CN217163224U

CN217163224U - Separation and purification equipment for hexachloroethane mixture

Info

Publication number: CN217163224U
Application number: CN202220431600.3U
Authority: CN
Inventors: 张海鹏; 钱文进; 陈刚; 姚李亮; 胡静
Original assignee: Nantong Donggang Chemical Co ltd
Current assignee: Nantong Donggang Chemical Co ltd
Priority date: 2022-03-01
Filing date: 2022-03-01
Publication date: 2022-08-12
Anticipated expiration: 2032-03-01

Abstract

The utility model discloses a separation and purification device of hexachloroethane mixture, a tank body is transversely erected in the tank body, two ends of the tank body are connected with side plates, a bracket is arranged on the lower surface of the tank body, a heating coil is arranged in the tank body, the heating coil is sleeved outside the tank body, a filter is arranged at the middle position in the tank body, a filter core is arranged in the filter, the upper surface of the filter is connected with a discharge port through a hose, the discharge port is arranged on the upper surface of the tank body, a main shaft is erected in the tank body, a stirrer is arranged on the main shaft, the stirrer is positioned at the filter and is provided with a recess, the recessed position is matched with the position of the filter, the structure of the utility model is reasonable, the stirrer is arranged in the tank body, the vaporization efficiency of hexachloroethane is improved through the stirrer, the filter is arranged at the top end in the tank body and is connected with the discharge port through the filter, the vaporized hexachloroethane is filtered, the purity of hexachloroethane is ensured while the efficiency is improved.

Description

Separation and purification equipment for hexachloroethane mixture

Technical Field

The utility model relates to a separation and purification equipment technical field specifically is a separation and purification equipment of hexachloroethane mixture.

Background

At present, the separation and purification equipment for hexachloroethane mixture generally adopts a steam heating standing mode for purification treatment, the efficiency is low, and the production efficiency of the whole hexachloroethane is influenced, so that an improved technology is urgently needed to solve the problem in the prior art.

SUMMERY OF THE UTILITY MODEL

An object of the utility model is to provide a separation and purification equipment of hexachloroethane mixture owing to be provided with the agitator to improve vaporization efficiency, but the stirring process is also taken up particulate impurity easily, consequently sets up the filter, filters with the cooperation, has still guaranteed product purity when improving efficiency, with the problem of proposing in solving above-mentioned background art.

In order to achieve the above object, the utility model provides a following technical scheme: a separation and purification device for a hexachloroethane mixture comprises a bin body, a support, a motor, heating coils, a filter, a main shaft and a stirrer, wherein the two ends of the bin body are provided with side plates, the outer side of any one of the side plates is provided with the motor, the bin body is transversely erected in the bin body, the two ends of the bin body are connected with the side plates, the support is arranged on the lower surface of the bin body, the heating coils are arranged in the bin body and sleeved outside the bin body, the two ends of each heating coil are respectively connected with a joint, the joints are arranged on the surface of the bin body, the filter is arranged in the middle of the interior of the bin body, a filter element is arranged in the filter, the upper surface of the filter is connected with a discharge port through a hose, the discharge port is arranged on the upper surface of the bin body, the upper surface of the bin body is also provided with a gas exhaust port, and the lower surface of the bin body is provided with a condensate liquid discharge port, the upper surface of one side of the tank body is also provided with a feed inlet, one side of the bottom end of the tank body is provided with a waste discharge port, the feed inlet is arranged on the upper surface of the bin body in a penetrating manner, the waste discharge port is arranged on the lower surface of the bin body in a penetrating manner, a main shaft is erected in the tank body, the main shaft is provided with a stirrer, the stirrer is positioned at the filter and provided with a recess, the position of the recess is matched with that of the filter, and one end of the main shaft is arranged at the end part of the tank body in a penetrating manner and is connected with a motor;

the filter comprises a shell, a connecting plate, a connecting sleeve and a bottom cover, wherein the connecting plate is arranged on the upper surface of the shell, the connecting sleeve is arranged on the upper surface of the connecting plate, the bottom end of the hose is connected with the connecting sleeve, the bottom cover is arranged on the lower surface of the shell, the filter element is arranged in the shell, and through grooves are formed in the shell and the bottom cover.

Preferably, the utility model provides a pair of separation and purification equipment of hexachloroethane mixture, wherein, the mounting groove has been seted up to the intermediate position of jar body upper surface, the filter passes through the bolt and sets up in mounting groove department to realize the installation and the dismantlement of filter.

Preferably, the utility model provides a pair of separation and purification equipment of hexachloroethane mixture, wherein, storehouse body upper surface still is provided with a plurality of access doors to be convenient for the maintenance of storehouse internal portion and the change of filter.

Preferably, the utility model provides a pair of separation and purification equipment of hexachloroethane mixture, wherein, feed inlet, discharge gate and waste discharge opening all are provided with the valve to realize the switching control of feed inlet, discharge gate and waste discharge opening.

Preferably, the utility model provides a pair of separation and purification equipment of hexachloroethane mixture, wherein, the motor supports in the motor cabinet upper surface, motor cabinet one end links to each other with the curb plate that corresponds to guarantee the stability of motor.

