CN218011198U - Traditional chinese medicine extract retreatment chromatography ware - Google Patents

Traditional chinese medicine extract retreatment chromatography ware Download PDF

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CN218011198U
CN218011198U CN202222226342.8U CN202222226342U CN218011198U CN 218011198 U CN218011198 U CN 218011198U CN 202222226342 U CN202222226342 U CN 202222226342U CN 218011198 U CN218011198 U CN 218011198U
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chromatography
tube
test
bottom plate
chinese medicine
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CN202222226342.8U
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陈晓双
陈勇
沈超
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West China Hospital of Sichuan University
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West China Hospital of Sichuan University
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Abstract

The utility model discloses a traditional Chinese medicine extract reprocessing chromatographic device, which comprises a bottom plate, a supporting mechanism and a chromatographic mechanism, wherein the supporting mechanism and the chromatographic mechanism are arranged above the bottom plate and are pivoted, and the chromatographic mechanism can rotate relative to the supporting mechanism; the chromatography mechanism comprises a chromatography tube, a conical tube and a hose, the chromatography tube, the conical tube and the hose are communicated with each other, the upper end of the chromatography tube is provided with a funnel, and the lower end of the chromatography tube is provided with a valve; one side of bottom plate top is equipped with placement machine and constructs, and placement machine constructs including carousel and test-tube rack and axostylus axostyle, and the carousel passes through the axostylus axostyle to rotate mutually with the bottom plate to be connected, and the test-tube rack comprises the clamp ring that a plurality of groups internal diameter of a solid fixed ring differ. The utility model discloses at the in-process that uses, can effectually avoid appearing the phenomenon that a small amount of samples adopted big test tube to lead to single test tube to collect a plurality of samples, a large amount of samples adopt the small test tube to promote work load again greatly, be favorable to reducing user's complex operation degree, promote traditional chinese medicine extract's chromatography efficiency.

