CN217114308U - Ionization ultraviolet lamp protection and sealing structure of integrated ion mobility spectrometer - Google Patents
Ionization ultraviolet lamp protection and sealing structure of integrated ion mobility spectrometer Download PDFInfo
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- CN217114308U CN217114308U CN202220481474.2U CN202220481474U CN217114308U CN 217114308 U CN217114308 U CN 217114308U CN 202220481474 U CN202220481474 U CN 202220481474U CN 217114308 U CN217114308 U CN 217114308U
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- ultraviolet lamp
- ionization
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- sleeve
- ion mobility
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- 238000007789 sealing Methods 0.000 title claims abstract description 61
- 239000011521 glass Substances 0.000 claims abstract description 59
- 230000003287 optical effect Effects 0.000 claims abstract description 40
- 239000012790 adhesive layer Substances 0.000 claims abstract description 10
- -1 polyoxymethylene Polymers 0.000 claims description 10
- 230000001846 repelling effect Effects 0.000 claims description 7
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 6
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 4
- 229910052802 copper Inorganic materials 0.000 claims description 4
- 239000010949 copper Substances 0.000 claims description 4
- 239000011810 insulating material Substances 0.000 claims description 4
- 239000007769 metal material Substances 0.000 claims description 4
- 229930040373 Paraformaldehyde Natural products 0.000 claims description 3
- 229910052782 aluminium Inorganic materials 0.000 claims description 3
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 3
- 229910052742 iron Inorganic materials 0.000 claims description 3
- 229920006324 polyoxymethylene Polymers 0.000 claims description 3
- 229910001220 stainless steel Inorganic materials 0.000 claims description 3
- 239000010935 stainless steel Substances 0.000 claims description 3
- BFKJFAAPBSQJPD-UHFFFAOYSA-N tetrafluoroethene Chemical group FC(F)=C(F)F BFKJFAAPBSQJPD-UHFFFAOYSA-N 0.000 claims description 3
- 239000004677 Nylon Substances 0.000 claims description 2
- 239000004698 Polyethylene Substances 0.000 claims description 2
- 229920001778 nylon Polymers 0.000 claims description 2
- 229920000515 polycarbonate Polymers 0.000 claims description 2
- 239000004417 polycarbonate Substances 0.000 claims description 2
- 229920000573 polyethylene Polymers 0.000 claims description 2
- 229920000122 acrylonitrile butadiene styrene Polymers 0.000 claims 1
- 235000021110 pickles Nutrition 0.000 claims 1
- 150000002500 ions Chemical class 0.000 description 24
- 238000001871 ion mobility spectroscopy Methods 0.000 description 6
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- 239000007789 gas Substances 0.000 description 4
- 238000001228 spectrum Methods 0.000 description 4
- 238000012546 transfer Methods 0.000 description 4
- 239000011261 inert gas Substances 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- RLLPVAHGXHCWKJ-IEBWSBKVSA-N (3-phenoxyphenyl)methyl (1s,3s)-3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropane-1-carboxylate Chemical compound CC1(C)[C@H](C=C(Cl)Cl)[C@@H]1C(=O)OCC1=CC=CC(OC=2C=CC=CC=2)=C1 RLLPVAHGXHCWKJ-IEBWSBKVSA-N 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
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- ORUIBWPALBXDOA-UHFFFAOYSA-L magnesium fluoride Chemical compound [F-].[F-].[Mg+2] ORUIBWPALBXDOA-UHFFFAOYSA-L 0.000 description 1
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Abstract
The utility model discloses an integral type ion mobility spectrometer's ionization ultraviolet lamp protection and seal structure, including lamp sleeve, ionization ultraviolet lamp, sealing washer and the repulsion utmost point of taking the seal groove. The adhesive layer is arranged between the inner end face of the hollow limiting end of the integrated glass light window and the outer edge of the glass light window of the ionization ultraviolet lamp, the ionization ultraviolet lamp is inserted into the lamp sleeve with the external thread until the inner end face of the hollow limiting end of the integrated glass light window, the ionization ultraviolet lamp is bonded and fixed in the lamp sleeve with the external thread through the adhesive layer, a new sleeve-type ionization ultraviolet lamp assembly is formed, and the ionization ultraviolet lamp is protected. The utility model provides an integral type ion mobility spectrometer's ionization ultraviolet lamp protection and seal structure has characteristics such as the leakproofness is good, the reliability is high, the practicality is strong, can protect ionization ultraviolet lamp glass optical window effectively to realize with the sealed between the ion mobility tube cavity.
