CN216799809U

CN216799809U - High temperature reaction cauldron convenient to ration sample

Info

Publication number: CN216799809U
Application number: CN202123136107.3U
Authority: CN
Inventors: 梁鹏
Original assignee: Foshan Shunde Lanying Silica Material Co ltd
Current assignee: Foshan Shunde Lanying Silica Material Co ltd
Priority date: 2021-12-13
Filing date: 2021-12-13
Publication date: 2022-06-24
Anticipated expiration: 2031-12-13

Abstract

The utility model discloses a high-temperature reaction kettle convenient for quantitative sampling, which comprises a reaction kettle, wherein a protective sleeve is fixedly sleeved on the outer wall of the reaction kettle, a sampling chamber is fixedly arranged on the side surface of the protective sleeve through a bolt, the sampling chamber is hermetically communicated with a sampling tube which penetrates through and extends to the inside of the reaction kettle, an electromagnetic valve is arranged in the sampling chamber, the output end of the electromagnetic valve is fixedly connected with a sliding rod which penetrates through and extends to the inside of the sampling chamber, and one end of the sliding rod, which is positioned in the sampling chamber, is fixedly connected with a piston which is slidably connected to the inner wall of the sampling chamber; the inner top surface of the reaction kettle is vertically and rotatably connected with a transmission rod through a sealing bearing, and the bottom end of the transmission rod is fixedly connected with a turning hopper. This kind of high temperature reaction cauldron convenient to ration sample can freely control takes out the volume of reaction liquid, and is quick convenient, and the quick ration of the user of being convenient for is taken a sample, can prevent simultaneously that the bottom from precipitating the fixed reactant of complete reaction in the reation kettle, and the inside temperature of control reation kettle has improved the reaction conversion rate, has practiced thrift the cost.

Description

High temperature reaction cauldron convenient to ration sample

Technical Field

The utility model relates to the technical field of high-temperature reaction kettles, in particular to a high-temperature reaction kettle convenient for quantitative sampling.

Background

The reaction kettle is a container for physical or chemical reaction and is widely applied to the fields of petroleum, chemical industry, rubber, pesticides, dyes, medicines, food and the like.

When the reaction kettle works, in order to know the reaction process and the residual amount of various reaction raw materials, reaction solution in the reaction kettle needs to be sampled in real time in the reaction process, the existing reaction kettle sampling method is very complicated, quantitative sampling is inconvenient, and reactants which are not completely reacted are easy to accumulate at the bottom of the reaction kettle, so that the reaction efficiency is influenced.

In order to solve the problems, the high-temperature reaction kettle is improved, and the high-temperature reaction kettle convenient for quantitative sampling is provided.

SUMMERY OF THE UTILITY MODEL

In order to solve the technical problems, the utility model provides the following technical scheme:

the utility model provides a high-temperature reaction kettle convenient for quantitative sampling, which comprises a reaction kettle, wherein a protective sleeve is fixedly sleeved on the outer wall of the reaction kettle, a sampling chamber is fixedly installed on the side surface of the protective sleeve through a bolt, the sampling chamber is hermetically communicated with a sampling pipe which penetrates through and extends into the reaction kettle, an electromagnetic valve is arranged in the sampling chamber, the output end of the electromagnetic valve is fixedly connected with a sliding rod which penetrates through and extends into the sampling chamber, and one end of the sliding rod, which is positioned in the sampling chamber, is fixedly connected with a piston which is slidably connected with the inner wall of the sampling chamber;

the inner top surface of the reaction kettle is vertically and rotatably connected with a transmission rod through a sealing bearing, the outer wall of the transmission rod is fixedly connected with a plurality of stirring blades, and the bottom end of the transmission rod, which is positioned inside the reaction kettle, is fixedly connected with a stirring hopper, which is positioned at the bottom in the reaction kettle.

As a preferred technical scheme of the utility model, the inner wall of the protective sleeve is wound with a conveying pipeline, and the outer wall of the protective sleeve is provided with a liquid inlet and a liquid outlet which are respectively communicated with two ends of the conveying pipeline.

