CN217404541U - Microstructure-based scintillating optical fiber, optical fiber array and luminous scintillator - Google Patents
Microstructure-based scintillating optical fiber, optical fiber array and luminous scintillator Download PDFInfo
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Abstract
Description
技术领域technical field
本实用新型属于核探测及射线、快中子成像领域,具体涉及一种基于微结构的闪烁光纤、光纤阵列及发光闪烁体。The utility model belongs to the fields of nuclear detection and ray and fast neutron imaging, in particular to a scintillation optical fiber, an optical fiber array and a luminescent scintillator based on a microstructure.
背景技术Background technique
闪烁探测系统在高能物理实验、核物理实验、核医学成像、天文探测、探矿测井、安检等领域都具有重要用途,往往涉及大科学工程或国家安全领域的重大需求。Scintillation detection systems have important uses in high-energy physics experiments, nuclear physics experiments, nuclear medicine imaging, astronomical detection, prospecting logging, security inspection and other fields, often involving major scientific projects or major needs in the field of national security.
闪烁体是闪烁探测系统中的核心功能材料,属于发光材料,可以吸收入射高能粒子(如电子、质子、中子、α粒子等)或高能光子(如X射线、γ射线),并将其能量转换成近紫外光或可见光,随后通过光电探测器件如光电倍增管、光电二极管或CCD最终实现对入射粒子或射线的探测。探测系统对闪烁体的普遍要求包括高光产额、快衰减、发射波长与光电探测器响应匹配、稳定的物理化学性质和低成本,对于γ射线探测还需要高密度。The scintillator is the core functional material in the scintillation detection system and belongs to the luminescent material, which can absorb incident high-energy particles (such as electrons, protons, neutrons, alpha particles, etc.) or high-energy photons (such as X-rays, γ-rays), and convert their energy It is converted into near-ultraviolet light or visible light, and then the detection of incident particles or rays is finally realized by photodetection devices such as photomultiplier tubes, photodiodes or CCDs. Common requirements for scintillators in detection systems include high light yield, fast decay, matching emission wavelengths with photodetector responses, stable physicochemical properties, and low cost, as well as high density for gamma-ray detection.
然而在实际应用中,由于无机闪烁体具有较高的折射率(约1.6~2.2),在辐射致闪烁体发光时,闪烁体内部的闪烁光子在出射界面会产生全反射,导致大量光子被限制在闪烁体的内部无法出射,即使小于全反射角的光可以出射,但由于出射角覆盖整个空间,而探测器可能布置于某个方向,会导致大部分出射角度的光无法进入探测器而被浪费。同时,闪烁光在传播的过程中容易发散,传输模式呈高斯分布如果不对光束进行调控,其成像质量仍然得不到显著提高。因此,提高闪烁体的光输出并控制其出射的方向性,对传输过程进行调控,对提高探测系统的探测效率和灵敏度、以及成像的质量都具有重要意义。However, in practical applications, due to the high refractive index (about 1.6-2.2) of the inorganic scintillator, when the scintillator emits light, the scintillation photons inside the scintillator will be totally reflected at the exit interface, resulting in a large number of photons being limited. It cannot be emitted from the interior of the scintillator, even if the light less than the total reflection angle can be emitted, but because the emission angle covers the entire space, and the detector may be arranged in a certain direction, most of the light with the emission angle cannot enter the detector and be rejected. waste. At the same time, the scintillation light is easy to diverge during the propagation process, and the transmission mode is Gaussian. If the beam is not controlled, the imaging quality will still not be significantly improved. Therefore, improving the light output of the scintillator, controlling the directionality of its output, and regulating the transmission process are of great significance to improving the detection efficiency and sensitivity of the detection system, as well as the imaging quality.
其次,在具有宏观尺寸(毫米至厘米尺度)的发光闪烁体的应用中,由于闪烁体被激发后闪烁光在闪烁体界面处发生多次反射可能导致时间特性的弥散,从而会降低探测系统的时间分辨能力。Second, in the application of luminescent scintillators with macroscopic dimensions (millimeter to centimeter scale), the multiple reflections of the scintillation light at the scintillator interface after the scintillator is excited may lead to the dispersion of temporal characteristics, which will reduce the detection efficiency. time resolution.
