CN217448997U - Broken wall formula foam separation and purification device - Google Patents
Broken wall formula foam separation and purification device Download PDFInfo
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- CN217448997U CN217448997U CN202221566522.4U CN202221566522U CN217448997U CN 217448997 U CN217448997 U CN 217448997U CN 202221566522 U CN202221566522 U CN 202221566522U CN 217448997 U CN217448997 U CN 217448997U
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Abstract
The utility model discloses a broken wall formula foam separation purification device is applied to biochemical equipment technical field, include: a rectification part, a filtration part and a defoaming part; the rectification part is sequentially connected with the filtering part and the defoaming part; the rectification part is internally provided with a stirring device, and the stirring device comprises: a stirring member and a wall breaking member; the stirring pieces and the wall breaking pieces are arranged on two sides of the rotating shaft in a staggered mode. Broken wall foam separation and purification device be provided with rectifying column, filter, defoamer simultaneously, separate the material earlier, filter after, purify at last, ensured the higher purity and the purification efficiency of the product after the separation and purification.
Description
Technical Field
The utility model relates to a biochemical equipment technical field, more specifically the wall breaking formula foam separation purification device that says so relates to.
Background
A continuous foam rectification separation and purification method is a novel separation technology for concentrating and purifying surface active substances and non-surface active substances by using bubbles as a separation medium based on surface (interface) surface physics and an attached principle, and is continuously and widely applied to large-scale industrial production, such as separation and purification of proteins, enzymes, viruses and the like in biological and medical engineering, treatment of textile printing and dyeing wastewater, extraction of gentamicin, separation and purification of food additives and preservatives, aquaculture water treatment and the like.
In the existing foam rectification separation and purification technology, a continuous process device with a complete system does not exist, or the efficiency of the continuous process device is low, especially the existing stirring device is used for separately stirring and wall breaking, so that the operation time is greatly prolonged, the defoaming step is too long, and the economic benefit of the whole process is reduced.
Therefore, the technical personnel in the field need to solve the problem of how to provide a continuous foam separation and purification device with integrated stirring and wall breaking, high separation and purification efficiency.
SUMMERY OF THE UTILITY MODEL
In view of this, the utility model provides a broken wall formula foam separation and purification device, simple structure, separation and purification is efficient.
In order to achieve the above purpose, the utility model adopts the following technical scheme:
the utility model provides a broken wall formula foam separation purification device which characterized in that includes: a rectification part, a filtration part and a defoaming part;
the rectification part is sequentially connected with the filtering part and the defoaming part;
the rectification part is internally provided with a stirring device, and the stirring device comprises: a stirring member and a wall breaking member; the stirring pieces and the wall breaking pieces are arranged on two sides of the rotating shaft in a staggered mode.
Optionally, in the above wall-broken foam separation and purification apparatus, a rectification liquid inlet, a rectification liquid outlet, and a rectification gas outlet are formed in the rectification part;
the rectification liquid inlet and the rectification gas outlet are formed in the side wall of the rectification part;
the rectification exhaust port is communicated with the filtering part;
the rectification liquid outlet is arranged on the side wall or the bottom end of the rectification part.
Optionally, in the above wall-broken foam separation and purification apparatus, a heating device is disposed in the rectification part.
Optionally, in the above wall-broken foam separating and purifying apparatus, the heating device is an infrared radiator.
Optionally, in the above wall-broken foam separation and purification apparatus, the defoaming part is filled with a filler.
Optionally, in the above wall-broken foam separation and purification apparatus, the filler is an antifoaming agent.
Optionally, in the above wall-broken foam separation and purification apparatus, two layers of filtration membranes are disposed at an outlet of the defoaming portion, and the filtration membrane is an ultrafiltration membrane.
Optionally, in the above wall-broken foam separation and purification apparatus, a ratio of a radius of the liquid inlet of the rectification part to a radius of the gas outlet of the rectification part is 1: 1.2-2.
Optionally, in the above wall-broken foam separation and purification apparatus, a ratio of a radius of the outlet to a radius of the inlet of the defoaming portion is 1: 1.5-2.5.
