CN218077897U - Nickel-glycine dissolves support for experiments - Google Patents
Nickel-glycine dissolves support for experiments Download PDFInfo
- Publication number
- CN218077897U CN218077897U CN202222093811.3U CN202222093811U CN218077897U CN 218077897 U CN218077897 U CN 218077897U CN 202222093811 U CN202222093811 U CN 202222093811U CN 218077897 U CN218077897 U CN 218077897U
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- Prior art keywords
- backup pad
- nickel
- main shaft
- section
- glycine
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- 238000002474 experimental method Methods 0.000 title claims abstract description 11
- HJPJOAYWRKTHED-UHFFFAOYSA-N 2-aminoacetic acid;nickel Chemical compound [Ni].NCC(O)=O HJPJOAYWRKTHED-UHFFFAOYSA-N 0.000 title description 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims abstract description 68
- 229910052759 nickel Inorganic materials 0.000 claims abstract description 34
- 235000010627 Phaseolus vulgaris Nutrition 0.000 claims abstract description 31
- 244000046052 Phaseolus vulgaris Species 0.000 claims abstract description 31
- 238000003756 stirring Methods 0.000 claims abstract description 21
- 238000006243 chemical reaction Methods 0.000 claims abstract description 19
- 238000001914 filtration Methods 0.000 claims abstract description 10
- 230000006978 adaptation Effects 0.000 claims abstract description 7
- 239000011148 porous material Substances 0.000 claims abstract description 7
- 238000009434 installation Methods 0.000 claims description 23
- 239000002253 acid Substances 0.000 claims description 10
- 230000002093 peripheral effect Effects 0.000 claims description 3
- 239000012530 fluid Substances 0.000 abstract description 17
- 238000002360 preparation method Methods 0.000 abstract description 2
- 238000004090 dissolution Methods 0.000 description 5
- 238000000034 method Methods 0.000 description 4
- LGQLOGILCSXPEA-UHFFFAOYSA-L nickel sulfate Chemical compound [Ni+2].[O-]S([O-])(=O)=O LGQLOGILCSXPEA-UHFFFAOYSA-L 0.000 description 4
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 3
- 229910000363 nickel(II) sulfate Inorganic materials 0.000 description 3
- 230000000694 effects Effects 0.000 description 2
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- -1 polyethylene Polymers 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 235000011149 sulphuric acid Nutrition 0.000 description 1
- 239000001117 sulphuric acid Substances 0.000 description 1
Images
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- Mixers Of The Rotary Stirring Type (AREA)
Abstract
The utility model belongs to preparation nickel beans solution experimental device field, concretely relates to nickel beans acid-soluble support for experiments, including setting up the backup pad in reaction vessel, the backup pad with the reaction vessel adaptation, the bottom of backup pad is supported through a plurality of bracing pieces, the below of backup pad is provided with the stirring leaf, backup pad top fixed connection sleeve pipe, the intraductal connection that is provided with of cover the main shaft of stirring leaf, the main shaft is connected with drive arrangement, set up a plurality of first filtration pores in the backup pad, compare prior art, the utility model provides the mobility of acidizing fluid has been improved, fully contacts with nickel beans for nickel beans acid-soluble speed.
Description
Technical Field
The utility model belongs to preparation nickel beans solution experimental device field, concretely relates to structurally improved of nickel beans acid-soluble support for experiments.
Background
With the continuous rise of new energy power battery industry, the nickel-soyate dissolution to prepare nickel sulfate solution becomes an effective way to prepare nickel sulfate salt. In the experimental process of preparing the nickel sulfate solution by dissolving nickel soyate, the nickel soyate is directly put into the acid solution for soaking, and the phenomenon of too low dissolution rate exists. If adopt the stirring mode improper, the nickel beans produce the motion, and the relative motion that produces between nickel beans and the acidizing fluid is little, can't effectively promote nickel beans acid dissolution rate to the nickel beans motion can directly lead to the beaker damaged, for accelerating nickel beans acid dissolution rate, proposes the utility model discloses a suitable mixing type is suitable for the industry.
SUMMERY OF THE UTILITY MODEL
The utility model aims at providing a nickel beans acid dissolves support for experiments to solve the problem that exists among the prior art.