Compared with the prior art, the beneficial effects of the utility model are that:

(1) the filter is arranged at the top end of the inner part of the tank body and is connected with the discharge hole through the filter, and the obtained vaporized hexachloroethane is filtered, so that the purity of hexachloroethane is greatly improved.

(2) The filter is arranged in the tank body, so that an external filter is not needed, and the space is saved while the filter is convenient to mount and dismount.

(3) Jar internal portion is provided with the agitator, and the agitator intermediate position sets up also to have sunken in order to avoid the filter, has improved the vaporization efficiency of hexachloroethane through the agitator.

Drawings

Fig. 1 is a schematic structural view of the present invention;

FIG. 2 is a schematic view of the filter portion of the present invention;

in the figure: the device comprises a bin body 1, a bin body 2, a support 3, a motor 4, a heating coil 5, a filter 6, a main shaft 7, a stirrer 8, a side plate 9, a joint 10, a filter element 11, a hose 12, a discharge hole 13, an exhaust port 14, a condensate liquid discharge port 15, a feed inlet 16, a waste discharge port 17, an access door 18, a motor base 19, a shell 601, a connecting plate 602, a connecting sleeve 603 and a bottom cover 604.

Detailed Description

The technical solution of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments of the present invention, all other embodiments obtained by those skilled in the art without creative efforts belong to the protection scope of the present invention;

it should be noted that, in the description of the present invention, it is to be noted that the terms "inside", "outside", "upper", "lower", "both sides", "one end", "the other end", "left", "right", and the like indicate the directions or positional relationships based on the directions or positional relationships shown in the drawings, and are only for convenience of description and simplification of the present invention, and do not indicate or imply that the device or element referred to must have a specific direction, be constructed and operated in a specific direction, and thus, should not be construed as limiting the present invention.

Referring to fig. 1-2, the present invention provides a technical solution: a separation and purification device for a hexachloroethane mixture comprises a bin body 1, a bin body 2, a support 3, a motor 4, a heating coil 5, a filter 6, a main shaft 7 and a stirrer 8, wherein side plates 9 are arranged at two ends of the bin body 1, the motor 4 is arranged on the outer side of any one side plate 9, the motor 4 is supported on the upper surface of a motor base 19, one end of the motor base 19 is connected with the corresponding side plate 9, the bin body 2 is transversely erected in the bin body 1, two ends of the bin body 2 are connected with the side plates 9, the support 3 is arranged on the lower surface of the bin body 1, the heating coil 5 is arranged in the bin body 1, the heating coil 5 is sleeved outside the bin body 2, two ends of the heating coil 5 are respectively connected with a joint 10, the joint 10 is arranged on the surface of the bin body 1, the filter 6 is arranged in the middle position of the inner part of the bin body 2, the filter 6 is arranged in the installation groove through a bolt, a filter element 11 is arranged in the filter 6, the upper surface of the filter 6 is connected with a discharge port 13 through a hose 12, the discharge port 13 is arranged on the upper surface of the bin body 1, the upper surface of the bin body 1 is also provided with an exhaust port 14, the lower surface of the bin body 1 is provided with a condensate liquid discharge port 15, the upper surface of one side of the bin body 2 is also provided with a feed inlet 16, one side of the bottom end of the bin body 2 is provided with a waste discharge port 17, the feed inlet 16 is arranged on the upper surface of the bin body 1 in a penetrating way, the waste discharge port 17 is arranged on the lower surface of the bin body 1 in a penetrating way, a main shaft 7 is erected in the bin body 2, the main shaft 7 is provided with a stirrer 8, the stirrer 8 is arranged at the position of the filter 6 and is provided with a recess, the position of the recess is matched with the position of the filter 6, one end of the main shaft 7 is arranged at the end part of the bin body 2 in a penetrating way and is connected with the motor 4, the upper surface of the bin body 1 is also provided with a plurality of access doors 18 and the feed inlet 16, the discharge port 13 and the waste discharge port 17 are provided with valves;

the filter 6 comprises a shell 601, a connecting plate 602, a connecting sleeve 603 and a bottom cover 604, wherein the connecting plate 602 is arranged on the upper surface of the shell 601, the connecting sleeve 603 is arranged on the upper surface of the connecting plate 602, the bottom end of the hose 12 is connected with the connecting sleeve 603, the bottom cover 604 is arranged on the lower surface of the shell 601, the filter element 11 is arranged in the shell 601, and through grooves are formed in the shell 601 and the bottom cover 604.