实用新型内容Utility model content
为了解决闪烁光的提取效率低及在传播的过程中容易发散,传输模式呈高斯分布,导致降低成像质量低的问题,本实用新型提供一种基于微结构的闪烁光纤、光纤阵列。In order to solve the problem of low extraction efficiency of scintillation light, easy divergence during propagation, and Gaussian distribution of transmission mode, resulting in low imaging quality, the utility model provides a scintillation optical fiber and an optical fiber array based on a microstructure.
同时,本实用新型还提供了一种基于微结构发光闪烁体,解决了发光闪烁体被激发后闪烁光在闪烁体界面处多次反射可能导致时间特性弥散和闪烁光出射效率低的问题。At the same time, the utility model also provides a light-emitting scintillator based on a microstructure, which solves the problems that the scintillation light is repeatedly reflected at the scintillator interface after the luminescent scintillator is excited, which may lead to time characteristic dispersion and low emission efficiency of the scintillation light.
本实用新型的具体技术方案如下:The concrete technical scheme of the present utility model is as follows:
一种基于微结构的闪烁光纤,用于提取和传输闪烁光,其改进之处在于:在闪烁材料制成的光纤基体上开设有外层空气孔组及内层空气孔阵列;A microstructure-based scintillation optical fiber is used for extracting and transmitting scintillation light. The improvement lies in that: an outer layer air hole group and an inner layer air hole array are opened on an optical fiber matrix made of a scintillation material;
外层空气孔组由多个第一空气孔构成;将所有第一空气孔的中心连接后围成规则的封闭图形;The outer layer air hole group is composed of a plurality of first air holes; the centers of all the first air holes are connected to form a regular closed figure;
内层空气孔阵列由多个第二空气孔构成,且所有第二空气孔均位于所述规则的封闭图形内部;The inner layer air hole array is composed of a plurality of second air holes, and all the second air holes are located inside the regular closed pattern;
多个第二空气孔的孔径由中心向外逐渐减小,且第一空气孔的孔径大于中心处的第二空气孔孔径。The diameters of the plurality of second air holes gradually decrease from the center to the outside, and the diameters of the first air holes are larger than the diameters of the second air holes at the center.
进一步地,上述多个第二空气孔的孔径由中心向外呈螺旋形逐渐梯度减小。Further, the apertures of the above-mentioned plurality of second air holes gradually decrease in a spiral shape from the center to the outside.
进一步地,上述规则的封闭图形为圆形或椭圆形或正多边形或矩形;Further, the closed figure of the above-mentioned rules is a circle or an ellipse or a regular polygon or a rectangle;
进一步地,上述第一空气孔和第二空气孔为圆形或椭圆形或正多边形或矩形。Further, the first air hole and the second air hole are circular or oval, regular polygon or rectangle.
进一步地,上述所有第一空气孔内填充有比光纤基体材料折射率低的有机液体闪烁材料或者固体闪烁体材料或者惰性气体;所有第二空气孔内填充有比光纤基体材料折射率低的有机液体闪烁材料或者固体闪烁体材料或者惰性气体。Further, all the above-mentioned first air holes are filled with organic liquid scintillator material or solid scintillator material or noble gas with a lower refractive index than the optical fiber matrix material; all second air holes are filled with organic liquid scintillator materials with a lower refractive index than the optical fiber matrix material. Liquid scintillator material or solid scintillator material or noble gas.
进一步地,上述光纤基体采用无机闪烁体材料或塑料闪烁体材料。Further, the above-mentioned optical fiber matrix adopts inorganic scintillator material or plastic scintillator material.
同时,本实用新型还提供了一种基于微结构的闪烁光纤阵列,包括多个上述的闪烁光纤,多个闪烁光纤之间以及多个闪烁光纤外围设置有杂光及核辐射射线吸收隔离层。At the same time, the utility model also provides a microstructure-based scintillation fiber array, comprising a plurality of the above scintillation fibers, and stray light and nuclear radiation ray absorption isolation layers are arranged between the plurality of scintillation fibers and the periphery of the plurality of scintillation fibers.
进一步地,上述闪烁光纤阵列为正多边形或平行四边形或圆形。Further, the above-mentioned scintillation fiber array is a regular polygon, a parallelogram or a circle.