Compared with the prior art, the foam separation and purification device has the following advantages:
(1) broken wall foam separation and purification device be provided with rectifying column, filter, defoamer simultaneously, separate the material earlier, filter after, purify at last, ensured the higher purity and the purification efficiency of the product after the separation and purification.
(2) The inner wall of the rectifying tower is provided with the infrared radiator, and the infrared radiator is arranged near the inner wall of the tower main body, so that the space is saved, the gas-liquid contact area is increased, and the efficiency is improved; and the infrared radiator has high thermal efficiency, the temperature is easy to control and adjust, and different temperature requirements of rectification can be met.
(3) The defoamer is provided with a filter membrane in the defoamer outlet, the filter membrane carries out secondary filtration to the material, the abundant purity of having guaranteed the material has improved the quality of product, has improved separation and purification efficiency.
(4) The stirring rod in the stirrer of the utility model is composed of a special structure, one side is in a stick shape, and the other side is in a knife shape. The stirring rod is used for stirring or breaking the wall through different rotating directions.
Drawings
In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings required to be used in the description of the embodiments or the prior art will be briefly described below, it is obvious that the drawings in the following description are only embodiments of the present invention, and for those skilled in the art, other drawings can be obtained according to the provided drawings without creative efforts.
Fig. 1 is a schematic structural diagram of the present invention.
1-rectifying tower, 2-filter, 3-defoamer, 4-rectifying tower liquid inlet, 5-rectifying tower liquid outlet, 6-rectifying tower exhaust port, 7-heater, 8-stirrer, 9-filter inlet, 10-filter outlet, 11-defoamer inlet, 12-defoamer outlet, 13-defoamer exhaust port, 14-filler, 15-filter membrane, 16-stirring piece and 17-wall breaking piece.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
The embodiment of the utility model discloses a broken wall formula foam separation purification device, as shown in figure 1, include: a rectification part, a filtration part and a defoaming part;
the rectification part is sequentially connected with the filtering part and the defoaming part;
the rectification part is internally provided with a stirring device, and the stirring device comprises: a stirring part 16 and a wall breaking part 17; the stirring pieces and the wall breaking pieces are arranged on two sides of the rotating shaft in a staggered mode.
Optionally, in the above wall-broken foam separation and purification apparatus, a rectification liquid inlet, a rectification liquid outlet, and a rectification gas outlet are formed in the rectification part;
the rectification liquid inlet and the rectification gas outlet are formed in the side wall of the rectification part;
the rectification exhaust port is communicated with the filtering part;
the rectification liquid outlet is arranged on the side wall or the bottom end of the rectification part.
Specifically, in the present embodiment, the rectifying section is a rectifying column 1;
in the present embodiment, the filter portion is a filter 2;
in the present embodiment, the defoaming section is a defoamer 3;
a rectifying tower liquid inlet 4 and a rectifying tower gas outlet 6 are arranged at the upper end of the rectifying tower 1, the rectifying tower liquid inlet 4 and the rectifying tower gas outlet 6 are arranged oppositely, a rectifying tower liquid outlet 5 is arranged at the lower end of the rectifying tower 1, a heater 7 is arranged on the inner wall of the rectifying tower 1, and a stirrer 8 is arranged in the rectifying tower 1;
the filter 2 is provided with a filter inlet 9 and a filter outlet 10, and the filter inlet 9 is connected with the exhaust port 6 of the rectifying tower through a pipeline;
the lower extreme of defoamer 3 is provided with defoamer import 11, defoamer export 12, and defoamer import 11 links to each other through the pipeline with filter export 10, and defoamer import 11 sets up with defoamer export 12 relatively, and defoamer export 12 department is provided with the filter membrane, and the top of defoamer 3 is provided with defoamer gas vent 13, is provided with filler 14 in the defoamer 3.
The heater 7 is selected to be an infrared radiator. The infrared radiator is arranged near the inner wall of the tower main body, so that the space is saved, the gas-liquid contact area is increased, and the efficiency is improved; and the infrared radiator has high thermal efficiency, the temperature is easy to control and adjust, and different temperature requirements of rectification can be met.