As a preferred technical scheme of the utility model, the electromagnetic valve comprises a shell, an electromagnet, a return spring and a sliding iron block, wherein the electromagnet is fixedly installed at the top of the shell, the return spring is fixedly connected between the electromagnet and the sliding iron block which is connected to the inner wall of the shell in a sliding manner, and one side, far away from the return spring, of the sliding iron block is fixedly connected to the sliding rod.

As a preferred technical scheme, the top surface of the reaction kettle is fixedly provided with a mounting base, the top surface of the mounting base is fixedly provided with a motor through a bolt, and the output end of the motor is coaxially and rotatably connected to the transmission rod through a coupler.

As a preferred technical scheme of the utility model, a filter screen is arranged at one end of the sampling tube, which is positioned in the reaction kettle.

As a preferred technical scheme of the utility model, a plurality of storage tanks are fixedly arranged at the bottom in the reaction kettle, the outlet ends at the bottoms of the storage tanks are provided with electric butterfly valves, and the storage tanks are correspondingly communicated with a plurality of feed inlets arranged on the top surface of the reaction kettle.

According to a preferable technical scheme of the utility model, a fixing support is fixedly installed on the outer wall of the protective sleeve through a bolt, the fixing support is vertically and fixedly connected with a plurality of supporting rods, the supporting rods are fixedly connected with a supporting plate, and four universal wheels are arranged on the bottom surface of the supporting plate.

As a preferred technical scheme of the utility model, an observation glass window is arranged on the side surface of the reaction kettle, and a liquid level meter for observing the liquid level of the sampling chamber is arranged on the outer wall of the sampling chamber.

The utility model has the beneficial effects that:

the utility model provides a, this kind of high temperature reaction cauldron convenient to ration sample, through the cooperation between solenoid valve, slide bar, piston, sampling chamber and the sampling tube, the reaction liquid of solenoid valve control piston in with reation kettle takes out through the sampling tube, can freely control the volume of taking reaction liquid out, and is quick convenient, the quick ration sample of the user of being convenient for.

Secondly, this kind of high temperature reaction cauldron convenient to ration sample through the turn-over fill that the transfer line bottom set up, can prevent that the bottom sediment in the reation kettle is the fixed reactant of complete reaction, has improved reaction conversion rate, has practiced thrift the cost.

Third, this kind of high temperature reaction cauldron convenient to ration sample through the pipeline that the inside winding of protective sheath set up, can improve reation kettle's temperature at the reaction initial stage for reaction rate, also can cool down reation kettle when reation kettle high temperature simultaneously.

Drawings

The accompanying drawings, which are included to provide a further understanding of the utility model and are incorporated in and constitute a part of this specification, illustrate embodiments of the utility model and together with the description serve to explain the principles of the utility model and not to limit the utility model. In the drawings:

FIG. 1 is a schematic diagram of a front view of a high temperature reaction vessel for facilitating quantitative sampling according to the present invention;

FIG. 2 is a schematic front sectional view of a high temperature reaction vessel for facilitating quantitative sampling according to the present invention;

FIG. 3 is an enlarged schematic view of a high temperature reaction vessel for facilitating quantitative sampling according to the present invention at FIG. 2A;

in the figure: 1. a reaction kettle; 101. observing the glass window; 2. a protective sleeve; 201. a delivery conduit; 3. a sampling chamber; 301. a liquid level meter; 4. a sampling tube; 5. an electromagnetic valve; 501. a housing; 502. an electromagnet; 503. a return spring; 504. sliding the iron block; 6. a slide bar; 7. a piston; 8. a transmission rod; 9. stirring blades; 10. mounting a base; 11. a motor; 12. a material turning hopper; 13. a material storage tank; 14. an electric butterfly valve; 15. fixing a bracket; 16. a support bar; 17. a support plate; 18. a universal wheel.

Detailed Description

The preferred embodiments of the present invention will be described in conjunction with the accompanying drawings, and it will be understood that they are described herein for the purpose of illustration and explanation and not limitation.