另外,本实用新型还提供了一种基于微结构的发光闪烁体,用于激发出可见光,该闪烁体包括块体,其特征在于:所述块体上开设有外层空气孔组及内层空气孔阵列;In addition, the present invention also provides a light-emitting scintillator based on a microstructure for exciting visible light, the scintillator includes a block, and is characterized in that: the block is provided with an outer layer air hole group and an inner layer air hole array;
外层空气孔组由多个第一空气孔构成;将所有第一空气孔的中心连接后围成规则的封闭图形;The outer layer air hole group is composed of a plurality of first air holes; the centers of all the first air holes are connected to form a regular closed figure;
内层空气孔阵列由多个第二空气孔构成,且所有第二空气孔均位于所述规则的封闭图形内部;The inner layer air hole array is composed of a plurality of second air holes, and all the second air holes are located inside the regular closed pattern;
多个第二空气孔的孔径由中心向外逐渐减少,且第一空气孔的孔径大于中心处的第二空气孔孔径;The apertures of the plurality of second air holes gradually decrease from the center to the outside, and the apertures of the first air holes are larger than the apertures of the second air holes at the center;
所有第一空气孔和第二空气孔内均填充有比块体材料折射率低的有机液体闪烁材料或者固体闪烁体材料或惰性气体。All the first air holes and the second air holes are filled with organic liquid scintillator material or solid scintillator material or inert gas with a lower refractive index than the bulk material.
进一步地,上述规则的封闭图形内部为圆形或椭圆形或正多边形或矩形;第一空气孔和第二空气孔为为圆形或椭圆形或正多边形或矩形;块体采用无机闪烁体材料或塑料闪烁体材料制成。Further, the inside of the above-mentioned regular closed figure is a circle or an ellipse or a regular polygon or a rectangle; the first air hole and the second air hole are a circle or an ellipse or a regular polygon or a rectangle; the block is made of inorganic scintillator material. or plastic scintillator material.
与现有技术相比,本实用新型的优点在于:Compared with the prior art, the advantages of the present utility model are:
1、本实用新型通过在闪烁光纤基体上设置外层空气孔组及内层空气孔阵列,内层空气孔阵列中所有第二空气孔孔径由内向外呈梯度形逐渐减小,且均小于外层空气孔组的第一空气孔孔径,使得整个微结构光纤界面的空气孔部分折射率呈现低-高-低的分布,使得闪烁光在传输过程中限制在光纤或光纤阵列中,实现柔性封闭化传输,不易发散,同时实现光场的均匀调控。1. In the present invention, the outer layer air hole group and the inner layer air hole array are arranged on the base of the scintillation fiber. The first air hole diameter of the layer air hole group makes the refractive index of the air hole part of the entire microstructure fiber interface present a low-high-low distribution, so that the scintillation light is confined in the fiber or fiber array during the transmission process, realizing flexible sealing The transmission is not easy to diverge, and the uniform regulation of the light field is achieved at the same time.
2、本实用新型通过在发光闪烁体上设置外层空气孔组及内层空气孔阵列,内层空气孔阵列中所有第二空气孔孔径由内向外呈梯度形逐渐减小,且均小于外层空气孔组的第一空气孔孔径,该微结构的设计避免了发光闪烁体被激发后闪烁光在发光闪烁体界面处发生多次反射可能导致时间特性的弥散,从而降低探测系统的时间分辨能力的问题,同时解决了闪烁体内部的闪烁光子在出射界面会产生全反射,导致大量光子被限制在闪烁体的内部无法出射,导致闪烁光无法有效提取的问题。2. In the present invention, the outer layer air hole group and the inner layer air hole array are arranged on the light-emitting scintillator, and the diameter of all the second air holes in the inner layer air hole array gradually decreases from the inside to the outside in a gradient shape, and is smaller than the outer layer. The first air hole diameter of the layer air hole group, the design of the microstructure avoids the multiple reflections of the scintillation light at the interface of the luminescent scintillator after the luminescent scintillator is excited, which may lead to the dispersion of time characteristics, thereby reducing the time resolution of the detection system. At the same time, it solves the problem that the scintillation photons inside the scintillator will be totally reflected at the exit interface, resulting in a large number of photons being confined inside the scintillator and unable to exit, resulting in the inability to effectively extract the scintillation light.