Description
Technical Field
The utility model relates to a non-radioactive lamp electric ion source of ion mobility spectrometry, especially integral type ion mobility spectrometry's ionization ultraviolet lamp protection and seal structure.
Background
Ion Mobility Spectrometry (IMS) is a technique for analyzing chemical substances by ionizing gas-phase molecules with an ionization source and by using the difference in migration velocity between different gas-phase ions in the same electric field, and has been widely used in the field for rapidly screening and detecting explosives, drugs, and toxicants.
The ionization ultraviolet lamp is a single photon ultraviolet light emission source, mainly comprising a lamp body, an optical window and electrodes, wherein the lamp is vacuumized and then filled with inert gas, and ultraviolet rays with the luminous energy of 8-12eV (about 150-110nm) are obtained by excitation of direct current high voltage or radio frequency high voltage; the glass optical window is made of magnesium fluoride material and can transmit ultraviolet light, and the transmission optical path of the ultraviolet light in the air is generally within 1 cm; organic matters in the air environment outside the glass optical window (generally, the ionization energy is 7-10eV, and for the organic matters with the ionization energy larger than 10eV, a dopant acetone with low ionization energy can be provided to assist ionization) are ionized into ions by ultraviolet light for analysis.
The assembly of the ionization ultraviolet lamp aims at realizing the sealing between the glass optical window and the cavity of the ion transfer tube, particularly the metal repelling electrode, a sealing groove and a sealing ring are usually arranged on the metal repelling electrode, and then the edge between the glass optical window and the ionization ultraviolet lamp body is pushed by a glass optical window limiting groove on a lamp sleeve with external threads, so that the sealing between the glass optical window and the metal repelling electrode is realized by the sealing ring. In actual operation, two problems occur, namely, the sealing ring is aged and thinned, so that the glass optical window is broken or damaged when contacting with a sealing groove of a metal repelling electrode; secondly, the glass optical window limiting groove on the lamp sleeve has overlarge ejection force, so that the glass optical window is damaged or even separated, and the assembly reliability and the service life of the ionization ultraviolet lamp are seriously influenced.
Gajiayi et al invented a method for assembling an ultraviolet lamp in an ion mobility spectrometry device and an ion mobility spectrometry device (patent No. ZL201210049161.0), wherein the ultraviolet lamp is horizontally arranged at the front end of an ionization region of an ion mobility tube, and an ionization channel with the width of 4mm is reserved in front of an ultraviolet window, so that the ionization region is kept complete and the movement direction of ions cannot be deviated when the ions pass through the ionization region.
The invention discloses a radio frequency ionization excitation device of a vacuum ultraviolet lamp (patent number ZL201420732503.3) invented by plum sea and the like, and the radio frequency ionization excitation device of the vacuum ultraviolet lamp is designed, wherein a cavity of the vacuum ultraviolet lamp is filled with inert gas, and after the inert gas is ionized and broken down through the ionization excitation device, light with a specific wavelength can be emitted through a light window. The device has small volume and compact structure, and is suitable for ionization excitation of a vacuum ultraviolet lamp ionization source in an ion mobility spectrometer.
The invention discloses an ion migration tube (patent No. ZL202023012576.X) capable of prolonging the service life of a photoionization source, and discloses an ion migration tube capable of prolonging the service life of the photoionization source, which comprises a vacuum ultraviolet lamp and an anti-reflection glass window, wherein the two components are coaxially arranged, ultraviolet light generated by the vacuum ultraviolet lamp is vertically emitted to the surface of the anti-reflection glass window, the vacuum ultraviolet lamp is isolated from an ionization region cavity of the migration tube by the anti-reflection glass window, and the anti-reflection glass is easy to replace, so that the effect of reducing the pollution of the vacuum ultraviolet lamp window is achieved.