Example (b): as shown in fig. 1-3, a high temperature reaction kettle convenient for quantitative sampling comprises a reaction kettle 1, a protective sleeve 2 is fixedly sleeved on the outer wall of the reaction kettle 1, a sampling chamber 3 is fixedly installed on the side surface of the protective sleeve 2 through a bolt, the sampling chamber 3 is hermetically communicated with a sampling tube 4 penetrating and extending into the reaction kettle 1, the sampling chamber 3 is provided with an electromagnetic valve 5, the output end of the electromagnetic valve 5 is fixedly connected with a sliding rod 6 penetrating and extending into the sampling chamber 3, and one end of the sliding rod 6 located in the sampling chamber 3 is fixedly connected with a piston 7 slidably connected to the inner wall of the sampling chamber 3;

the inner top surface of the reaction kettle 1 is vertically and rotatably connected with a transmission rod 8 through a sealing bearing, the outer wall of the transmission rod 8 is fixedly connected with a plurality of stirring blades 9, and the bottom end of the transmission rod 8, which is positioned inside the reaction kettle 1, is fixedly connected with a material turning hopper 12, which is positioned at the bottom in the reaction kettle 1.

The winding of 2 inner walls of protective sheath is provided with pipeline 201 to 2 outer walls of protective sheath are provided with inlet and the liquid outlet that communicates with pipeline 201 both ends respectively, can improve reation kettle 1's temperature at the initial stage of reaction for reaction rate also can cool down reation kettle 1 when reation kettle 1 high temperature simultaneously.

The electromagnetic valve 5 comprises a shell 501, an electromagnet 502, a return spring 503 and a sliding iron block 504, wherein the electromagnet 502 is fixedly mounted at the top of the shell 501, the return spring 503 is fixedly connected between the electromagnet 502 and the sliding iron block 504 which is connected to the inner wall of the shell 501 in a sliding manner, and one side of the sliding iron block 504, which is far away from the return spring 503, is fixedly connected to the sliding rod 6.

The top surface of the reaction kettle 1 is fixedly provided with a mounting base 10, the top surface of the mounting base 10 is fixedly provided with a motor 11 through a bolt, and the output end of the motor 11 is coaxially and rotatably connected to the transmission rod 8 through a coupler.

Sampling tube 4 is located the inside one end of reation kettle 1 and is provided with the filter screen, filters large granule impurity, prevents that sampling tube 4 from blockking up.

Bottom fixed mounting has a plurality of storage tanks 13 in reation kettle 1, and a plurality of storage tanks 13 bottom exit end is provided with electric butterfly valve 14 to a plurality of storage tanks 13 correspond the intercommunication and have a plurality of feed inlets of setting at reation kettle 1 top surface, control feed rate through electric butterfly valve 14.

The outer wall of the protective sleeve 2 is fixedly provided with a fixing support 15 through a bolt, a plurality of support rods 16 are fixedly connected to the fixing support 15 vertically, a support plate 17 is fixedly connected with the support rods 16, and four universal wheels 18 are arranged on the bottom surface of the support plate 17, so that the reaction kettle 1 can be moved conveniently.

The side of the reaction kettle 1 is provided with an observation glass window 101, and the outer wall of the sampling chamber 3 is provided with a liquid level meter 301 for observing the liquid level of the sampling chamber 3.

The working principle is as follows: this kind of high temperature reaction cauldron convenient to ration sample, when using, put into reation kettle 1 through the cooperation between a plurality of storage tanks 13 and a plurality of electric butterfly valve 14 with reaction raw materials, motor 11 stirs again in operation, the stirring in-process, prevent through turning over hopper 12 that reation kettle 1 inner bottom from deposiing the fixed reactant of complete reaction, simultaneously through 2 built-in pipeline 201 of protective sheath improvement reation kettle 1 inside temperatures of reaction initial stage, accelerate initial stage reaction efficiency, also can be when reation kettle 1 high temperature, cool down reation kettle 1, the ration sample is carried out in needs, solenoid valve 5 can be started, drive the reaction liquid ration sample of piston 7 in with reation kettle 1.

In the description of the present invention, it should be noted that the terms "vertical", "upper", "lower", "horizontal", and the like indicate orientations or positional relationships based on those shown in the drawings, and are only for convenience of describing the present invention and simplifying the description, but do not indicate or imply that the referred device or element must have a specific orientation, be constructed in a specific orientation, and be operated, and thus, should not be construed as limiting the present invention.