3、本实用新型提出的闪烁光纤、光纤阵列可以实现闪烁光的可柔性弯曲传输,扩大应用场景,且成像质量和分辨率高。3. The scintillation optical fibers and optical fiber arrays proposed by the present invention can realize flexible and bendable transmission of scintillation light, expand application scenarios, and have high imaging quality and resolution.
附图说明Description of drawings
图1为本实施例的结构示意图。FIG. 1 is a schematic structural diagram of this embodiment.
图2为本实施例的折射率分布区域示意图。FIG. 2 is a schematic diagram of a refractive index distribution region of this embodiment.
图3为本实施例的光纤中闪烁光传输的模场图。FIG. 3 is a mode field diagram of scintillation light transmission in the optical fiber of the present embodiment.
图4为中间为实心的光纤传输模场图。FIG. 4 is a transmission mode field diagram of an optical fiber with a solid center.
图5为具有均匀空气孔微结构的光纤传输模场图。FIG. 5 is a transmission mode field diagram of an optical fiber with a uniform air hole microstructure.
图6为本实施例的光纤中光纤传输能量呈平坦分布的曲线图。FIG. 6 is a graph showing a flat distribution of optical fiber transmission energy in the optical fiber of the present embodiment.
图7为空气孔呈螺旋结构光纤横截面微结构结构示意图。FIG. 7 is a schematic diagram of the microstructure of the cross-sectional microstructure of an optical fiber with air holes in a helical structure.
图8为光纤按正六边形阵列排布的闪烁光纤阵列单体结构图。FIG. 8 is a structural diagram of a single scintillation fiber array in which the fibers are arranged in a regular hexagonal array.
图9为光纤按正方形阵列排布的闪烁光纤阵列单体结构图。FIG. 9 is a structural diagram of a single scintillation optical fiber array with optical fibers arranged in a square array.
图10为通过拼接熔并拉伸后的闪烁光纤阵列结构图。FIG. 10 is a structural diagram of the scintillation fiber array after fusion and stretching by splicing.
附图标记如下:The reference numbers are as follows:
1-光纤基体、2-外层空气孔组、3-内层空气孔阵列、21-第一空气孔、31-第二空气孔、4-闪烁光纤、5-杂光及核辐射射线吸收隔离层。1-fiber matrix, 2-outer layer air hole group, 3-inner layer air hole array, 21-first air hole, 31-second air hole, 4-scintillation fiber, 5-stray light and nuclear radiation ray absorption and isolation Floor.
具体实施方式Detailed ways
为使本实用新型的上述目的、特征和优点能够更加明显易懂,下面结合说明书附图对本实用新型的具体实施方式做详细的说明,显然所描述的实施例是本实用新型的一部分实施例,而不是全部实施例。基于本实用新型中的实施例,本领域普通人员在没有做出创造性劳动前提下所获得的所有其他实施例,都应当属于本实用新型的保护的范围。In order to make the above-mentioned purposes, features and advantages of the present utility model more obvious and easy to understand, the specific embodiments of the present utility model will be described in detail below in conjunction with the accompanying drawings. Obviously, the described embodiments are part of the present utility model. not all examples. Based on the embodiments of the present invention, all other embodiments obtained by those of ordinary skill in the art without creative work shall fall within the protection scope of the present invention.
在下面的描述中阐述了很多具体细节以便于充分理解本实用新型,但是本实用新型还可以采用其他不同于在此描述的其它方式来实施,本领域技术人员可以在不违背本实用新型内涵的情况下做类似推广,因此本实用新型不受下面公开的具体实施例的限制。In the following description, many specific details are set forth in order to fully understand the present utility model, but the present utility model can also be implemented in other ways different from those described herein, and those skilled in the art can do so without departing from the connotation of the present utility model. Therefore, the present invention is not limited by the specific embodiments disclosed below.