In order to realize the purpose of the utility model, the utility model adopts the technical proposal that:
the utility model provides an experiment is with nickel beans acid-soluble support, is including setting up the backup pad in reaction vessel, the backup pad with the reaction vessel adaptation, the bottom of backup pad is supported through a plurality of bracing pieces, the below of backup pad is provided with the stirring leaf, backup pad top fixed connection sleeve pipe, the intraductal connection that is provided with of cover the main shaft of stirring leaf, the main shaft is connected with drive arrangement, set up a plurality of first filtration pores in the backup pad.
Furthermore, the sleeve pipe is including setting up the major diameter section in the lower part, main shaft bottom extends the major diameter section, and fixed connection the stirring leaf, the main shaft be global with have the space between the medial surface of major diameter section, the major diameter section is global to set up a plurality of second filtration pores.
Further, the sleeve pipe is including setting up the installation section on upper portion, the bottom of installation section sets up the path section, the internal diameter of path section is less than the internal diameter of installation section, drive arrangement sets up in the installation section, the fixed spacing portion that sets up of global of main shaft, spacing position in the installation section, and the butt installation section bottom.
Furthermore, the driving device is arranged at the bottom of the cover plate and arranged in the sleeve, and the cover plate is detachably connected with the top opening of the sleeve.
Furthermore, the top of the cover plate is fixedly connected with a holding rod, a holding part is arranged on the peripheral surface of the holding rod, and the holding part is positioned above the reaction vessel.
Furthermore, the holding rod is provided with a cavity, and a battery connected with the driving device is arranged in the cavity.
Further, the driving device is a motor.
The utility model discloses following beneficial effect has: backup pad level sets up, is divided into two upper and lower cavities with reaction vessel, and its upper chamber is used for placing the nickel beans, and lower cavity separates the acidizing fluid, and drive stirring She Huansu stirs the acidizing fluid to dissolve the nickel beans, at the in-process that acid dissolves, the nickel beans remain relatively motionless, and the acidizing fluid is rotatory, then produces relative motion between acidizing fluid and the nickel beans, makes acidizing fluid and nickel beans fully contact, compares prior art, the utility model provides the mobility of acidizing fluid has improved the fully contact of acidizing fluid with the nickel beans for the acid dissolution rate of nickel beans.
Drawings
Fig. 1 is a schematic view of the overall structure of the present invention;
fig. 2 is a schematic view of the connection relationship of the driving device.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings 1-2 in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Unless otherwise specified, the technical means used in the examples are conventional means well known to those skilled in the art.
In the description of the present invention, it is to be understood that the terms "longitudinal", "lateral", "up", "down", "front", "back", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outer", and the like indicate orientations or positional relationships based on those shown in the drawings, and are merely for convenience of description of the present invention, and do not indicate or imply that the device or element so referred to must have a particular orientation, be constructed and operated in a particular orientation, and therefore, should not be construed as limiting the present invention.
Fig. 1 and 2 show an experimental nickel-glycine-soluble support, which comprises a supporting plate 2 arranged in a reaction vessel 1, wherein the supporting plate 2 is adapted to the reaction vessel 1, the bottom of the supporting plate 2 is supported by a plurality of supporting rods 9, a stirring blade 8 is arranged below the supporting plate 2, the top of the supporting plate 2 is fixedly connected with a sleeve, a main shaft 6 connected with the stirring blade 8 is arranged in the sleeve, the main shaft 6 is connected with a driving device, and a plurality of first filtering holes are formed in the supporting plate 2.
The reaction container 1 is the prior art, as the container of preparing nickel sulfate solution in the experiment, can be beaker etc., backup pad 2 level sets up, it and reaction container 1's internal diameter adaptation, divide reaction container 1 into two upper and lower cavities, its upper chamber is used for placing the nickel beans, under the filtering action of first filtration pore, its lower cavity separates the acidizing fluid, the acidizing fluid is sulphuric acid, bracing piece 9 plays the supporting role, it is provided with a plurality ofly around the circumference of backup pad 2, drive arrangement then is used for driving main shaft 6 rotatory, thereby make stirring vane 8 stir the acidizing fluid.