Description

Traditional chinese medicine extract retreatment chromatography ware
Technical Field
The utility model relates to a chromatography apparatus technical field of traditional chinese medicine extract product especially relates to a traditional chinese medicine extract product retreatment chromatography ware.
Background
The adsorption column chromatography is a method for separating each component by utilizing different adsorption forces of adsorbents on different substances, the effective components in the traditional Chinese medicinal materials have obvious physiological activity and pharmacological action, wherein the application of polysaccharide, alkaloid, flavone and the like is the most extensive, but the effective components of the traditional Chinese medicinal materials are complex, low in content and more in impurities, and the extract obtained by the conventional extraction method is still a mixture and needs to be further separated and purified. The column chromatography technology is to make use of the differences of physicochemical properties of the material, such as molecular shape, size, charged state, solubility, adsorption capacity, distribution coefficient, molecular polarity and affinity, etc., to distribute the components in the mixture in the stationary phase and the mobile phase in different degrees, so as to gradually separate the components. The method has the advantages of high separation efficiency, wide application range, strong parameter selectivity of separation conditions, mild operation conditions and the like, and is widely applied to separation and purification of metabolites such as polysaccharide, alkaloid, flavone, enzyme, pigment, glycoside and the like and biomacromolecules.
Traditional chinese medicine extract's column chromatography is in operation process, when carrying out the collection of sample, collects the test tube and adopts the test tube of the equal specification of standard basically, if the phenomenon that a plurality of samples were collected to single test tube appears promptly in the big test tube of small sample adoption, a large amount of samples adopt the small test tube to promote the work load again greatly, and the sample collection is too loaded down with trivial details, needs frequently to collect the test tube and take, put down. Therefore, we propose a traditional Chinese medicine extract reprocessing dialyzer.
SUMMERY OF THE UTILITY MODEL
The utility model aims at solving the defects in the prior art and providing a Chinese medicine extract reprocessing chromatographic device.
In order to realize the purpose, the utility model adopts the following technical scheme:
a Chinese medicinal extract reprocessing chromatographic apparatus comprises a bottom plate, a supporting mechanism and a chromatography mechanism which are arranged above the bottom plate, wherein the supporting mechanism is pivoted with the chromatography mechanism, and the chromatography mechanism can rotate relative to the supporting mechanism; the chromatography mechanism comprises a chromatography tube, a conical tube and a hose, the chromatography tube, the conical tube and the hose are communicated with each other, a funnel is arranged at the upper end of the chromatography tube, and a valve is arranged at the lower end of the chromatography tube; one side of bottom plate top is equipped with placement mechanism, placement mechanism is including carousel and test-tube rack and axostylus axostyle, the carousel passes through the axostylus axostyle and is connected with the bottom plate is rotated mutually, the test-tube rack comprises the clamp ring that a plurality of groups internal diameter of a solid fixed ring differ, one of them the clamp ring on the test-tube rack is located chromatographic mechanism under, the test-tube rack is inserted through the clamp ring and is equipped with the collection test tube, the collection test tube comprises the standard test tube of the different specifications of a plurality of.
Preferably, the supporting mechanism comprises a bottom rod and a top rod, wherein a plurality of rods are connected between the bottom rod and the top rod, and one end of a protrusion on each rod faces outwards.
Preferably, the carousel upper end is the opening form, the heelpiece is installed to the inside bottom of carousel, test-tube rack fixed mounting is in the upper end of carousel inner wall, the indent has been seted up to the clip ring that the heelpiece corresponds on the test-tube rack.
Preferably, a supporting rod and a rotating rod are installed at the upper end of the outer portion of the chromatography tube, a fastening mechanism is arranged on one side, close to the supporting mechanism, of the chromatography mechanism, and the chromatography tube is rotatably connected with the fastening mechanism through the rotating rod.
Preferably, fastening device comprises bolt, the lantern ring and fixed plate, fastening device locates outside the supporting mechanism and accomplishes the locking by the bolt through the lantern ring cover, the change is installed to one side of fastening device, the change rotates with the bull stick mutually and is connected.
Preferably, the ultraviolet lamp is fixedly installed in the middle of the upper surface of the base pad and coaxially rotates with the turntable.
Preferably, a plurality of anti-skidding convex strips are arranged at the upper end of the outer ring surface of the turntable.
The utility model provides a traditional chinese medicine extract retreats decanter, beneficial effect lies in:
1. because the sample amount is different, the collection test tubes of the extract components to be collected are pre-arranged in a one-to-one correspondence manner on the test tube rack according to the size of the collection test tubes, after the previous extract component is collected, the next collection test tube on the test tube rack is shifted and corresponds to the hose again by rotating the turntable, and therefore the phenomenon that a single test tube collects a plurality of samples due to the fact that a small amount of samples adopt large test tubes, and the workload is greatly increased due to the fact that a large amount of samples adopt small test tubes is avoided;
2. and need not collect taking of test tube and stably place again, be favorable to reducing user's complex operation degree, promote the chromatography efficiency of traditional chinese medicine extract product.
Drawings
FIG. 1 is a schematic view of a chromatography device for reprocessing Chinese herb extracts according to the present invention;
FIG. 2 is a schematic view showing a disassembled mounting structure of a chromatography mechanism of a Chinese herb extract reprocessing chromatography device of the present invention;
FIG. 3 is a schematic view of a placing mechanism of a collecting test tube of a Chinese herb extract reprocessing dialyzer in accordance with the present invention;
FIG. 4 is a side view of a Chinese herb extract reprocessing decanter of the present invention;
FIG. 5 is a top view of a Chinese herb extract reprocessing dialyzer in accordance with the present invention.