同时在本实用新型的描述中,需要说明的是,术语中的“前、后、内和外”等指示的方位或位置关系为基于附图所示的方位或位置关系,仅是为了便于描述本实用新型和简化描述,而不是指示或暗示所指的装置或元件必须具有特定的方位、以特定的方位构造和操作,因此不能理解为对本实用新型的限制。此外,术语“第一、第二或第三”仅用于描述目的,而不能理解为指示或暗示相对重要性。At the same time, in the description of the present utility model, it should be noted that the orientation or positional relationship indicated by "front, rear, inner and outer" in the terms is based on the orientation or positional relationship shown in the accompanying drawings, which is only for the convenience of description. The present invention and the simplified description are not intended to indicate or imply that the devices or elements referred to must have a particular orientation, be constructed and operate in a particular orientation, and therefore should not be construed as a limitation of the present invention. Furthermore, the terms "first, second or third" are used for descriptive purposes only and should not be construed to indicate or imply relative importance.
本实用新型中除非另有明确的规定和限定,术语“安装、相连、连接”应做广义理解,例如:可以是固定连接、可拆卸连接或一体式连接:同样可以是机械连接、电连接或直接连接,也可以通过中间媒介间接相连,也可以是两个元件内部的连通。对于本领域的普通技术人员而言,可以具体情况理解上述术语在本实用新型中的具体含义。Unless otherwise expressly specified and limited in this utility model, the term "installation, connection, connection" should be understood in a broad sense, for example: it may be a fixed connection, a detachable connection or an integrated connection: it may also be a mechanical connection, an electrical connection or a Direct connection, indirect connection through an intermediate medium, or internal communication between two elements. For those of ordinary skill in the art, the specific meanings of the above terms in the present invention can be understood in specific situations.
本实施例提供一种基于微结构的闪烁光纤以及由这种光纤制备的光纤阵列,如图1所示为微结构闪烁光纤的横截面图,微结构闪烁光纤包括:闪烁材料制成的光纤基体1、外层空气孔组2,内层空气孔阵列3;This embodiment provides a microstructure-based scintillation optical fiber and an optical fiber array prepared from the optical fiber. FIG. 1 is a cross-sectional view of the microstructured scintillation optical fiber. The microstructured scintillation optical fiber includes: an optical fiber matrix made of a
外层空气孔组由2多个第一空气孔21构成;将所有第一空气孔21的中心连接后围成规则的封闭图形;本实施例中规则的封闭图形为正六边形。The outer layer air hole group is composed of two or more first air holes 21; the centers of all the first air holes 21 are connected to form a regular closed figure; in this embodiment, the regular closed figure is a regular hexagon.
内层空气孔阵列3由多个第二空气孔31构成,且所有第二空气孔31均位于所述规则的封闭图形内部;The inner layer
第一空气孔21的孔直径比第二空气孔31的孔直径大;多个第二空气孔31中孔径最大的为中心处的第二空气孔31,且多个第二空气孔31的孔径由中心至外呈逐渐减小的变化趋势。假设内层空气孔阵列33中心区域折射率为n1(如图2中虚线圆A内的区域),外层空气孔组2构成的区域折射率为n3(如图2中虚线圆B和虚线圆C间的环形区域),二者之间的区域折射率为n2(如图2中虚线圆A和虚线圆B间的环形区域),则有n1<n2>n3,整个微结构光纤界面的空气孔部分折射率呈现低-高-低的分布。这种结构可以实现光束光场的均匀调控,具体如图3所示,本实用新型设计的梯度折射率的微结构闪烁光纤,传输时闪烁光能量分布比较均匀,说明光束传输的光场比较均匀,该结构可以实现光束光场的均匀性调控。图4为中间实心的光纤传输模场图,图5为所有空气孔设置为均匀孔径时光纤传输模场图。将图4、5与图3进行比较可见,图4、5中闪烁光的能量传输呈高斯分布,这种模式影响最终的成像质量。图6为光纤中光纤传输能量呈平坦分布的曲线图,进一步佐证了本实用新型设计的光纤可实现能量均匀传输。The hole diameter of the
除此本实施例之外,规则的封闭图形还可以为圆形或椭圆形或其他正多边形或矩形。内层空气孔阵列可以是正六边形如图1所示,也可以是正方形或椭圆形形或圆形或其他正多边形等任意形状。In addition to this embodiment, the regular closed figure may also be a circle or an ellipse or other regular polygons or rectangles. The air hole array in the inner layer can be a regular hexagon as shown in Figure 1, or it can be any shape such as a square, an ellipse, a circle or other regular polygons.
