CN217593884U - Supercritical CO 2 Separation heater of extraction device - Google Patents

Supercritical CO 2 Separation heater of extraction device Download PDF

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Publication number
CN217593884U
CN217593884U CN202121224691.5U CN202121224691U CN217593884U CN 217593884 U CN217593884 U CN 217593884U CN 202121224691 U CN202121224691 U CN 202121224691U CN 217593884 U CN217593884 U CN 217593884U
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China
Prior art keywords
barrel
hot water
flange
fixedly connected
cylinder body
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CN202121224691.5U
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Chinese (zh)
Inventor
王成东
王剑武
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Shanghai Chengdong Technology Co ltd
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Shanghai Chengdong Technology Co ltd
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/54Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids

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  • Extraction Or Liquid Replacement (AREA)

Abstract

The utility model discloses a supercritical CO 2 A separation heater of an extraction device comprises a barrel, wherein a baffle plate is arranged in the barrel, a vertical tube nest is arranged in the barrel, an upper tube plate and a lower tube plate are respectively arranged at the upper end and the lower end of the barrel, the upper end and the lower end of the tube nest are fixedly connected with the upper tube plate and the lower tube plate in a sealing mode respectively, a lower end socket with a second flange is fixedly connected to the lower end of the barrel, the lower end socket is fixedly connected in a flange mode, and the bottom wall of the lower end socket is connected with a lower end socketCO 2 An outlet; the upper end of the cylinder is fixedly connected with an upper end enclosure with a first flange, the upper end enclosure is fixedly connected in a flange mode, and the top wall of the upper end enclosure is connected with CO 2 The inlet, the upper right portion of barrel is connected with the hot water export, and the left lower part of barrel is connected with the hot water import, and the hookup has hot water to arrange the clean mouth on the lateral wall of barrel below the hot water import.

Description

Supercritical CO 2 Separation heater of extraction device
Technical Field
The utility model relates to a supercritical CO 2 An extraction device, in particular to supercritical CO 2 A separation heater of an extraction device.
Background
Supercritical CO 2 In the extraction circulation process of the extraction device, the carbon dioxide coming out of the extraction kettle enters the separation kettlePreviously, the process temperature needed to be reached by separate heater heating according to the process requirements. Because the carbon dioxide from the extraction kettle is dissolved with the extraction product, the solubility of the extraction product and the carbon dioxide is changed after the pressure is reduced and the temperature is changed, and part of the extraction product is adsorbed on the tube wall of the heat exchange tube of the separation heater, so that the heat exchange effect of the separation heater is reduced, the inside of the heat exchange tube of the separation heater needs to be cleaned on time, but the existing separation heater has design defects, so that the cleaning of the heat exchange tube of the separation heater is difficult.
Disclosure of Invention
The utility model provides a convenient supercritical CO cleaning to the above deficiency 2 A separation heater of an extraction device.
The utility model discloses a realize like this: supercritical CO 2 A separation heater of an extraction device comprises a barrel, wherein a baffle plate is arranged in the barrel, a vertical tube nest is arranged in the barrel, an upper tube plate and a lower tube plate are respectively arranged at the upper end and the lower end of the barrel, the upper end and the lower end of the tube nest are fixedly connected with the upper tube plate and the lower tube plate in a sealing mode respectively, a lower end socket with a second flange is fixedly connected to the lower end of the barrel, the lower end socket is connected in a flange mode, and the bottom wall of the lower end socket is connected with CO 2 An outlet; the upper end of the cylinder is fixedly connected with an upper end enclosure with a first flange, the upper end enclosure is fixedly connected in a flange mode, and the top wall of the upper end enclosure is connected with CO 2 The inlet, the upper right portion of barrel is connected with the hot water export, and the left lower part of barrel is connected with the hot water import, and the hookup has hot water to arrange the clean mouth on the lateral wall of barrel below the hot water import.
With the above structure, when cleaning the inside of the tube array (heat exchange tube) of the separation heater, the pressure in the tube array is reduced to normal pressure, and CO is discharged from the upper end of the separation heater 2 Cleaning liquid is injected into the inlet, enters the tube nest through the inner cavity of the upper seal head 2 and then passes through the lower opening of the tube nest and CO 2 The outlet is discharged, and simultaneously the dirt of the tube array is washed out under the action of the cleaning liquid. Because the array of pipes are vertical, the dirt in the pipes can be washed down from top to bottom,the cleaning is easier, thereby solving the problem that the cleaning of the heat exchange tube is more difficult.
Drawings
FIG. 1 shows the supercritical CO of the present invention 2 The structure of the separation heater of the extraction device is shown schematically.
Detailed Description
The following describes the embodiments of the present invention in further detail with reference to the accompanying drawings.
As shown in FIG. 1, supercritical CO 2 The separation heater of the extraction device is provided with a vertical cylinder 13, a vertical tube array 6 and a baffle plate 7 are arranged in the cylinder 13, an upper tube plate 14 and a lower tube plate 8 are respectively arranged at the upper end and the lower end of the cylinder 13, the upper end and the lower end of the tube array 6 are respectively fixedly connected with the upper tube plate 14 and the lower tube plate 8 in a sealing manner, a lower end enclosure 9 with a second flange 9a is fixedly connected at the lower end of the cylinder 13, the fixed connection is realized in a flange manner, and the bottom wall of the lower end enclosure 9 is connected with CO 2 An outlet 10; the upper end of the cylinder 13 is fixedly connected with an upper end enclosure 2 with a first flange 3, the fixed connection is realized in a flange mode, and the top wall of the upper end enclosure 2 is connected with CO 2 The hot water purifier comprises an inlet 1, a hot water outlet 4 is connected to the upper right part of a cylinder 13, a hot water inlet 12 is connected to the lower left part of the cylinder 13, and a hot water discharge port 11 is connected to the side wall of the cylinder below the hot water inlet 12; the outer part of the cylinder body 13 is connected with a support lug 5. And (4) separating a heater shell pass and introducing hot water.