The invention discloses an integrated vacuum ultraviolet lamp ionization source differential ion mobility spectrometer (patent number ZL201611041188.x) invented by Liyang et al, which comprises a differential ion mobility spectrum, an ultraviolet lamp ionization source and a fixed groove, wherein all carrier gas between two parallel migration polar plates of the differential ion mobility spectrum horizontally enters the migration polar plates through a gas inlet, and all gas is completely discharged through a horizontal gas outlet, so that the sealing problem of the differential ion mobility spectrum is solved, the gas flow of the differential ion mobility spectrum is stable, and the detection reliability is ensured.
In summary, none of the above inventions and prior art designs address the specific assembly and problems that can occur with ionizing ultraviolet lamps.
SUMMERY OF THE UTILITY MODEL
To the technical problem, the utility model provides an ionization ultraviolet lamp protection and seal structure of integral type ion mobility spectrometer has advantages such as the leakproofness is good, the reliability is high, the practicality is strong.
The utility model discloses technical scheme as follows:
the protection and sealing structure of the ionization ultraviolet lamp of the integrated ion mobility spectrometer comprises a lamp sleeve, the ionization ultraviolet lamp, a sealing ring and a repeller with a sealing groove;
the ionization ultraviolet lamp comprises an ionization ultraviolet lamp body, two symmetrical radio-frequency electrode plates are attached to the outer wall of the ionization ultraviolet lamp body, and the electrode plates are respectively led out by two conducting wires and connected with a high-voltage radio-frequency power supply; one end of the ionizing ultraviolet lamp body is provided with an ionizing ultraviolet lamp glass optical window, and the outer diameter of the ionizing ultraviolet lamp glass optical window is larger than that of the ionizing ultraviolet lamp body stuck with the symmetrical radio-frequency electrode plates;
the lamp sleeve is a hollow cylinder and is nested outside the ionization ultraviolet lamp, and the inner diameter of the lamp sleeve is slightly larger than the outer diameter of a glass light window of the ionization ultraviolet lamp; one end of the lamp sleeve is provided with an integrated glass optical window hollow limiting end, the inner diameter of the hollow part of the hollow limiting end is equal to that of the ionization ultraviolet lamp body, and ultraviolet light emitted from the ultraviolet lamp glass optical window passes through the hollow part; the other end of the lamp sleeve is provided with two electrode wire leading-out holes for leading out wires connected with two symmetrical radio frequency electrode plates;
an adhesive layer is arranged between the inner end face of the hollow limiting end, the inner wall of the lamp sleeve part, the partial lamp body of the ionization ultraviolet lamp and the outer edge of the glass optical window of the ionization ultraviolet lamp, the ionization ultraviolet lamp is inserted into the lamp sleeve until reaching the inner end face of the hollow limiting end, the outer edge of the glass optical window of the ionization ultraviolet lamp, the partial lamp body of the ionization ultraviolet lamp and the inner wall of the lamp sleeve part are bonded and sealed through the adhesive layer, the ionization ultraviolet lamp is bonded and fixed in the lamp sleeve with the external threads, and a novel sleeve type ionization ultraviolet lamp assembly is formed to protect the ionization ultraviolet lamp;
the sleeve type ionizing ultraviolet lamp assembly is tightly attached to a repeller with a sealing groove through the outer end face of the hollow limiting end of the integrated glass light window, a sealing ring is arranged at the attaching position, and the sealing ring is embedded into the sealing groove of the repeller, so that the ionization ultraviolet lamp and the ion transfer tube cavity are sealed and used.
Preferably, the inner diameter of the sealing ring is slightly larger than the inner diameter of the ionization ultraviolet lamp body, and the outer diameter of the sealing ring is slightly smaller than the outer diameter of the outer end face of the hollow limiting end.
Preferably, the inner diameter of the lamp sleeve is 0.1-1mm larger than the outer diameter of the glass light window of the ionizing ultraviolet lamp.
