沸腾蒸发形成的浮沫打散,通过清洗螺旋钢丝36的阻挡减速和搅动,有效增大了换热效率,强化了加热效果。The up and down reciprocating movement of the cleaning spiral steel wire 36 can scrape off the salt scale deposited on the inner wall of the heating tube during the movement, avoiding the blockage of the heating tube due to the deposition of salt scale, strong descaling and cleaning ability, and extending the length of the heating chamber 3 and the whole set of equipment In the process of reciprocating up and down, it can also increase the fluctuation range of the material liquid in the heating tube, and at the same time, it can also break up the foam formed by boiling and evaporation. By cleaning the spiral steel wire 36 to block deceleration and agitation, it can effectively increase the temperature. The heat exchange efficiency is increased, and the heating effect is strengthened.

具体的,限位卡板35与弹簧34相连的端部的宽度为加热管的外径的1.1-1.5倍,限位卡板35的长度为50-100mm。Specifically, the width of the end of the limiting clip 35 connected to the spring 34 is 1.1-1.5 times the outer diameter of the heating tube, and the length of the limiting clip 35 is 50-100 mm.

限位卡板35的作用是对清洗螺旋钢丝36的运动进行极限定位,用于防止清洗螺旋钢丝36随气流无限度上升,进而致使弹簧34因过度拉伸而形变损坏无法复原,限位卡板35的设置,避免了自动清垢结构因弹簧34变形而失去提供往复运动的动力,进而避免了清垢结构的自动清洗功能的丧失。The function of the limit clamp 35 is to limit the movement of the cleaning spiral steel wire 36, so as to prevent the cleaning spiral steel wire 36 from rising indefinitely with the air flow, thereby causing the spring 34 to be deformed and damaged due to excessive stretching and cannot be recovered. The setting of 35 prevents the automatic descaling structure from losing the power to provide reciprocating motion due to the deformation of the spring 34, thereby avoiding the loss of the automatic cleaning function of the descaling structure.

具体的,清洗螺旋钢丝36的长度比加热管的长度短200-500mm,清洗螺旋钢丝36的外径为加热管的内径的0.7-0.9倍。Specifically, the length of the cleaning spiral steel wire 36 is 200-500 mm shorter than that of the heating tube, and the outer diameter of the cleaning spiral steel wire 36 is 0.7-0.9 times the inner diameter of the heating tube.

KCl蒸发析盐生产装置,具体工作时,含有氯化钾的料液利用进料泵1送入进料预热器2中进行预热,预热后的料液进入加热室3,通过外源蒸汽加热汽化后变为汽水混合物。其中,料液在加热管中向上运动的同时,带动加热管中的清洗螺旋钢丝36也向上运动,与之连接的限位卡板35也随之运动,使得弹簧34自然伸长,当料液从加热管排出后,料液部分汽化泄压,清洗螺旋钢丝36会在弹簧34的拉力作用下向下复位,再循环往复运动,在往复运动过程中,清洗螺旋钢丝36能将加热管内壁上沉积的盐垢剐蹭下来,避免盐垢沉积而堵塞加热管,还能加大加热管内料液的波动幅度,同时还能将沸腾蒸发形成的浮沫打散,有效增大了换热效率,强化了加热效果。KCl evaporative salt production device, during specific work, the feed liquid containing potassium chloride is sent to the feed preheater 2 by the feed pump 1 for preheating, the preheated feed liquid enters the heating chamber 3, and is passed through an external source The steam turns into a soda-water mixture after being heated and vaporized. Wherein, when the feed liquid moves upward in the heating tube, it drives the cleaning spiral steel wire 36 in the heating tube to also move upward, and the limit clamp 35 connected therewith also moves accordingly, so that the spring 34 naturally elongates, and when the feed liquid After being discharged from the heating tube, part of the feed liquid is vaporized and released to release pressure, and the cleaning spiral steel wire 36 will reset downward under the tension of the spring 34, and recirculate and reciprocate. The deposited salt scale is rubbed off to avoid the blockage of the heating tube due to the deposition of salt scale, and it can also increase the fluctuation range of the material liquid in the heating tube, and at the same time, it can also break up the foam formed by boiling and evaporation, effectively increasing the heat transfer efficiency and strengthening heating effect.