Claims (1)

1. Supercritical CO 2 The separation heater of the extracting device comprises a cylinder body, wherein a baffle plate is arranged in the cylinder body, and the separation heater is characterized in that: be equipped with vertical tubulation (6) in barrel (13), the upper and lower both ends of barrel (13) are equipped with tube sheet (14) and lower tube sheet (8) respectively, and the upper and lower both ends of tubulation (6) respectively with upper tube sheet (14) and lower tube sheet (8) with sealed mode rigid coupling, have low head (9) of second flange (9 a) at the lower extreme fixedly connected with of barrel (13), fixed connection is for connecting through the mode of flange, and the diapire of this low head (9) is connected with CO 2 An outlet (10); the upper end of the cylinder body (13) is fixedly connected with an upper seal head (2) with a first flange (3), and the fixed connection is thatConnected by a flange, and the top wall of the upper seal head (2) is connected with CO 2 The hot water purifier comprises an inlet (1), wherein the upper right part of a cylinder body (13) is connected with a hot water outlet (4), the lower left part of the cylinder body (13) is connected with a hot water inlet (12), and the side wall of the cylinder body below the hot water inlet (12) is connected with a hot water drainage port (11).
CN202121224691.5U 2021-05-31 2021-05-31 Supercritical CO 2 Separation heater of extraction device Active CN217593884U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202121224691.5U CN217593884U (en) 2021-05-31 2021-05-31 Supercritical CO 2 Separation heater of extraction device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202121224691.5U CN217593884U (en) 2021-05-31 2021-05-31 Supercritical CO 2 Separation heater of extraction device

Publications (1)

Publication Number Publication Date
CN217593884U true CN217593884U (en) 2022-10-18

Family

ID=83562201

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202121224691.5U Active CN217593884U (en) 2021-05-31 2021-05-31 Supercritical CO 2 Separation heater of extraction device

Country Status (1)

Country Link
CN (1) CN217593884U (en)

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