The installation method and the use principle are as follows: firstly, the stirrer 8 and the main shaft 7 are installed in the tank body 2, and then the conical end covers at the two ends of the tank body 2 are covered to complete the installation of the tank body 2. One of them curb plate 9 is fixed in 1 one end in the storehouse body earlier afterwards, establish the coil cover at the 2 outsides of jar body again, place jar body 2 in the storehouse body 1, and with jar 2 front end fixed in curb plate 9, install the curb plate 9 of the other end afterwards, link to each other jar body 2 rear end and the curb plate 9 of back installation simultaneously, accomplish jar body 2 fixed, install motor 4 on corresponding curb plate 9 afterwards, and support on the motor cabinet 19 of corresponding curb plate 9, link to each other the output shaft of main shaft 7 extension through shaft coupling and motor 4 simultaneously. And finally, the feed inlet 16 and the waste discharge port 17 are respectively connected with the tank body 2, the filter 6 is arranged in the mounting groove on the upper surface of the tank body 2 and is connected with the discharge port 13 through the high-temperature resistant hose 12, and the mounting is finished. When the device is used, a hexachloroethane mixture is fed into the tank body 2 from the feeding hole 16, the stirrer 8 and the heating coil 5 are started, the interior of the tank body 2 is heated to 100-130 degrees, steam is discharged from the discharging hole 13 after passing through the filter 6, and hexachloroethane is obtained after subsequent cooling and crystallization processes. Owing to be provided with agitator 6 to improve vaporization efficiency, but the stirring process is also taken up particulate impurity easily, consequently sets up the filter, filters with the cooperation, has still guaranteed product purity when improving efficiency. The utility model has reasonable structure, the top end in the tank body 2 is provided with the filter 6, the filter 6 is connected with the discharge hole 13, and the obtained vaporized hexachloroethane is filtered, thereby greatly improving the purity of hexachloroethane; the filter 6 is arranged in the tank body 2, so that the filter 6 does not need to be externally connected, the installation and the disassembly are convenient, and the space is saved; the inside agitator 8 that is provided with of

jar body

2, and 8 intermediate positions of agitator set up and also have sunken in order to avoid filter 6, have improved the vaporization efficiency of hexachloroethane through agitator 8.

The details of the present invention are well known to those skilled in the art.

Finally, it is to be noted that: the above embodiments are only used for illustrating the technical solutions of the present invention and not for limiting, and although the present invention has been described in detail with reference to the examples, it should be understood by those skilled in the art that the technical solutions of the present invention can be modified and replaced with equivalents without departing from the spirit and scope of the technical solutions of the present invention, which should be covered by the scope of the claims of the present invention.

Claims

1. A separation and purification equipment for hexachloroethane mixture is characterized in that: comprises a bin body (1), a bin body (2), a support (3), a motor (4), a heating coil (5), a filter (6), a main shaft (7) and a stirrer (8), wherein side plates (9) are arranged at the two ends of the bin body (1), the motor (4) is arranged on the outer side of any one of the side plates (9), the bin body (2) is transversely erected inside the bin body (1), the two ends of the bin body (2) are connected with the side plates (9), the support (3) is arranged on the lower surface of the bin body (1), the heating coil (5) is arranged inside the bin body (1), the heating coil (5) is sleeved outside the bin body (2), the two ends of the heating coil (5) are respectively connected with a joint (10), the joint (10) is arranged on the surface of the bin body (1), the filter (6) is arranged at the middle position inside the bin body (2), the filter is characterized in that a filter element (11) is arranged inside the filter (6), the upper surface of the filter (6) is connected with a discharge port (13) through a hose (12), the discharge port (13) is arranged on the upper surface of the bin body (1), an exhaust port (14) is further arranged on the upper surface of the bin body (1), a condensate liquid discharge port (15) is arranged on the lower surface of the bin body (1), a feed inlet (16) is further arranged on the upper surface of one side of the bin body (2), a waste discharge port (17) is arranged on one side of the bottom end of the bin body (2), the feed inlet (16) is arranged on the upper surface of the bin body (1), the waste discharge port (17) is arranged on the lower surface of the bin body (1), a main shaft (7) is erected inside the bin body (2), a stirrer (8) is arranged on the main shaft (7), a recess is arranged at the position of the stirrer (8) on the filter (6), and the recessed position is matched with the position of the filter (6), one end of the main shaft (7) penetrates through the end part of the tank body (2) and is connected with the motor (4);

the filter (6) comprises a shell (601), a connecting plate (602), a connecting sleeve (603) and a bottom cover (604), wherein the connecting plate (602) is arranged on the upper surface of the shell (601), the connecting sleeve (603) is arranged on the upper surface of the connecting plate (602), the bottom end of the hose (12) is connected with the connecting sleeve (603), the bottom cover (604) is arranged on the lower surface of the shell (601), the filter element (11) is arranged in the shell (601), and the shell (601) and the bottom cover (604) are both provided with through grooves.

2. The apparatus for separating and purifying hexachloroethane mixture according to claim 1, wherein: the mounting groove has been seted up to the intermediate position of jar body (2) upper surface, filter (6) pass through the bolt and set up in mounting groove department.

3. The apparatus for separating and purifying hexachloroethane mixture according to claim 1, wherein: the upper surface of the bin body (1) is also provided with a plurality of access doors (18).

4. The apparatus for separating and purifying hexachloroethane mixture according to claim 1, wherein: the feed inlet (16), the discharge outlet (13) and the waste discharge outlet (17) are all provided with valves.

5. The apparatus for separating and purifying hexachloroethane mixture according to claim 1, wherein: the motor (4) is supported on the upper surface of the motor base (19), and one end of the motor base (19) is connected with the corresponding side plate (9).