当料液在加热室3中换热蒸发时,启动振动除垢机构,由振动电机32带动振动杆31进行持续或间歇地振动,若加料量出现波动或加热室3温度控制过高而造成加热室3中料液过饱和并在加热管中析晶时,能及时将加热管内壁上的晶体进行振动驱除,有效防止加热管内壁结垢堵塞,有利于提高加热室3的换热效率。When the feed liquid is heat-exchanged and evaporated in the heating chamber 3, the vibration descaling mechanism is started, and the vibration rod 31 is driven by the vibration motor 32 to vibrate continuously or intermittently. When the feed liquid in chamber 3 is supersaturated and crystallizes in the heating tube, the crystals on the inner wall of the heating tube can be vibrated and removed in time, effectively preventing the inner wall of the heating tube from fouling and clogging, and improving the heat exchange efficiency of the heating chamber 3.

上述汽水混合物通过管道切向进入蒸发结晶室4中,在蒸发结晶室4中进行蒸发和结晶分离。蒸发产生的二次蒸汽进入进料预热器2中作为加热介质使用,最终通过进料预热器2的加热介质出口通过冷水管道排往回收池。蒸发剩余的料液下落至蒸发结晶室4的下部进行结晶,并利用倒锥形结构的重力作用将氯化钾结晶体进行粗细分层,大颗粒氯化钾结晶体沉积在底部,通过结晶体出口输往集盐罐6;微小颗粒的结晶体混合未蒸发的水分浮在上层,从循环料出口通过循环泵5再次进入加热室3进行蒸发结晶,使得微小颗粒的结晶体能在再循环过程中长大,获得晶体颗粒较大的氯化钾晶体产品。The above steam-water mixture enters the evaporative crystallization chamber 4 tangentially through the pipeline, and evaporates and crystallizes and separates in the evaporative crystallization chamber 4 . The secondary steam generated by evaporation enters the feed preheater 2 and is used as a heating medium, and finally passes through the outlet of the heating medium of the feed preheater 2 and is discharged to the recovery pool through the cold water pipeline. The remaining material liquid after evaporation falls to the lower part of the evaporation and crystallization chamber 4 for crystallization, and the potassium chloride crystals are coarsely subdivided by the gravity of the inverted cone structure, and the large grains of potassium chloride crystals are deposited at the bottom, and are transported through the crystal outlet to Salt collection tank 6; the crystals of tiny particles are mixed with unevaporated water and float on the upper layer, and enter the heating chamber 3 again from the outlet of the circulating material through the circulation pump 5 for evaporation and crystallization, so that the crystals of tiny particles can grow up in the recirculation process and obtain Potassium chloride crystal product with larger crystal grains.

在另一个实施例中,上述汽水混合物通过管道切向进入蒸发结晶室4中,在蒸发结晶室4中进行蒸发和结晶分离。蒸发产生的二次蒸汽向上通过除沫网板41进行除沫后,从蒸发结晶室4的蒸汽出口进入进料预热器2中作为加热介质使用,最终通过进料预热器2的加热介质出口通过冷水管道排往回收池。除沫网板41上方的防堵喷淋管42定时向除沫网板41上喷淋蒸汽凝液或洁净水,及时对除沫网板41进行清洗和疏通,避免除沫网板41堵塞。蒸发剩余的料液下落至蒸发结晶室4的下部进行结晶,并利用倒锥形结构的重力作用将氯化钾结晶体进行粗细分层,大颗粒氯化钾结晶体沉积在底部,从蒸发结晶室4的结晶体出口先输往压滤机7,在压滤机7中进行固液分离后,纯度较高、含水量低的氯化钾结晶产品从压滤机7的结晶出管输往集盐罐6,经压滤机7分离的母液则送入进料预热器2中循环进行蒸发,能使得母液中残留的氯化钾再一次结晶回收,能最大限度地回收氯化钾。In another embodiment, the above steam-water mixture enters the evaporative crystallization chamber 4 tangentially through the pipeline, and evaporates and crystallizes and separates in the evaporative crystallization chamber 4 . The secondary steam generated by evaporation passes upward through the defoaming screen 41 for defoaming, then enters the feed preheater 2 from the steam outlet of the evaporation crystallization chamber 4 to be used as a heating medium, and finally passes through the heating medium of the feed preheater 2 The outlet drains to a recovery tank through a cold water pipe. The anti-blocking spray pipe 42 above the defoaming screen 41 regularly sprays steam condensate or clean water on the defoaming screen 41, and cleans and dredges the defoaming screen 41 in time to prevent the defoaming screen 41 from clogging. The remaining material liquid after evaporation falls to the lower part of the evaporation crystallization chamber 4 for crystallization, and the potassium chloride crystals are coarsely subdivided by the gravity of the inverted cone structure, and the large particle potassium chloride crystals are deposited on the bottom, and the crystallization is carried out from the evaporation crystallization chamber 4 The crystal outlet of the crystal is first transported to the filter press 7, and after the solid-liquid separation is carried out in the filter press 7, the potassium chloride crystallization product with higher purity and low water content is transported to the salt collection tank from the crystallization outlet pipe of the filter press 7 6. The mother liquor separated by the filter press 7 is sent to the feed preheater 2 to circulate and evaporate, so that the residual potassium chloride in the mother liquor can be crystallized and recovered again, and the potassium chloride can be recovered to the maximum extent.

