CN217403876U - Anti-adhesion vacuum reaction kettle sampling device - Google Patents
Anti-adhesion vacuum reaction kettle sampling device Download PDFInfo
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- CN217403876U CN217403876U CN202220170556.5U CN202220170556U CN217403876U CN 217403876 U CN217403876 U CN 217403876U CN 202220170556 U CN202220170556 U CN 202220170556U CN 217403876 U CN217403876 U CN 217403876U
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Abstract
The utility model discloses an antiseized vacuum reaction cauldron sampling device who attaches relates to sampling device technical field, and it includes the reation kettle body, the right side of reation kettle body is provided with sampling device, sampling device's upper and lower side is provided with conveyor and lower conveyor respectively. Through the conveyer pipe one that sets up and the upper and lower side of conveyer pipe two respectively intercommunication at the sampling tube, open valve two and valve three on the conveyer pipe one, open back with valve four and valve five on the conveyer pipe two, this internal feed liquid of reation kettle can enter into in the sampling tube this moment, then with valve two, valve three, valve four and valve five are all closed, and will dock valve one on the pipe closed, through rotatory butt joint cover one and butt joint cover two, break away from on two butt joint pipes, can take off the sampling tube directness this moment, can avoid the feed liquid of sample to expose.
Description
Technical Field
The utility model relates to a sampling device, in particular to anti-adhesion vacuum reaction kettle sampling device.
Background
At present in the chemical industry, operating personnel need draw the feed liquid from the vacuum reation kettle in operation and detect, need pour into the graduated flask in from sample connection blowing to the container earlier at present, and operation process is loaded down with trivial details like this, and very easily causes the feed liquid to pollute, and can cause the feed liquid adhesion at other positions such as sample connection after the sample, the feed liquid of sample simultaneously also is not convenient for add vacuum reation kettle again in, consequently, need the vacuum reation kettle sampling device of an antiseized adhesion to solve above-mentioned problem.
SUMMERY OF THE UTILITY MODEL
An object of the utility model is to provide an antiseized vacuum reation kettle sampling device who attaches to the present sampling process who proposes among the solution above-mentioned background art is loaded down with trivial details, and very easily causes the feed liquid to pollute, and can cause the feed liquid adhesion to other positions such as sample connection after the sample, the feed liquid of sample simultaneously also is not convenient for add the problem in the vacuum reation kettle again.
In order to achieve the above purpose, the utility model provides a following technical scheme: an anti-adhesion vacuum reaction kettle sampling device comprises a reaction kettle body, wherein a sampling device is arranged on the right side of the reaction kettle body, an upper conveying device and a lower conveying device are respectively arranged on the upper side and the lower side of the sampling device, a liquid storage device is arranged on the upper side of the upper conveying device, and a pressurizing device is arranged on the right side of the liquid storage device;
the sampling device comprises sampling tubes, butt joint tubes are fixedly arranged at the upper end and the lower end of each sampling tube, external threads I are arranged on the outer walls of the two butt joint tubes, and valves I are arranged on the two butt joint tubes;
the upper conveying device comprises a first conveying pipe, the first conveying pipe is communicated with the reaction kettle body, and a second valve is arranged on one side, close to the reaction kettle body, of the first conveying pipe;
the lower conveying device comprises a second conveying pipe, the second conveying pipe is communicated with the bottom side of the reaction kettle body, and a fourth valve is arranged on one side, close to the bottom side of the reaction kettle body, of the second conveying pipe.
As an optimal technical scheme of the utility model, the stock solution device includes the liquid reserve tank, and the bottom intercommunication of institute liquid reserve tank has transfer line and a conveyer pipe intercommunication, install valve six on the transfer line, and the fixed right side wall that sets up at the reation kettle body of liquid reserve tank.
As the utility model discloses a preferred technical scheme, pressure device is including adding the pressure cylinder, add the pressure cylinder through two connecting rods and reation kettle body fixed connection, the top side intercommunication that adds the pressure cylinder has a gas-supply pipe and a conveyer pipe intercommunication, valve seven is installed to the bottom of gas-supply pipe, it is provided with otic placode, two all to fix in the back wall upper and lower end of adding the pressure cylinder the otic placode is all connected through the rotation of the last lower extreme optical axis department of bearing with the threaded rod.