In the description of the present invention, it should also be noted that, unless otherwise explicitly specified or limited, the terms "disposed," "mounted," "connected," and "connected" are to be construed broadly and may, for example, be fixedly connected, detachably connected, or integrally connected; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meanings of the above terms in the present invention can be understood by those skilled in the art according to specific situations.

Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that modifications may be made to the embodiments described above, or equivalents may be substituted for elements thereof. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.

Claims

1. The high-temperature reaction kettle convenient for quantitative sampling comprises a reaction kettle (1) and is characterized in that a protective sleeve (2) is fixedly sleeved on the outer wall of the reaction kettle (1), a sampling chamber (3) is fixedly mounted on the side surface of the protective sleeve (2) through a bolt, the sampling chamber (3) is hermetically communicated with a sampling pipe (4) penetrating and extending into the reaction kettle (1), the sampling chamber (3) is provided with an electromagnetic valve (5), the output end of the electromagnetic valve (5) is fixedly connected with a sliding rod (6) penetrating and extending into the sampling chamber (3), and one end, located inside the sampling chamber (3), of the sliding rod (6) is fixedly connected with a piston (7) slidably connected to the inner wall of the sampling chamber (3);

the inner top surface of the reaction kettle (1) is vertically and rotatably connected with a transmission rod (8) through a sealing bearing, the outer wall of the transmission rod (8) is fixedly connected with a plurality of stirring blades (9), and the bottom end of the transmission rod (8) inside the reaction kettle (1) is fixedly connected with a material turning hopper (12) at the bottom in the reaction kettle (1).

2. A high-temperature reaction kettle convenient for quantitative sampling according to claim 1, wherein a conveying pipeline (201) is wound on the inner wall of the protective sleeve (2), and a liquid inlet and a liquid outlet which are respectively communicated with two ends of the conveying pipeline (201) are arranged on the outer wall of the protective sleeve (2).

3. The high-temperature reaction kettle convenient for quantitative sampling according to claim 1, wherein the electromagnetic valve (5) comprises a housing (501), an electromagnet (502), a return spring (503) and a sliding iron block (504), the electromagnet (502) is fixedly installed at the top of the housing (501), the return spring (503) is fixedly connected between the electromagnet (502) and the sliding iron block (504) which is slidably connected to the inner wall of the housing (501), and one side of the sliding iron block (504) away from the return spring (503) is fixedly connected to the sliding rod (6).

4. A high-temperature reaction kettle convenient for quantitative sampling according to claim 1, wherein a mounting base (10) is fixedly mounted on the top surface of the reaction kettle (1), a motor (11) is fixedly mounted on the top surface of the mounting base (10) through a bolt, and the output end of the motor (11) is coaxially and rotatably connected to the transmission rod (8) through a shaft coupling.

5. A high-temperature reaction kettle convenient for quantitative sampling according to claim 1, characterized in that a filter screen is arranged at one end of the sampling tube (4) positioned in the reaction kettle (1).

6. A high-temperature reaction kettle convenient for quantitative sampling according to claim 1, wherein a plurality of storage tanks (13) are fixedly installed at the bottom of the reaction kettle (1), the outlet ends at the bottoms of the storage tanks (13) are provided with electric butterfly valves (14), and the storage tanks (13) are correspondingly communicated with a plurality of feed inlets arranged on the top surface of the reaction kettle (1).

7. The high-temperature reaction kettle convenient for quantitative sampling according to claim 1, wherein a fixing support (15) is fixedly installed on the outer wall of the protective sleeve (2) through bolts, the fixing support (15) is vertically and fixedly connected with a plurality of supporting rods (16), a plurality of supporting rods (16) are fixedly connected with a supporting plate (17), and four universal wheels (18) are arranged on the bottom surface of the supporting plate (17).

8. A high-temperature reaction kettle convenient for quantitative sampling according to claim 1, characterized in that an observation glass window (101) is arranged on the side of the reaction kettle (1), and a liquid level meter (301) for observing the liquid level of the sampling chamber (3) is arranged on the outer wall of the sampling chamber (3).