An antifoaming agent is added to the filler 14. The air bubbles are effectively eliminated, and the separation and purification effects are achieved.
Two layers of filter membranes are arranged at the outlet 12 of the defoamer, and the filter membranes use ultrafiltration membranes. The ultrafiltration membrane is used for carrying out secondary filtration on the materials, so that the purity of the materials is fully ensured, the quality of products is improved, and the separation and purification efficiency is improved.
The ratio of the radius of the liquid inlet 4 of the rectifying tower to the radius of the exhaust port 6 of the rectifying tower is 1: 1.5. the radius of the gas exhaust port 6 of the rectifying tower is larger than that of the liquid inlet 4 of the rectifying tower, so that foams can be fully discharged, the moving speed of the foams is increased, the speed of material separation and purification is increased, and the production efficiency is improved.
The ratio of the radii of the defoamer outlet 12 to the defoamer inlet 11 is 1: 1.5.
the embodiments in the present description are described in a progressive manner, each embodiment focuses on differences from other embodiments, and the same and similar parts among the embodiments are referred to each other. The device disclosed by the embodiment corresponds to the method disclosed by the embodiment, so that the description is simple, and the relevant points can be referred to the method part for description.
The previous description of the disclosed embodiments is provided to enable any person skilled in the art to make or use the present invention. Various modifications to these embodiments will be readily apparent to those skilled in the art, and the generic principles defined herein may be applied to other embodiments without departing from the spirit or scope of the invention. Thus, the present invention is not intended to be limited to the embodiments shown herein but is to be accorded the widest scope consistent with the principles and novel features disclosed herein.
Claims (9)
1. The utility model provides a broken wall formula foam separation purification device which characterized in that includes: a rectification part, a filtration part and a defoaming part;
the rectification part is sequentially connected with the filtering part and the defoaming part;
the rectification part is internally provided with a stirring device, and the stirring device comprises: a stirring member and a wall breaking member; the stirring pieces and the wall breaking pieces are arranged on two sides of the rotating shaft in a staggered mode.
2. The wall-broken foam separating and purifying device according to claim 1, wherein the rectifying part is provided with a rectifying liquid inlet, a rectifying liquid outlet and a rectifying exhaust port;
the rectification liquid inlet and the rectification gas outlet are formed in the side wall of the rectification part;
the rectification exhaust port is communicated with the filtering part;
the rectification liquid outlet is arranged on the side wall or the bottom end of the rectification part.
3. The wall-broken foam separating and purifying device as claimed in claim 1, wherein a heating device is arranged in the rectifying part.
4. A wall-broken type foam separating and purifying apparatus as claimed in claim 3, wherein the heating device is an infrared radiator.
5. The wall-broken foam separating and purifying device as claimed in claim 1, wherein the defoaming part is filled with a filler.
6. The wall-broken foam separating and purifying device as claimed in claim 5, wherein the filler is an antifoaming agent.
7. The wall-broken foam separating and purifying device as claimed in claim 1, wherein two layers of filter membranes are arranged at the outlet of the defoaming part, and the filter membranes are ultrafiltration membranes.
8. The wall-broken foam separating and purifying device of claim 1, wherein the ratio of the radius of the liquid inlet of the rectifying part to the radius of the gas outlet of the rectifying part is 1: 1.2-2.
9. The wall-broken foam separating and purifying device as claimed in claim 1, wherein the ratio of the radius of the outlet to the radius of the inlet of the defoaming part is 1: 1.5-2.5.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN202221566522.4U CN217448997U (en) | 2022-06-22 | 2022-06-22 | Broken wall formula foam separation and purification device |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CN202221566522.4U CN217448997U (en) | 2022-06-22 | 2022-06-22 | Broken wall formula foam separation and purification device |
Publications (1)
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CN217448997U true CN217448997U (en) | 2022-09-20 |
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CN202221566522.4U Active CN217448997U (en) | 2022-06-22 | 2022-06-22 | Broken wall formula foam separation and purification device |
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CN (1) | CN217448997U (en) |
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2022
- 2022-06-22 CN CN202221566522.4U patent/CN217448997U/en active Active
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