As an optimal technical scheme of the utility model, threaded connection has a screw thread section of thick bamboo on the threaded rod, screw thread section of thick bamboo external fixation is provided with L shape connecting rod, L shape connecting rod and the pull pole fixed connection who pressurizes a section of thick bamboo, the fixed rotary rod that is provided with of lower extreme of threaded rod.
As the utility model discloses a preferred technical scheme, external screw thread two has been seted up to the bottom side outer wall of conveyer pipe one, threaded connection has a butt joint cover one on the external screw thread two, the conveyer pipe is first to install the valve three with two adjacent positions of external screw thread.
As a preferred technical scheme of the utility model, external screw thread three has been seted up to the bottom side outer wall of conveyer pipe two, threaded connection has a butt joint cover two on the external screw thread three, the valve five is installed with three adjacent positions of external screw thread on the conveyer pipe two, install the fluid-discharge tube with one side that reation kettle body bottom side is close to on the conveyer pipe two, and install the rotary valve on the fluid-discharge tube.
As an optimal technical scheme of the utility model, butt joint cover one and butt joint cover two respectively with two external screw thread threaded connection on the butt joint pipe of upper and lower side.
Compared with the prior art, the beneficial effects of the utility model are that:
the utility model discloses a first conveyer pipe and second conveyer pipe that set up communicate respectively on the upper and lower sides of sampling tube, when opening second valve and third valve on the conveyer pipe, after opening fourth valve and fifth valve on the conveyer pipe, the feed liquid in the reation kettle body can enter into the sampling tube at this moment, then close second valve, third valve, fourth valve and fifth valve all, and close first valve on the butt joint pipe, through rotatory butt joint cover one and butt joint cover two, break away from two butt joint pipes, can take off the sampling tube directly at this moment, can avoid the feed liquid of sample to expose, and later stage through butt joint pipe and conveyer pipe and second conveying pipe of butt joint of upper and lower extreme of sampling tube, through the gaseous conveying in the sampling tube of pressure device, can insert the feed liquid in the sampling tube into the reation kettle body again, and the liquid that stores through the liquid reserve tank that sets up can also carry the interior washing of sampling tube, the sample tube, the first conveying pipe and the second conveying pipe can be prevented from being adhered with the feed liquid.
Drawings
FIG. 1 is a schematic perspective view of the present invention;
FIG. 2 is a schematic view of a partial three-dimensional structure of the present invention;
FIG. 3 is a schematic view of the three-dimensional structure of the sampling device of the present invention;
FIG. 4 is a schematic view of the local top-view three-dimensional structure of the present invention;
fig. 5 is a schematic view of the three-dimensional structure of the pressurizing device of the present invention.
In the figure: 1 reaction kettle body, 2 sampling device, 21 sampling tube, 22 butt joint tube, 23 external thread I, 24 valve I, 3 upper conveying device, 31 conveying pipe I, 32 valve II, 33 external thread II, 34 butt joint sleeve I, 35 valve III, 4 lower conveying device, 41 conveying pipe II, 42 external thread III, 43 butt joint sleeve II, 44 valve V, 45 valve IV, 46 liquid discharge pipe, 5 liquid storage device, 51 liquid storage tank, 52 liquid conveying pipe, 53 valve VI, 6 pressurizing device, 61 pressurizing barrel, 62 gas conveying pipe, 63 valve seven, 64 lug plate, 65 threaded rod, 66 threaded barrel, 67 rotating rod and 68L-shaped connecting rod.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
As shown in fig. 1-5, the utility model provides a technical solution: an anti-adhesion vacuum reaction kettle sampling device comprises a reaction kettle body 1, wherein a sampling device 2 is arranged on the right side of the reaction kettle body 1, an upper conveying device 3 and a lower conveying device 4 are respectively arranged on the upper side and the lower side of the sampling device 2, a liquid storage device 5 is arranged on the upper side of the upper conveying device 3, and a pressurizing device 6 is arranged on the right side of the liquid storage device 5;
the sampling device 2 comprises sampling tubes 21, butt-joint tubes 22 are fixedly arranged at the upper and lower ends of the sampling tubes 21, external threads I23 are arranged on the outer walls of the two butt-joint tubes 22, and valves I24 are arranged on the two butt-joint tubes 22;
the upper conveying device 3 comprises a first conveying pipe 31, the first conveying pipe 31 is communicated with the reaction kettle body 1, and a second valve 32 is arranged on one side, close to the reaction kettle body 1, of the first conveying pipe 31;
the lower conveying device 4 comprises a second conveying pipe 41, the second conveying pipe 41 is communicated with the bottom side of the reaction kettle body 1, and a fourth valve 45 is arranged on one side, close to the bottom side of the reaction kettle body 1, of the second conveying pipe 41.
