CN217830005U - Graphite oxidation reation kettle is used in graphite alkene production - Google Patents
Graphite oxidation reation kettle is used in graphite alkene production Download PDFInfo
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- CN217830005U CN217830005U CN202221774966.7U CN202221774966U CN217830005U CN 217830005 U CN217830005 U CN 217830005U CN 202221774966 U CN202221774966 U CN 202221774966U CN 217830005 U CN217830005 U CN 217830005U
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- Prior art keywords
- fixedly connected
- dwang
- casing
- graphite
- oxidation reaction
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- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims abstract description 46
- 229910002804 graphite Inorganic materials 0.000 title claims abstract description 42
- 239000010439 graphite Substances 0.000 title claims abstract description 42
- 238000007254 oxidation reaction Methods 0.000 title claims abstract description 22
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 19
- 230000003647 oxidation Effects 0.000 title claims abstract description 9
- -1 graphite alkene Chemical class 0.000 title claims abstract description 8
- 238000003756 stirring Methods 0.000 claims abstract description 14
- 229910021389 graphene Inorganic materials 0.000 claims description 12
- 239000003381 stabilizer Substances 0.000 claims description 5
- 238000007599 discharging Methods 0.000 claims description 2
- 238000009434 installation Methods 0.000 claims 2
- 239000000463 material Substances 0.000 abstract description 14
- 239000002253 acid Substances 0.000 abstract description 4
- 238000000034 method Methods 0.000 abstract description 3
- 239000007800 oxidant agent Substances 0.000 abstract description 3
- 230000001590 oxidative effect Effects 0.000 abstract description 3
- 238000007790 scraping Methods 0.000 abstract description 3
- 239000002699 waste material Substances 0.000 abstract description 3
- 230000000694 effects Effects 0.000 description 9
- 230000000087 stabilizing effect Effects 0.000 description 4
- 238000004880 explosion Methods 0.000 description 2
- 239000003292 glue Substances 0.000 description 2
- 238000004026 adhesive bonding Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003575 carbonaceous material Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
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- Mixers Of The Rotary Stirring Type (AREA)
Abstract
The utility model relates to a graphite alkene production technical field discloses a graphite oxidation reation kettle is used in graphite alkene production, which comprises a housin, the top middle part fixedly connected with motor of casing, the top middle part fixedly connected with dwang of casing is run through to the output bottom of motor, the equal fixedly connected with connecting rod in the middle part left and right sides of dwang, one side fixed connection mounting panel of keeping away from the dwang of connecting rod, one side fixedly connected with a plurality of springs of the dwang of keeping away from of mounting panel, the other end fixedly connected with scraper blade of spring. The utility model discloses in, realized scraping the material to the casing inner wall to the waste of material has been prevented, and can be reinforced in-process limit, the limit stirring, mix graphite and strong acid oxidant fully, prevented because mix the local overheat that the inequality leads to, greatly reduced danger coefficient.
Description
Technical Field
The utility model relates to a graphite alkene production technical field especially relates to a graphite oxidation reation kettle is used in graphite alkene production.
Background
Graphene is as an excellent novel carbon material, and graphene generally is mixing oxidation with graphite and strong acid at the in-process of making, reduces again and obtains graphite, consequently can generally use graphite oxidation reation kettle when graphite production, oxidizes graphite.
Oxidation reaction kettle among the prior art, when graphite carries out oxidation reaction, graphite can be because the inflation and glue on reation kettle's inner wall, and then be difficult for falling, consequently causes the waste of material to when adding strong acid oxidant in oxidation reaction, if mix inadequately, lead to local temperature too high easily, thereby lead to the explosion, greatly increased the danger coefficient.
SUMMERY OF THE UTILITY MODEL
The utility model aims at solving the defects existing in the prior art and providing a graphite oxidation reaction kettle for graphene production.
In order to achieve the above purpose, the utility model adopts the following technical scheme: the utility model provides a graphite oxidation reation kettle is used in graphite alkene production, which comprises a housin, the top middle part fixedly connected with motor of casing, the top middle part fixedly connected with dwang of casing is run through to the output bottom of motor, the equal fixedly connected with connecting rod in the middle part left and right sides of dwang, one side fixed connection mounting panel of keeping away from the dwang of connecting rod, a plurality of springs of one side fixedly connected with of dwang of mounting panel, the other end fixedly connected with scraper blade of spring, the equal fixedly connected with erection pin in both ends about one side of being close to the dwang of scraper blade, the equal fixedly connected with stirring leaf in both sides about the outside of dwang.
As a further description of the above technical solution:
two one side of installing pin that is close to the dwang is respectively through the through-hole fixedly connected with stopper at the upper and lower both ends of mounting panel, the scraper blade contacts with the inner wall of casing.
As a further description of the above technical solution:
the top left side fixedly connected with drain hole of casing, the top threaded connection of drain hole has the screw thread lid.