Preferably, the outer diameter of the outer end face of the hollow limiting end of the integrated glass optical window is 0.1-10mm smaller than the outer diameter of the screw thread of the lamp sleeve with the external screw thread.
Preferably, the thickness of the glass optical window of the ionization ultraviolet lamp is 0.5-2 mm.
Preferably, the inner diameter of the sealing ring is 0.1-1mm larger than the inner diameter of the ionizing ultraviolet lamp body; the outer diameter of the sealing ring is 0.1-10mm smaller than the outer diameter of the screw thread of the lamp sleeve with the external screw thread.
Preferably, the repelling electrode with the sealing groove is a metallic material, such as stainless steel, such as iron, such as aluminum, such as copper, or the like.
Preferably, two symmetrical RF electrode plates made of metal, such as copper, such as aluminum, such as iron, are attached to the outer wall of the ionizing ultraviolet lamp body.
Preferably, the lamp sleeve is made of an insulating material, such as tetrafluoroethylene, such as pek, ABS, such as nylon, such as Polyoxymethylene (POM), such as polyethylene, such as polycarbonate, or the like.
Advantageous effects
The utility model provides an ionization ultraviolet lamp protection and sealing structure of an integrated ion mobility spectrometer, by arranging the hollow limiting end of the integrated glass light window at one end of the lamp sleeve and arranging the adhesive layer between the inner end surface of the hollow limiting end and the outer edge of the glass light window of the ionization ultraviolet lamp, the inner end face of the hollow limiting end, the outer edge of the glass optical window of the ionization ultraviolet lamp, the partial lamp body of the ionization ultraviolet lamp and the inner wall of the lamp sleeve part are bonded and sealed through the adhesive layer, the ionization ultraviolet lamp is bonded and fixed in the lamp sleeve with the external thread to form a novel sleeve type ionization ultraviolet lamp assembly, the protection of the ionization ultraviolet lamp is realized, the novel sleeve type ionization ultraviolet lamp assembly has the advantages of good sealing performance, high reliability, strong practicability and the like, and the problems of damage, breakage and separation of the glass optical window are solved, the glass optical window of the ionization ultraviolet lamp can be effectively protected, and the sealing between the glass optical window and the cavity of the ion transfer tube is realized.
Drawings
Fig. 1 is an explosion diagram of the protection and sealing structure of the ionization ultraviolet lamp of the integrated ion mobility spectrometer of the present invention;
FIG. 2 is a schematic view of an original ionizing ultraviolet lamp assembly;
in the figure, 1-electrode wire leading-out hole; 2-a lamp sleeve; 3-lamp glass light window limiting groove; 4-symmetrical radio frequency electrode plates; 5-ionizing the ultraviolet lamp body; 6-ionizing ultraviolet lamp glass optical window; 7-hollow limiting end of the integrated glass light window; 8-sealing ring; 9-repeller with sealing slot; 10-external thread.
Detailed Description
Example 1
An ionization ultraviolet lamp protection and sealing structure of an integrated ion mobility spectrometer comprises a lamp sleeve 2 with external threads 10, an ionization ultraviolet lamp, a sealing ring 8 and a repeller 9 with a sealing groove.
The ionization ultraviolet lamp comprises a cylindrical ionization ultraviolet lamp body 5, and one end of the ionization ultraviolet lamp body 5 is provided with a circular ionization ultraviolet lamp glass light window 6; two symmetrical radio frequency electrode plates 4 are pasted on the outer wall of the ionization ultraviolet lamp body 5, and the electrode plates are respectively led out by two wires and connected with a radio frequency power supply; the outer diameter of the glass light window 6 of the ionization ultraviolet lamp is larger than that of the lamp body of the ionization ultraviolet lamp stuck with the symmetrical radio-frequency electrode plate 4.