Stock solution device 5 includes liquid reserve tank 51, the bottom intercommunication of liquid reserve tank 51 has transfer line 52 and 31 intercommunications of conveyer pipe, install six 53 of valve on the transfer line 52, and liquid reserve tank 51 is fixed to be set up at the right side wall of reation kettle body 1, open six 53 of valve, liquid stored through the liquid reserve tank 51 that sets up also can carry and wash in the sampling tube 21, liquid reserve tank 51's top is provided with one-way admission valve, can make the entering gas in the liquid reserve tank 51, can guarantee that the washing liquid in the liquid reserve tank 51 utilizes gravity to flow into in the conveyer pipe 31, then discharge through fluid-discharge tube 46, can avoid sampling tube 21, conveyer pipe 31 and two 41 inner wall adhesion feed liquids of conveyer pipe.
A threaded barrel 66 is connected with the threaded rod 65 through threads, an L-shaped connecting rod 68 is fixedly arranged outside the threaded barrel 66, the L-shaped connecting rod 68 is fixedly connected with a pulling rod of the pressurizing barrel 61, a rotating rod 67 is fixedly arranged at the lower end of the threaded rod 65, when feed liquid needs to be added into the reaction kettle body 1 again, the butt joint pipe 22 at the upper end and the lower end of the sampling tube 21 is in butt joint with the conveying pipe I31 and the conveying pipe II 41, the valve VII 63 is opened, the threaded rod 65 is rotated through the rotating rod 67, the threaded barrel 66 can ascend on the threaded rod 65 at the moment, the L-shaped connecting rod 68 can drive the pulling rod of the pressurizing barrel 61 to ascend, a piston in the pressurizing barrel 61 ascends, air in the pressurizing barrel 61 is conveyed into the conveying pipe I31 through the air conveying pipe 62, at the moment, the air can convey the feed liquid in the sampling tube 21 into the reaction kettle body 1 through the conveying pipe II 41, and further realize the air conveying to the sampling tube 21 through the pressurizing device 6, the feed liquid in the sampling tube 21 can be connected into the reaction kettle body 1 again.
The outer wall of the bottom side of the first conveying pipe 31 is provided with a second external thread 33, the second external thread 33 is in threaded connection with a first butting sleeve 34, and a third valve 35 is installed on the first conveying pipe 31 at a position adjacent to the second external thread 33.
The outer wall of the bottom side of the conveying pipe II 41 is provided with an external thread III 42, the external thread III 42 is in threaded connection with a butting sleeve II 43, a valve fifth 44 is arranged on the conveying pipe II 41 and adjacent to the external thread III 42, a liquid discharge pipe 46 is arranged on one side, close to the bottom side of the reaction kettle body 1, of the conveying pipe II 41, a rotary valve is arranged on the liquid discharge pipe 46, the valve second 32 and the valve third 35 on the conveying pipe I31 are opened, after the valve fourth 45 and the valve fifth 44 on the conveying pipe II 41 are opened, the liquid in the reaction kettle body 1 can enter the sampling pipe 21, the valve second 32, the valve third 35, the valve fourth 45 and the valve fifth 44 are closed, the valve first 24 on the butting pipe 22 is closed, the butting sleeve I34 and the butting sleeve II 43 are rotated, at this time, the butting sleeve I34 can rise to the upper side part of the external thread II 33, the butting sleeve II 43 descends to the lower side part of the external thread III 42, the separation from the two butt joint pipes 22 on the first butt joint sleeve 34 and the second butt joint sleeve 43 is realized, the sampling pipe 21 can be directly taken down, and the upper end and the lower end of the sampling pipe 21 can be sealed by the butt joint pipes 22 on the upper side and the lower side of the sampling pipe 31 due to the arrangement of the first valve 24, so that the liquid material for sampling can be prevented from being exposed.