需要说明的是,在本实用新型中,部分设备的详细结构并未详述,但属于本领域技术人员已知的现有技术,故在此不再赘述。It should be noted that, in this utility model, the detailed structure of some devices is not described in detail, but it belongs to the prior art known to those skilled in the art, so it will not be repeated here.

需要说明的是,系统内部的输送管道上在不同单元或装置、设备间设置有压力传感器、流量计或温度传感器,同时也设置有不同阀门,如泄压阀、调压阀、安全阀等用于调节和稳定整个系统压力的阀门。It should be noted that the conveying pipeline inside the system is provided with pressure sensors, flow meters or temperature sensors between different units or devices and equipment, and is also provided with different valves, such as pressure relief valves, pressure regulating valves, safety valves, etc. Valves used to regulate and stabilize the pressure of the entire system.

需要说明的是,本领域技术人员在本实用新型的指导下,还能对上述系统做出部分修改设计。例如,系统内的设备上还设置有液位计、溢流/氮气管道等;系统内部的输送管道上在不同单元或装置、设备间设置有泵、压力传感器、流量计或温度传感器等,同时也设置有不同阀门,如泄压阀、调压阀、安全阀、气动阀等用于调节和稳定整个系统压力的阀门,也可调节阀门的开度以调节管道内物料流量等。It should be noted that those skilled in the art can make some modifications to the above system under the guidance of the utility model. For example, liquid level gauges, overflow/nitrogen pipelines, etc. are installed on the equipment in the system; pumps, pressure sensors, flow meters, or temperature sensors, etc. are installed between different units or devices and equipment on the delivery pipelines inside the system. There are also different valves, such as pressure relief valves, pressure regulating valves, safety valves, pneumatic valves, etc., which are used to adjust and stabilize the pressure of the entire system. The opening of the valve can also be adjusted to adjust the flow of materials in the pipeline.

最后应说明的是,以上各实施例仅用以说明本实用新型的技术方案,而非对其限制;尽管参照前述各实施例对本实用新型进行了详细的说明,本领域的普通技术人员应当理解;其依然可以对前述各实施例所记载的技术方案进行修改,或者对其中部分或者全部技术特征进行等同替换;而这些修改或者替换,并不使相应技术方案的本质脱离本实用新型各实施例技术方案的范围。Finally, it should be noted that the above embodiments are only used to illustrate the technical solution of the present utility model, rather than limit it; although the utility model has been described in detail with reference to the foregoing embodiments, those of ordinary skill in the art should understand It can still modify the technical solutions described in the foregoing embodiments, or perform equivalent replacements to some or all of the technical features; and these modifications or replacements do not make the essence of the corresponding technical solutions depart from the various embodiments of the present invention Scope of technical solutions.