In the figure: 1. a base plate;
2. a placement mechanism; 21. a shaft lever; 22. a turntable; 23. anti-slip raised lines; 24. an ultraviolet lamp; 25. a test tube rack; 26. a recessed groove; 27. collecting the test tubes; 28. a bottom pad;
3. a chromatography mechanism; 31. a funnel; 32. a chromatography tube; 33. a valve; 34. a tapered tube; 35. a hose; 36. a strut; 37. a rotating rod; 38. a fastening mechanism; 39. rotating the ring;
4. a support mechanism; 41. a bottom bar; 42. a rod shaped like a Chinese character 'ji'; 43. and a push rod.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments.
In the description of the present invention, it is to be understood that the terms "upper", "lower", "front", "rear", "left", "right", "top", "bottom", "inner", "outer", and the like indicate orientations or positional relationships based on the orientations or positional relationships shown in the drawings, and are only for convenience of description and simplicity of description, and do not indicate or imply that the device or element being referred to must have a particular orientation, be constructed and operated in a particular orientation, and therefore, should not be construed as limiting the present invention.
Referring to fig. 1-5, a Chinese medicine extract reprocessing chromatographic apparatus comprises a bottom plate 1, a supporting mechanism 4 and a chromatographic mechanism 3 arranged above the bottom plate 1, wherein the supporting mechanism 4 is pivoted with the chromatographic mechanism 3, and the chromatographic mechanism 3 can rotate relative to the supporting mechanism 4; the chromatography mechanism 3 comprises a chromatography tube 32, a conical tube 34 and a hose 35, the chromatography tube 32, the conical tube 34 and the hose 35 are communicated, the upper end of the chromatography tube 32 is provided with a funnel 31, and the lower end of the chromatography tube 32 is provided with a valve 33; one side of 1 top of bottom plate is equipped with placement mechanism 2, placement mechanism 2 is including carousel 22 and test-tube rack 25 and axostylus axostyle 21, a plurality of anti-skidding sand grips 23 are installed to the upper end of the outer anchor ring of carousel 22, carousel 22 rotates with bottom plate 1 through axostylus axostyle 21 mutually and is connected, test-tube rack 25 comprises the clamp ring that a plurality of solid fixed ring group internal diameters differ, clamp ring on one of them test-tube rack 25 is located chromatographic mechanism 3 under, test-tube rack 25 is inserted through the clamp ring and is equipped with collection test tube 27, it comprises the standard test tube of the different specifications of a plurality of to collect test tube 27.
The supporting mechanism 4 comprises a bottom rod 41 and a top rod 43, wherein a plurality of character rods 42 are connected between the bottom rod 41 and the top rod 43, one end of each protrusion on each character rod 42 faces outwards, interference caused by the bottom rod 41 and the top rod 43 on the supporting mechanism 4 in the rotating process of the turntable 22 is avoided, and a supporting effect is achieved.
Carousel 22 upper end is the opening form, the heelpiece 28 is installed to the inside bottom of carousel 22, test-tube rack 25 fixed mounting is in the upper end of carousel 22 inner wall, the indent 26 has been seted up to the clamp ring that heelpiece 28 corresponds on the test-tube rack 25, the middle part fixed mounting of heelpiece 28 upper surface has purple light lamp 24, purple light lamp 24 and carousel 22 coaxial rotation, setting through purple light lamp 24, purple light lamp 24 aligns with chromatography tube 23, during the chromatography, shine chromatography tube 23 can be clear observe inside chromatography product position through purple light lamp 24, avoid the phenomenon that colorless product runs off.
A supporting rod 36 and a rotating rod 37 are mounted at the upper end of the outer portion of the chromatographic tube 32, a fastening mechanism 38 is arranged on one side, close to the supporting mechanism 4, of the chromatographic mechanism 3, the chromatographic tube 32 is rotatably connected with the fastening mechanism 38 through the rotating rod 37, the fastening mechanism 38 is composed of a bolt, a sleeve ring and a fixing plate, the fastening mechanism 38 is sleeved outside the supporting mechanism 4 through the sleeve ring and locked through the bolt, a rotating ring 39 is mounted on one side of the fastening mechanism 38, the rotating ring 39 is rotatably connected with the rotating rod 37, the whole locking mechanism 38 can control the height of the chromatographic mechanism 2 and complete fixing, and the fixing mode is the existing mature technical content and is not described in detail herein.
The use principle and the advantages are as follows: this chromatography ware is when using, the user carries out traditional chinese medicine extract's reprocessing according to the chromatography step, traditional chinese medicine extract composition after the chromatography passes through chromatography pipe 32, toper pipe 34 and hose 35 arrange in proper order in the collection test tube 27 on the test-tube rack 25, when the collection of traditional chinese medicine extract composition is in process, because the sample size is different, the collection test tube 27 that corresponds chromatography pipe 32 below, according to the size of collecting test tube 27, the collection test tube 27 one-to-one test-tube rack 25 that will wait to collect extract composition places in advance, after the present extract composition is collected, through rotating turntable 22, make next collection test tube 27 on the test-tube rack 25 shift and again correspond with hose 35, thereby avoid appearing the phenomenon that small amount of samples adopts big test tube to lead to single test tube to collect a plurality of samples, a large amount of samples adopts little test tube to promote work load again greatly, and need not collect taking of test tube 27 and stablize and place again, be favorable to reducing user's complex operation degree, promote traditional chinese medicine extract's chromatography efficiency.
To sum up: this chromatography ware can effectually avoid appearing that the small sample adopts big test tube to lead to single test tube to collect a plurality of samples, a large amount of samples adopt the small test tube to promote the phenomenon of work load again greatly, is favorable to reducing user's complex operation degree, promotes traditional chinese medicine extract's chromatography efficiency.
The above, only be the embodiment of the preferred of the present invention, but the protection scope of the present invention is not limited thereto, and any person skilled in the art is in the technical scope of the present invention, according to the technical solution of the present invention and the utility model, which are designed to be replaced or changed equally, all should be covered within the protection scope of the present invention.