The first butting sleeve 34 and the second butting sleeve 43 are in threaded connection with the first external thread 23 on the two butting pipes 22 on the upper side and the lower side respectively.
The utility model discloses an operating procedure does:
by opening the second valve 32 and the third valve 35 on the first conveying pipe 31, opening the fourth valve 45 and the fifth valve 44 on the second conveying pipe 41, then allowing the material liquid in the reaction kettle body 1 to enter the sampling pipe 21, then closing the second valve 32, the third valve 35, the fourth valve 45 and the fifth valve 44, closing the first valve 24 on the butt joint pipe 22, rotating the butt joint sleeve 34 and the butt joint sleeve 43, at this time, the butt joint sleeve 34 rises to the upper side part of the second external thread 33, the butt joint sleeve 43 descends to the lower side part of the third external thread 42, so that the first butt joint sleeve 34 and the butt joint sleeve 43 are separated from the two butt joint pipes 22, at this time, the sampling pipe 21 can be directly taken down, the butt joint pipes 22 on the upper side and the lower side of the sampling pipe 31 are provided with the first valve 24, the upper end and the lower end of the sampling pipe 21 can be sealed, the sampled material liquid can be prevented from being exposed, and the butt joint pipes 22 on the upper end and the lower end of the sampling pipe 21 are butted with the first conveying pipe 31 and the second conveying pipe 41, open valve seven 63, through the rotatory threaded rod 65 of rotary rod 67, a screw section of thick bamboo 66 can rise on threaded rod 65 this moment, L shape connecting rod 68 can drive the pull pole of a pressurization section of thick bamboo 61 and rise, make the piston in a pressurization section of thick bamboo 61 rise, carry the air in a pressurization section of thick bamboo 61 in the conveyer pipe 31 through gas-supply pipe 62, gas can carry the feed liquid in the sampling tube 21 in the reation kettle body 1 through conveyer pipe two 41 this moment, and then realize through pressure device 6 in sampling tube 21 conveying gas, can insert the reation kettle body 1 again with the feed liquid in the sampling tube 21, and the liquid that stores through the liquid reserve tank 51 that sets up also can be carried in the sampling tube 21 and wash, then discharge through fluid-discharge tube 46, can avoid sampling tube 21, conveyer pipe one 31 and two 41 inner wall adhesion feed liquids of conveyer pipe.
In the description of the present invention, it should be understood that the indicated orientation or positional relationship is based on the orientation or positional relationship shown in the drawings, and is only for convenience of description and simplification of the description, and does not indicate or imply that the indicated device or element must have a particular orientation, be constructed and operated in a particular orientation, and therefore should not be construed as limiting the invention.
In the present invention, unless otherwise explicitly specified or limited, for example, it may be fixedly connected, detachably connected, or integrated; can be mechanically or electrically connected; they may be directly connected or indirectly connected through an intermediate medium, and may be connected through the inside of two elements or in an interaction relationship between two elements, unless otherwise specifically defined, and the specific meaning of the above terms in the present invention will be understood by those skilled in the art according to specific situations.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (7)
1. The utility model provides an antiseized vacuum reaction cauldron sampling device who adheres, includes reation kettle body (1), its characterized in that: a sampling device (2) is arranged on the right side of the reaction kettle body (1), an upper conveying device (3) and a lower conveying device (4) are respectively arranged on the upper side and the lower side of the sampling device (2), a liquid storage device (5) is arranged on the upper side of the upper conveying device (3), and a pressurizing device (6) is arranged on the right side of the liquid storage device (5);
the sampling device (2) comprises sampling tubes (21), butt-joint tubes (22) are fixedly arranged at the upper end and the lower end of each sampling tube (21), external threads I (23) are arranged on the outer walls of the two butt-joint tubes (22), and valves I (24) are arranged on the two butt-joint tubes (22);
the upper conveying device (3) comprises a first conveying pipe (31), the first conveying pipe (31) is communicated with the reaction kettle body (1), and a second valve (32) is arranged on one side, close to the reaction kettle body (1), of the first conveying pipe (31);
the lower conveying device (4) comprises a second conveying pipe (41), the second conveying pipe (41) is communicated with the bottom side of the reaction kettle body (1), and a fourth valve (45) is arranged on one side, close to the bottom side of the reaction kettle body (1), of the second conveying pipe (41).