During concrete implementation, place in reaction vessel 1 with backup pad 2 earlier, then put into nickel beans to backup pad 2's top, later slowly pour into solution, at last actuating drive arrangement restarts, drive stirring leaf 8 slow stirring acidizing fluid to dissolve nickel beans, at the in-process of acid-soluble, nickel beans remain motionless relatively, and the acidizing fluid is rotatory, then produces relative motion between acidizing fluid and the nickel beans, makes acidizing fluid and nickel beans fully contact, compares prior art, the utility model provides the mobility of acidizing fluid has been improved, and nickel beans fully contacts for nickel beans acid-soluble speed has been accelerated.
In addition, the sleeve, the support plate 2, the stirring blades 8, the main shaft 6 and the support rod 9 are made of a material that does not react with sulfuric acid, such as glass, ceramic, silicate, plastic (polyethylene), etc., and the driving means is installed on the top of the sleeve, which extends out of the reaction vessel 1, and the height of the driving means is much higher than that of the top of the reaction vessel 1.
Further, the sleeve pipe is including setting up big footpath section 3 in the lower part, 6 bottom extensions of main shaft big footpath section 3, and fixed connection stirring leaf 8, main shaft 6 global with have the space between the medial surface of big footpath section 3, 3 global setting a plurality of second filtration pores of big footpath section.
Specifically, the sleeve is arranged coaxially with the main shaft 6, the inner diameter of the large-diameter section 3 is larger than that of the main shaft 6, a gap is formed between the large-diameter section and the peripheral surface of the main shaft 6, centrifugal force is generated in the rotating process of the stirring blade 8, acid liquor is pushed to pass through the gap between the nickel beans and move downwards along the large-diameter section 3 through the second filtering holes, and the flowability of the acid liquor is further improved and the acid liquor is fully contacted with the nickel beans.
Further, the sleeve pipe is including setting up installation section 4 on upper portion, the bottom of installation section 4 sets up path section 5, path section 5's internal diameter is less than the internal diameter of installation section 4, drive arrangement sets up in installation section 4, the fixed spacing portion 16 that sets up of main shaft 6 global, spacing portion 16 is located in installation section 4, and the butt installation section 4 bottom.
Specifically, the sleeve pipe includes installation section 4, path section 5 and major diameter section 3 from top to bottom in proper order, and the internal diameter of path section 5 is less than major diameter section 3 and installation section 4, and with main shaft 6 adaptation, spacing portion 16 is the ring structure, and fixed cover is established on main shaft 6, forms limit structure with the cooperation of installation section 4, plays the effect of supporting main shaft 6, can set up footstep bearing between the bottom of spacing portion 16 and installation section 4 to improve rotation performance.
Further, the driving device is installed at the bottom of the cover plate 11 and is arranged in the sleeve, and the cover plate 11 is detachably connected with the top opening of the sleeve.
In particular, the cover plate 11 may be connected to the top of the sleeve, i.e. the top of the mounting section 4, by means of screws, threads or the like.
Further, the top of the cover plate 11 is fixedly connected with a holding rod 10, a holding part 12 is arranged on the circumferential surface of the holding rod 10, and the holding part 12 is located above the reaction vessel 1.
Specifically, the holding portion 12 can be in the form of a ripple, friction line, wave portion, etc., and is convenient for a worker to hold the holding portion during an experiment, and the cover plate 11 and the driving device can be taken down by the holding rod 10, so that the purpose of convenient installation and disassembly is achieved.
During the concrete implementation, the staff holds the portion of gripping 12, with whole support downstream, makes backup pad 2 slide down to the reaction vessel 1 in, after the experiment, whole support has been taken out to accessible portion of gripping 12, has played the purpose of being convenient for place, take out the experiment support.
Further, the holding rod 10 is provided with a cavity, and a battery 13 connected with the driving device is arranged in the cavity.
Further, the driving device is a motor 7.
The battery 13 supplies power to the motor 7, specifically, the motor 7 is a miniature and small-sized motor, and can be a speed reduction motor, and drives the stirring blade 8 to rotate at a slow speed, the battery 13 is prior art, and can be a storage battery, and is connected with the motor 7 through a wire, and wire holes 15 for the wire to pass through are arranged on the bottom of the holding rod 10 and the cover plate 11, so as to be used for the wire to pass through and be connected to the motor 7.