As a further description of the above technical solution:
the inside bottom fixedly connected with stabilizer bar of casing, the bottom of dwang is rotated and is connected in the top middle part of stabilizer bar.
As a further description of the above technical solution:
the bottom of the shell is fixedly connected with a funnel, the bottom of the funnel is fixedly connected with a discharge valve, and an inserting plate is slidably connected inside the discharge valve.
As a further description of the above technical solution:
the outside bottom fixedly connected with three fixed block of casing, the bottom fixedly connected with support column of fixed block.
As a further description of the above technical solution:
the front side fixedly connected with handle of picture peg, the shape of casing is cylindrical.
As a further description of the above technical solution:
the drain hole penetrates through the left side of the top of the shell.
The utility model discloses following beneficial effect has:
1. the utility model discloses in, through casing, motor, dwang, connecting rod, mounting panel, scraper blade isotructure, realized scraping the material to the casing inner wall, consequently glue glutinous graphite with shells inner wall and scrape down, prevented the waste of material.
2. The utility model discloses in, through casing, motor, dwang, stirring leaf isotructure, realized that the limit is reinforced, the limit stirring mixes graphite and strong acid oxidant fully, has prevented because the local overheat that the mixing inequality leads to, and then has prevented the explosion, greatly reduced danger coefficient.
Drawings
Fig. 1 is a front sectional view of a graphite oxidation reaction kettle for graphene production according to the present invention;
fig. 2 is a front view of a graphite oxidation reaction kettle for producing graphene according to the present invention;
fig. 3 is an enlarged view of a point a in fig. 1.
Illustration of the drawings:
1. a housing; 2. a motor; 3. rotating the rod; 4. a connecting rod; 5. mounting a plate; 6. a spring; 7. a squeegee; 8. mounting a pin; 9. a limiting block; 10. stirring blades; 11. a fixed block; 12. a threaded cap; 13. a discharging port; 14. a stabilizer bar; 15. a funnel; 16. a discharge valve; 17. inserting plates; 18. and (7) supporting the column.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative efforts all belong to the protection scope of the present invention.
Referring to fig. 1-3, the present invention provides an embodiment: the utility model provides a graphite oxidation reation kettle is used in graphite production, which comprises a housin 1, the top middle part fixedly connected with motor 2 of casing 1, motor 2's effect is for stirring and scraping the graphite of casing 1 inner wall down and provide power, motor 2's output bottom runs through casing 1's top middle part fixedly connected with dwang 3, dwang 3 rotates and drives connecting rod 4 and rotate, the equal fixedly connected with connecting rod 4 in the middle part left and right sides of dwang 3, connecting rod 4 rotates and drives mounting panel 5 and rotate, one side fixed connection mounting panel 5 of dwang 3 of keeping away from of connecting rod 4, mounting panel 5 rotates and drives mounting pin 8 and rotate, the equal fixedly connected with in one side of dwang 3 of keeping away from of mounting panel 5 a plurality of springs 6, the effect of spring 6 is extrusion scraper blade 7, make scraper blade 7 can laminate casing 1's inner wall tightly, spring 6's other end fixedly connected with scraper blade 7, scraper blade 7's effect is scraped the inside graphite of casing 1 down, scraper blade 7's the equal fixedly connected with mounting pin 8 in both ends about one side of dwang 3 that is close to scraper blade 7, the effect is connection scraper blade 7 is connection scraper blade 10 about the outside, the effect of stirring leaf 10 is the material of stirring leaf 1 inside mixing, the stirring of casing 1, the material mixing.
One side of the two mounting pins 8 close to the rotating rod 3 is fixedly connected with a limiting block 9 through holes at the upper end and the lower end of the mounting plate 5 respectively, the limiting block 9 is used for preventing the mounting pins 8 from being separated from the mounting plate 5, the scraper 7 is contacted with the inner wall of the shell 1 and can be tightly attached and contacted to scrape off the graphite adhered on the inner wall of the shell 1, the left side of the top of the shell 1 is fixedly connected with a discharge hole 13, the discharge hole 13 is used for facilitating the material to be put in, the top of the discharge hole 13 is in threaded connection with a threaded cover 12, the threaded cover 12 is used for covering the discharge hole 13 and preventing the material from flying out of the interior of the shell 1 in the stirring process, the bottom end of the interior of the shell 1 is fixedly connected with a stabilizing rod 14, the stabilizing rod 14 is used for stabilizing the rotating rod 3, and the bottom of the rotating rod 3 is rotatably connected to the middle part of the top end of the stabilizing rod 14, the fixed funnel 15 that has connect in bottom of casing 1, the effect of funnel 15 makes things convenient for the material to fall down, the bottom fixedly connected with bleeder valve 16 of funnel 15, the speed of falling down of bleeder valve 16 cooperation picture peg 17 can control the material, the inside sliding connection of bleeder valve 16 has picture peg 17, the three fixed block 11 of outside bottom fixedly connected with of casing 1, the effect of fixed block 11 is the support column 18 of easy to assemble, the bottom fixedly connected with support column 18 of fixed block 11, the effect of support column 18 is to prop up whole device, the front side fixedly connected with handle of picture peg 17, the effect of handle makes things convenient for the user to use, casing 1's shape is cylindrical, casing 1 is circular just can make things convenient for sticky graphite to scrape off on the casing 1 inner wall when scraper blade 7 rotates, drain hole 13 runs through casing 1's top left side.