2. The anti-adhesion vacuum reaction kettle sampling device as set forth in claim 1, wherein: liquid storage device (5) include liquid reserve tank (51), and the bottom intercommunication of liquid reserve tank (51) has transfer line (52) and conveyer pipe (31) intercommunication, install valve six (53) on transfer line (52), and liquid reserve tank (51) fixed set up the right side wall at reation kettle body (1).
3. The anti-adhesion vacuum reaction kettle sampling device according to claim 2, wherein: pressure device (6) are including a pressurization section of thick bamboo (61), a pressurization section of thick bamboo (61) is through two connecting rods and reation kettle body (1) fixed connection, the top side intercommunication of a pressurization section of thick bamboo (61) has gas-supply pipe (62) and conveyer pipe (31) intercommunication, seven (63) of valve are installed to the bottom of gas-supply pipe (62), the rear wall of a pressurization section of thick bamboo (61) is gone up the lower extreme and is all fixed otic placode (64) of being provided with, two the last lower extreme optical axis department rotation that otic placode (64) all pass through bearing and threaded rod (65) is connected.
4. An anti-adhesion vacuum autoclave sampling device according to claim 3, wherein: threaded connection has a screw thread section of thick bamboo (66) on threaded rod (65), screw thread section of thick bamboo (66) external fixation is provided with L shape connecting rod (68), L shape connecting rod (68) and the pull pole fixed connection of pressurization section of thick bamboo (61), the lower extreme of threaded rod (65) is fixed and is provided with rotary rod (67).
5. The anti-adhesion vacuum reaction kettle sampling device according to claim 4, wherein: the outer wall of the bottom side of the first conveying pipe (31) is provided with a second external thread (33), the second external thread (33) is in threaded connection with a first butt joint sleeve (34), and a third valve (35) is installed at a position, adjacent to the second external thread (33), on the first conveying pipe (31).
6. An anti-adhesion vacuum autoclave sampling device according to claim 5, wherein: the outer wall of the bottom side of the second conveying pipe (41) is provided with a third external thread (42), the third external thread (42) is connected with a second butting sleeve (43) in a threaded mode, a fifth valve (44) is installed at a position, adjacent to the third external thread (42), on the second conveying pipe (41), one side, close to the bottom side of the reaction kettle body (1), of the second conveying pipe (41) is provided with a liquid discharge pipe (46), and a rotary valve is installed on the liquid discharge pipe (46).
7. An anti-adhesion vacuum autoclave sampling device according to claim 6, wherein: the first butt joint sleeve (34) and the second butt joint sleeve (43) are in threaded connection with the first external threads (23) on the two butt joint pipes (22) on the upper side and the lower side respectively.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202220170556.5U CN217403876U (en) | 2022-01-21 | 2022-01-21 | Anti-adhesion vacuum reaction kettle sampling device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202220170556.5U CN217403876U (en) | 2022-01-21 | 2022-01-21 | Anti-adhesion vacuum reaction kettle sampling device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN217403876U true CN217403876U (en) | 2022-09-09 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202220170556.5U Active CN217403876U (en) | 2022-01-21 | 2022-01-21 | Anti-adhesion vacuum reaction kettle sampling device |
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| Country | Link |
|---|---|
| CN (1) | CN217403876U (en) |
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- 2022-01-21 CN CN202220170556.5U patent/CN217403876U/en active Active
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Denomination of utility model: A vacuum reaction kettle sampling device for anti adhesion Effective date of registration: 20230512 Granted publication date: 20220909 Pledgee: Bank of China Limited Huanggang branch Pledgor: Hubei Qianjia Chemical Co.,Ltd. Registration number: Y2023420000202 |