The lamp sleeve 2 with the external threads is a hollow cylinder and is nested outside the ionization ultraviolet lamp, and the inner diameter of the lamp sleeve 2 with the external threads is slightly larger than the outer diameter of the glass optical window 6 of the ionization ultraviolet lamp; the end face of one end of the lamp sleeve 2 is provided with an integrated glass optical window hollow limiting end 7, the inner diameter of the hollow part of the hollow limiting end 7 is equal to the inner diameter of the ionization ultraviolet lamp body 5, ultraviolet light emitted from the ultraviolet lamp glass optical window 6 can pass through the hollow limiting end, and the external thread 10 is positioned on the side face of one end of the lamp sleeve 2, which is provided with the hollow limiting end 7; the side surface of the other end of the lamp sleeve 2 with external threads is provided with two electrode wire leading-out holes 1 for leading out wires connected with two symmetrical radio-frequency electrode plates 4.
An adhesive layer is arranged between the inner end face of the hollow limiting end 7 of the integrated glass light window, part of the inner wall of the lamp sleeve 2, part of the lamp body of the ionization ultraviolet lamp 5 and the outer edge of the glass light window of the ionization ultraviolet lamp 6, the ionization ultraviolet lamp is inserted into the lamp sleeve 2 until the inner end face of the hollow limiting end 7, the outer edge of the glass light window of the ionization ultraviolet lamp 6, part of the lamp body of the ionization ultraviolet lamp and the inner wall of the lamp sleeve part are bonded and sealed through the adhesive layer (in detail, the thickened part of the line shown in figure 1), the ionization ultraviolet lamp is bonded and fixed in the lamp sleeve 2 with the external thread, a new sleeve type ionization ultraviolet lamp is formed, and the protection of the ionization ultraviolet lamp is realized.
The sleeve type ionizing ultraviolet lamp assembly is tightly attached to a repeller 9 with a sealing groove through the outer end face of an integrated glass light window hollow limiting end 7, a sealing ring 8 is arranged at the attaching position, and the sealing ring 8 is embedded into the sealing groove of the repeller, so that the ionization ultraviolet lamp and an ion transfer tube cavity are sealed and used. The inner diameter of the sealing ring 8 is slightly larger than the inner diameter of the ionization ultraviolet lamp body 5, and the outer diameter of the sealing ring 8 is slightly smaller than the outer end surface outer diameter of the hollow limiting end 7 of the integrated glass optical window.
Wherein,
the inner diameter of the lamp sleeve 2 with external threads is 0.1mm larger than the outer diameter of the glass optical window 6 of the ionization ultraviolet lamp;
the outer diameter of the outer end face of the hollow limiting end 7 of the integrated glass optical window is 0.1mm smaller than the outer diameter of the thread of the lamp sleeve 2 with the external thread;
the thickness of the glass optical window 6 of the ionization ultraviolet lamp is 1.2 mm;
the inner diameter of the sealing ring 8 is 0.1mm larger than the inner diameter of the ionizing ultraviolet lamp body 5; the outer diameter of the sealing ring 8 is 0.1mm smaller than the outer diameter of the thread of the lamp sleeve 2 with the external thread;
the repeller 9 with the seal groove is a metal material, such as stainless steel;
the outer wall of the ionization ultraviolet lamp body 5 is pasted with two symmetrical radio frequency electrode plates 4 made of metal, such as copper;
the lamp sleeve 2 is made of an insulating material, such as tetrafluoroethylene, e.g., picket, etc., and has an external thread.