优选地,本实施例中多个第二空气孔31的孔径由中心至外呈螺旋形逐渐减小,如图7所示。Preferably, in this embodiment, the apertures of the plurality of second air holes 31 gradually decrease in a spiral shape from the center to the outside, as shown in FIG. 7 .
第一空气孔21和第二空气孔31也可以是圆形或椭圆形正方形或三角形或其他正多边形等任意形状,本实施例中第一空气孔21和第二空气孔31为圆形。The
第一空气孔21和第二空气孔31可以由比光纤基体材料折射率低的有机液体闪烁体填充,或者可以由比光纤基体材料折射率低的固体闪烁体材料填充或者惰性气体。The first air holes 21 and the second air holes 31 may be filled with an organic liquid scintillator having a lower refractive index than the optical fiber matrix material, or may be filled with a solid scintillator material having a lower refractive index than the optical fiber matrix material or an inert gas.
本实施例中,光纤基体可以为无机闪烁体材料,包括但不限于:NaI(Tl)、CsI(Tl)、ZnS(Ag)、BGO等中的一种或几种组合,也可以为塑料闪烁体材料,包括但不限于:EJ200,EJ230、NE213、ST401、NE102A、NE104中的一种或几种组合。In this embodiment, the optical fiber matrix may be an inorganic scintillator material, including but not limited to: one or a combination of NaI(Tl), CsI(Tl), ZnS(Ag), BGO, etc., or a plastic scintillator material Body materials, including but not limited to: one or several combinations of EJ200, EJ230, NE213, ST401, NE102A, and NE104.
如图8所示,本实施例提供了一种由上述闪烁光纤构成的闪烁光纤阵列单体,该阵列单体包括多根闪烁光纤4,多个闪烁光纤4之间以及多个闪烁光纤4外围设置有杂光及核辐射射线吸收隔离层5,该杂光及核辐射射线吸收隔离层5的设置目的是为了避免闪烁光纤之间产生串扰。As shown in FIG. 8 , this embodiment provides a single scintillation fiber array composed of the above-mentioned scintillation fibers. The array includes a plurality of
该光纤阵列单体的制作方法有以下两种:The fabrication methods of the fiber array monomer are as follows:
第一种方法是:采用多个闪烁光纤按照切割-拼接的方式直接制作而成,但是该方法对制作工艺要求较高,且实施过程比较繁琐。The first method is to use multiple scintillation optical fibers to directly fabricate in a cutting-splicing method, but this method requires higher fabrication process and is more complicated to implement.
第二种方法是:将直径较粗的闪烁光纤穿插进多孔的闪烁光纤和杂光复合隔离层制成的预制棒中,再通过预制棒拉伸的方法将光纤阵列的像元素提高,最后将拉伸后的多个光纤阵列单体通过切割-拼接-熔并-拉伸的方法提高整个光纤阵列的总的像元数,这种方法解决了拼接方法对制作工艺要求较高,且拼接工艺繁琐的弊端。The second method is to insert a scintillation fiber with a larger diameter into a preform made of a porous scintillation fiber and a stray light composite isolation layer, and then stretch the preform to improve the image element of the fiber array. The stretched multiple fiber array monomers are cut-spliced-melted and stretched to increase the total number of pixels in the entire fiber array. This method solves the problem that the splicing method has high requirements on the manufacturing process, and splicing The disadvantages of cumbersome process.
该闪烁光纤阵列的探测区域可以如图8所示的正六边形、图9所示的正方形,也可以为平行四边形、多边形、圆形等不限于以上几种形状的其他形状,且图10所示的结构为图8所示闪烁光纤阵列单体通过切割-拼接-熔并-拉伸后得到的具有更大矩阵且分辨率更高的闪烁光纤阵列。The detection area of the scintillation fiber array can be a regular hexagon as shown in FIG. 8 , a square as shown in FIG. 9 , or a parallelogram, a polygon, a circle, and other shapes that are not limited to the above shapes. The structure shown is a scintillation fiber array with a larger matrix and higher resolution obtained by cutting-splicing-melting-drawing of the scintillation fiber array monomer shown in FIG. 8 .
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