The working principle is as follows: at first unscrew screw cap 12, pour the material into from drain hole 13, screw cap 12 on once more, starter motor 2, motor 2's output rotates and drives dwang 3 and rotate, dwang 3 rotates and drives stirring leaf 10 and rotates, stirring leaf 10 rotates and stirs the material of inside, the mixing, after the material reaction, for preventing gluing after the graphite inflation start motor 2 once more at casing 1's inner wall, motor 2's output rotates, drive connecting rod 4 and rotate, connecting rod 4 rotates and drives mounting panel 5 and rotate, mounting panel 5 rotates and drives mounting pin 8 and rotate, mounting pin 8 rotates and drives scraper blade 7 and rotate, scraper blade 7 rotates the back alright scrape sticky graphite on casing 1 inner wall.
Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that modifications and variations can be made in the embodiments or in part of the technical features of the embodiments without departing from the spirit and the scope of the invention.
Claims (8)
1. The utility model provides a graphite oxidation reation kettle is used in graphite alkene production, includes casing (1), its characterized in that: the utility model discloses a motor, including casing (1), the top middle part fixedly connected with motor (2) of casing (1), the top middle part fixedly connected with dwang (3) of casing (1) is run through to the output bottom of motor (2), the equal fixedly connected with connecting rod (4) of the middle part left and right sides of dwang (3), one side fixed connection mounting panel (5) of keeping away from dwang (3) of connecting rod (4), a plurality of springs (6) of one side fixedly connected with of keeping away from dwang (3) of mounting panel (5), the other end fixedly connected with scraper blade (7) of spring (6), the equal fixedly connected with installing pin (8) in both ends about the one side of being close to dwang (3) of scraper blade (7), the equal fixedly connected with stirring leaf (10) in both sides about the outside of dwang (3).
2. The graphite oxidation reaction kettle for graphene production according to claim 1, wherein: two one side of the installation pin (8) close to the rotating rod (3) is respectively provided with a limiting block (9) through the through holes at the upper end and the lower end of the installation plate (5), and the scraper (7) is in contact with the inner wall of the shell (1).
3. The graphite oxidation reaction kettle for graphene production according to claim 1, characterized in that: the top left side fixedly connected with drain hole (13) of casing (1), the top threaded connection of drain hole (13) has screw cap (12).
4. The graphite oxidation reaction kettle for graphene production according to claim 1, characterized in that: the inside bottom fixedly connected with stabilizer bar (14) of casing (1), the bottom of dwang (3) is rotated and is connected in the top middle part of stabilizer bar (14).
5. The graphite oxidation reaction kettle for graphene production according to claim 1, wherein: the bottom of casing (1) is fixed to be connect with funnel (15), the bottom fixedly connected with bleeder valve (16) of funnel (15), the inside sliding connection of bleeder valve (16) has picture peg (17).
6. The graphite oxidation reaction kettle for graphene production according to claim 1, characterized in that: the outer bottom end of the shell (1) is fixedly connected with three fixing blocks (11), and the bottom of each fixing block (11) is fixedly connected with a supporting column (18).
7. The graphite oxidation reaction kettle for graphene production according to claim 5, characterized in that: the front side of the inserting plate (17) is fixedly connected with a handle, and the shell (1) is cylindrical.
8. The graphite oxidation reaction kettle for graphene production according to claim 3, characterized in that: and the discharging port (13) penetrates through the left side of the top of the shell (1).
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN202221774966.7U CN217830005U (en) | 2022-07-11 | 2022-07-11 | Graphite oxidation reation kettle is used in graphite alkene production |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202221774966.7U CN217830005U (en) | 2022-07-11 | 2022-07-11 | Graphite oxidation reation kettle is used in graphite alkene production |
Publications (1)
Publication Number | Publication Date |
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CN217830005U true CN217830005U (en) | 2022-11-18 |
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CN202221774966.7U Active CN217830005U (en) | 2022-07-11 | 2022-07-11 | Graphite oxidation reation kettle is used in graphite alkene production |
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CN (1) | CN217830005U (en) |
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2022
- 2022-07-11 CN CN202221774966.7U patent/CN217830005U/en active Active
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
GR01 | Patent grant | ||
GR01 | Patent grant | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of utility model: A graphite oxidation reactor for graphene production Granted publication date: 20221118 Pledgee: Bank of Nanjing Co.,Ltd. Changzhou Branch Pledgor: Changzhou lanyue New Material Technology Co.,Ltd. Registration number: Y2024980024829 |