Claims (10)
1. An ionization ultraviolet lamp protection and sealing structure of an integrated ion mobility spectrometer is characterized by comprising a lamp sleeve, an ionization ultraviolet lamp, a sealing ring and a repeller with a sealing groove;
the ionization ultraviolet lamp comprises an ionization ultraviolet lamp body, two symmetrical radio frequency electrode plates are attached to the outer wall of the ionization ultraviolet lamp body, and the electrode plates are respectively led out by two wires and connected with a high-voltage radio frequency power supply; one end of the ionizing ultraviolet lamp body is provided with an ionizing ultraviolet lamp glass optical window, and the outer diameter of the ionizing ultraviolet lamp glass optical window is larger than that of the ionizing ultraviolet lamp body stuck with the symmetrical radio-frequency electrode plates;
the lamp sleeve is a hollow cylinder and is nested outside the ionization ultraviolet lamp, and the inner diameter of the lamp sleeve is slightly larger than the outer diameter of a glass light window of the ionization ultraviolet lamp; one end of the lamp sleeve is provided with an integrated glass optical window hollow limiting end, the inner diameter of the hollow part of the hollow limiting end is equal to that of the ionization ultraviolet lamp body, and ultraviolet light emitted from the ultraviolet lamp glass optical window passes through the hollow part; the other end of the lamp sleeve is provided with two electrode wire leading-out holes for leading out wires connected with two symmetrical radio frequency electrode plates;
an adhesive layer is arranged between the inner end face of the hollow limiting end, the inner wall of the lamp sleeve part, the ionization ultraviolet lamp part lamp body and the outer edge of the glass optical window of the ionization ultraviolet lamp, the ionization ultraviolet lamp is inserted into the lamp sleeve until reaching the inner end face of the hollow limiting end, and the inner end face of the hollow limiting end, the outer edge of the glass optical window of the ionization ultraviolet lamp, the lamp body of the ionization ultraviolet lamp part and the inner wall of the lamp sleeve part are bonded and sealed through the adhesive layer; the outer end face of the hollow limiting end is tightly attached to the repelling electrode with the sealing groove, a sealing ring is arranged at the attaching position, and the sealing ring is embedded into the sealing groove of the repelling electrode.
2. The protection and sealing structure for the ionization ultraviolet lamp of the integrated ion mobility spectrometer of claim 1, wherein: the inner diameter of the sealing ring is slightly larger than the inner diameter of the ionization ultraviolet lamp body, and the outer diameter of the sealing ring is slightly smaller than the outer end face outer diameter of the hollow limiting end.
3. The protection and sealing structure for the ionization ultraviolet lamp of the integrated ion mobility spectrometer of claim 1, wherein: the inner diameter of the lamp sleeve is 0.1-1mm larger than the outer diameter of the glass optical window of the ionization ultraviolet lamp.
4. The protection and sealing structure for the ionization ultraviolet lamp of the integrated ion mobility spectrometer of claim 1, wherein: the outer diameter of the outer end face of the hollow limiting end is 0.1-10mm smaller than the outer diameter of the screw thread of the lamp sleeve with the external screw thread.
5. The integrated ion mobility spectrometer's ionizing ultraviolet lamp protection and sealing structure according to claim 1, characterized in that: the thickness of the glass optical window of the ionization ultraviolet lamp is 0.5-2 mm.
6. The protection and sealing structure for the ionization ultraviolet lamp of the integrated ion mobility spectrometer of claim 2, wherein: the inner diameter of the sealing ring is 0.1-1mm larger than the inner diameter of the ionizing ultraviolet lamp body; the outer diameter of the sealing ring is 0.1-10mm smaller than the outer diameter of the screw thread of the lamp sleeve.
7. The protection and sealing structure for the ionization ultraviolet lamp of the integrated ion mobility spectrometer of claim 1, wherein: the repeller with the sealing groove and the two symmetrical radio-frequency electrode plates are made of metal materials.
8. The protection and sealing structure for the ionizing ultraviolet lamp of the integrated ion mobility spectrometer of claim 7, wherein: the metal material is one of stainless steel, iron, aluminum and copper.
9. The protection and sealing structure for the ionization ultraviolet lamp of the integrated ion mobility spectrometer of claim 1, wherein: the lamp sleeve is made of insulating materials.
10. The protection and sealing structure for the ionization ultraviolet lamp of the integrated ion mobility spectrometer of claim 9, wherein: the insulating material is one of tetrafluoroethylene, pickles, ABS, nylon, polyoxymethylene, polyethylene and polycarbonate.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN202220481474.2U CN217114308U (en) | 2022-03-07 | 2022-03-07 | Ionization ultraviolet lamp protection and sealing structure of integrated ion mobility spectrometer |
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CN202220481474.2U CN217114308U (en) | 2022-03-07 | 2022-03-07 | Ionization ultraviolet lamp protection and sealing structure of integrated ion mobility spectrometer |
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CN217114308U true CN217114308U (en) | 2022-08-02 |
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