In addition, the side fixed connection arch 14 of the axis of rotation of motor 7, the top of main shaft 6 is provided with the blind hole, blind hole and axis of rotation adaptation, the blind hole medial surface be provided with the spacing groove of protruding 14 adaptations, during the concrete implementation, the axis of rotation of motor 7 inserts in the blind hole down to make protruding 14 and spacing groove cooperation, thereby form the restraint in the circumference of main shaft 6, and still have the effect of being convenient for connect main shaft 6 and dismantling motor 7.
The above-mentioned embodiments are only for describing the preferred embodiments of the present invention, and are not intended to limit the scope of the present invention, and various changes, modifications, amendments, and substitutions made by the technical solutions of the present invention by those skilled in the art should fall within the protection scope defined by the claims of the present invention without departing from the design spirit of the present invention.
Claims (7)
1. The utility model provides a nickel beans acid dissolves support for experiments which characterized in that: including setting up backup pad (2) in reaction vessel (1), backup pad (2) with reaction vessel (1) adaptation, the bottom of backup pad (2) is supported through a plurality of bracing pieces (9), the below of backup pad (2) is provided with stirring leaf (8), backup pad (2) top fixed connection sleeve pipe, the intraductal connection that is provided with of cover main shaft (6) of stirring leaf (8), main shaft (6) are connected with drive arrangement, set up a plurality of first filtration pores on backup pad (2).
2. The experimental nickel coumaric acid-soluble scaffold as claimed in claim 1, wherein: the sleeve pipe is including setting up major diameter section (3) in the lower part, main shaft (6) bottom extends major diameter section (3), and fixed connection stirring leaf (8), the global of main shaft (6) with have the space between the medial surface of major diameter section (3), a plurality of second filtration pores are set up on the global of major diameter section (3).
3. The experimental nickel-glycine-soluble scaffold as claimed in claim 1, wherein: the sleeve pipe is including setting up in installation section (4) on upper portion, the bottom of installation section (4) sets up path section (5), the internal diameter of path section (5) is less than the internal diameter of installation section (4), drive arrangement sets up in installation section (4), the fixed spacing portion (16) that sets up of global of main shaft (6), spacing portion (16) are located in installation section (4), and the butt installation section (4) bottom.
4. The experimental nickel-glycine-soluble scaffold as claimed in claim 1, wherein: the driving device is installed at the bottom of the cover plate (11) and arranged in the sleeve, and the cover plate (11) is detachably connected with the top opening of the sleeve.
5. The experimental nickel-glycine-soluble scaffold as claimed in claim 4, wherein: the top of the cover plate (11) is fixedly connected with a holding rod (10), a holding part (12) is arranged on the peripheral surface of the holding rod (10), and the holding part (12) is positioned above the reaction container (1).
6. The experimental nickel-glycine-soluble scaffold as claimed in claim 5, wherein: the holding rod (10) is provided with a cavity, and a battery (13) connected with the driving device is arranged in the cavity.
7. The experimental nickel-glycine-soluble scaffold as claimed in claim 1, wherein: the driving device is a motor (7).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202222093811.3U CN218077897U (en) | 2022-08-10 | 2022-08-10 | Nickel-glycine dissolves support for experiments |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202222093811.3U CN218077897U (en) | 2022-08-10 | 2022-08-10 | Nickel-glycine dissolves support for experiments |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN218077897U true CN218077897U (en) | 2022-12-20 |
Family
ID=84486549
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202222093811.3U Active CN218077897U (en) | 2022-08-10 | 2022-08-10 | Nickel-glycine dissolves support for experiments |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN218077897U (en) |
-
2022
- 2022-08-10 CN CN202222093811.3U patent/CN218077897U/en active Active
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20240220 Address after: 737100 No. 2 Lanzhou Road, Beijing Road Street, Jinchuan District, Jinchang City, Gansu Province Patentee after: Jinchuan Group Nickel Cobalt Co.,Ltd. Country or region after: China Address before: 737199 Beijing Road, Jinchuan District, Jinchang City, Gansu Province Patentee before: JINCHUAN GROUP Co.,Ltd. Country or region before: China |
|
| TR01 | Transfer of patent right |