Claims (7)

1. A traditional Chinese medicine extract reprocessing dialyzer is characterized by comprising a bottom plate (1), a supporting mechanism (4) and a chromatography mechanism (3) which are arranged above the bottom plate (1), wherein the supporting mechanism (4) is pivoted with the chromatography mechanism (3), and the chromatography mechanism (3) can rotate relative to the supporting mechanism (4); the chromatography mechanism (3) comprises a chromatography tube (32), a conical tube (34) and a hose (35), the chromatography tube (32), the conical tube (34) and the hose (35) are communicated, a funnel (31) is installed at the upper end of the chromatography tube (32), and a valve (33) is installed at the lower end of the chromatography tube (32); one side of bottom plate (1) top is equipped with placement machine structure (2), placement machine structure (2) is including carousel (22) and test-tube rack (25) and axostylus axostyle (21), carousel (22) rotate with bottom plate (1) through axostylus axostyle (21) mutually and are connected, test-tube rack (25) comprise a plurality of clamp rings that the internal diameter of solid fixed ring group differs, one of them the clamp ring on test-tube rack (25) is located chromatography mechanism (3) under, test-tube rack (25) are inserted through the clamp ring and are equipped with collection test tube (27), it comprises the standard test tube of the different specifications of a plurality of to collect test tube (27).
2. The dialyzer for retreatment of Chinese herbal extracts according to claim 1, wherein the supporting mechanism (4) comprises a bottom rod (41) and a top rod (43), the bottom rod (41) and the top rod (43) are connected with a plurality of rods (42), and one end of each protrusion on the plurality of rods (42) faces outward.
3. The dialyzer for retreatment of traditional Chinese medicine extracts according to claim 1, wherein the upper end of the rotary plate (22) is open, the bottom pad (28) is mounted at the bottom end inside the rotary plate (22), the test tube rack (25) is fixedly mounted at the upper end of the inner wall of the rotary plate (22), and the bottom pad (28) is provided with a concave groove (26) corresponding to the clamp ring on the test tube rack (25).
4. The chromatography apparatus for reprocessing the traditional Chinese medicine extract according to claim 1, wherein the upper end of the outside of the chromatography tube (32) is provided with a support rod (36) and a rotating rod (37), one side of the chromatography mechanism (3) close to the support mechanism (4) is provided with a fastening mechanism (38), and the chromatography tube (32) is rotatably connected with the fastening mechanism (38) through the rotating rod (37).
5. The dialyzer for reprocessing of Chinese herbal extracts according to claim 4, wherein the fastening mechanism (38) comprises a bolt, a collar and a fixing plate, the fastening mechanism (38) is sleeved outside the support mechanism (4) through the collar and locked by the bolt, a rotating ring (39) is installed on one side of the fastening mechanism (38), and the rotating ring (39) is rotatably connected with the rotating rod (37).
6. The dialyzer for reprocessing of Chinese herbal medicine extracts as claimed in claim 3, wherein a UV lamp (24) is fixedly installed in the middle of the upper surface of the bottom pad (28), and the UV lamp (24) rotates coaxially with the rotating disc (22).
7. The chromatography apparatus for reprocessing a herbal extract according to claim 1, wherein the upper end of the outer circumferential surface of said rotating disk (22) is provided with a plurality of anti-slip ribs (23).
CN202222226342.8U 2022-08-24 2022-08-24 Traditional chinese medicine extract retreatment chromatography ware Active CN218011198U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202222226342.8U CN218011198U (en) 2022-08-24 2022-08-24 Traditional chinese medicine extract retreatment chromatography ware

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202222226342.8U CN218011198U (en) 2022-08-24 2022-08-24 Traditional chinese medicine extract retreatment chromatography ware

Publications (1)

Publication Number Publication Date
CN218011198U true CN218011198U (en) 2022-12-13

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ID=84348802

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202222226342.8U Active CN218011198U (en) 2022-08-24 2022-08-24 Traditional chinese medicine extract retreatment chromatography ware

Country Status (1)

Country Link
CN (1) CN218011198U (en)

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