Claims (8)

1. A KCl evaporation salting production device is characterized by comprising: the system comprises a feed pump, a feed preheater, a heating chamber, an evaporation crystallization chamber, a circulating pump and a salt collecting tank;
the feeding pump, the feeding preheater and the feeding port at the lower part of the heating chamber are sequentially connected through a feeding pipeline, and a material outlet at the top of the heating chamber is connected with the feeding port of the evaporative crystallization chamber;
a steam outlet at the top of the evaporative crystallization chamber is connected with a heating medium inlet of the feed preheater, a crystal outlet at the bottom of the evaporative crystallization chamber is connected with the salt collecting tank, and a circulating material outlet at the lower part of the evaporative crystallization chamber is connected with an inlet of the circulating pump; the outlet of the circulating pump is connected with the feed inlet of the heating chamber; a heating medium outlet of the feeding preheater is discharged to a recovery tank through a cold water pipeline;
a vibration descaling mechanism is arranged in a gap between the outer walls of the heating pipes of the heating chamber, and comprises a plurality of vibrating rods penetrating through the heating chamber and vibrating motors arranged at two ends of the vibrating rods; the vibration motor is disposed outside the heating chamber.
2. The KCl evaporative salt-separating production device of claim 1, wherein the feed inlet of the evaporative crystallization chamber is arranged in the tangential direction of the barrel of the evaporative crystallization chamber, and the material outlet at the top of the heating chamber is tangentially connected with the evaporative crystallization chamber through a pipeline.
3. The KCl evaporative salt-separating production device according to claim 1, wherein a filter press is further arranged between the evaporative crystallization chamber and the salt collecting tank; the feed inlet of the filter press is connected with a crystal outlet at the bottom of the evaporation crystallization chamber, a mother liquid outlet of the filter press is connected with a material inlet of the feed preheater, and a crystallization outlet pipe of the filter press is connected with the salt collecting tank.
4. The KCl evaporative salt-separating production device according to claim 1, wherein a defoaming screen plate is further arranged below the steam outlet of the evaporative crystallization chamber, and an anti-blocking spray pipe is further arranged above the defoaming screen plate.
5. The KCl evaporative salt deposition production device according to claim 1, wherein the lower part of the evaporative crystallization chamber has an inverted conical structure, and the conicity is 45-60 °.
6. The KCl evaporative salting production device according to any one of claims 1 to 5, wherein an automatic scale cleaning structure is arranged in the heating chamber, and the automatic scale cleaning structure comprises a spring bracket, a spring, a limiting clamping plate and a cleaning spiral steel wire;
one end of the spring is fixedly connected with the spring support, the other end of the spring is fixedly connected with one end of the limiting clamping plate, and the other end of the limiting clamping plate is connected with one end of the cleaning spiral steel wire;
the spring support is fixedly connected with the lower part of the heating chamber and is arranged above the feeding hole of the heating chamber;
the spring and the limiting clamping plate are arranged outside the heating pipe of the heating chamber, and the cleaning spiral steel wire extends into the heating pipe; the spring, the limiting clamping plate and the cleaning spiral steel wire are arranged in one-to-one correspondence with the heating pipes.
7. The KCl evaporative salt deposition apparatus according to claim 6, wherein the width of the end of the limiting catch plate connected to the spring is 1.1-1.5 times the outer diameter of the heating tube, and the length of the limiting catch plate is 50-100mm.
8. The KCl evaporative salting production apparatus according to claim 6, wherein the cleaning spiral wire has a length 200-500mm shorter than the heating tube, and an outer diameter 0.7-0.9 times an inner diameter of the heating tube.
CN202222426342.2U 2022-09-13 2022-09-13 KCl evaporating salt production device Active CN218107679U (en)

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Date Code Title Description
GR01 Patent grant
GR01 Patent grant
PE01 Entry into force of the registration of the contract for pledge of patent right
PE01 Entry into force of the registration of the contract for pledge of patent right

Denomination of utility model: KCl evaporation and salt precipitation production equipment

Granted publication date: 20221223

Pledgee: Bank of China Limited BAYANHOT branch

Pledgor: Inner Mongolia Kunpeng New Material Co.,Ltd.

Registration number: Y2025980003149