CN216792759U - Temperature control device for sulfonation reaction - Google Patents
Temperature control device for sulfonation reaction Download PDFInfo
- Publication number
- CN216792759U CN216792759U CN202123413120.9U CN202123413120U CN216792759U CN 216792759 U CN216792759 U CN 216792759U CN 202123413120 U CN202123413120 U CN 202123413120U CN 216792759 U CN216792759 U CN 216792759U
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- temperature control
- fixedly connected
- box
- face
- mixing
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- 238000006277 sulfonation reaction Methods 0.000 title claims abstract description 29
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 80
- 239000007788 liquid Substances 0.000 claims abstract description 53
- 230000000903 blocking effect Effects 0.000 claims description 10
- 230000000149 penetrating effect Effects 0.000 claims description 3
- 230000000694 effects Effects 0.000 abstract description 13
- 238000006243 chemical reaction Methods 0.000 description 9
- 238000000926 separation method Methods 0.000 description 7
- 239000000203 mixture Substances 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 3
- 239000003814 drug Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000004071 biological effect Effects 0.000 description 1
- 239000002775 capsule Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000003599 detergent Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 230000002452 interceptive effect Effects 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000011259 mixed solution Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
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Abstract
The utility model discloses a temperature control device for sulfonation reaction in the technical field of temperature control, which comprises a temperature control box, wherein a temperature control cavity is arranged in the temperature control box, the upper end surface of the temperature control cavity is fixedly connected with a mixing box, the outer circumferential surface of the mixing box is fixedly connected with a liquid outlet pipe, a mixing cavity is arranged in the mixing box, the circumferential surface in the mixing cavity is provided with a limiting groove, a limiting block is connected in the limiting groove in a sliding manner, the outer end surface of the limiting block is fixedly connected with a baffle plate, the lower end surface of the baffle plate is fixedly connected with a floating plate, the upper end surface of the baffle plate is provided with an air outlet hole, the outer side of the mixing box is provided with an outer connecting plate, and a water tank is formed between the outer connecting plate and the mixing box. The gas outlet, outer connecting plate, basin, first liquid feeding pipe, second liquid feeding pipe, water tank and outer takeover have reached the effect that can prevent the product spill that the sulfonation reaction produced and then pollute external device.
Description
Technical Field
The utility model relates to the technical field of temperature control, in particular to a temperature control device for sulfonation reaction.
Background
The sulfonation reaction plays an important role in the field of modern chemical industry, is an important step for synthesizing various organic products, and has wide application in the industries such as medicine, pesticide, fuel, detergent, petroleum and the like. Some medicines have problems in clinical application due to poor water solubility, such as low bioavailability, large dosage, slow absorption in the body of prepared tablets or capsules, and the like. The compound can enhance the water solubility and the biological activity after being sulfonated.
The problem of violent reaction of sulfonation reaction in the reaction process in the prior art can cause the phenomenon that the mixture violently splashes out in the reaction process, and finally the reaction cavity is damaged and external equipment is polluted.
SUMMERY OF THE UTILITY MODEL
The present invention is directed to a temperature control device for sulfonation reaction, which solves the above problems.
In order to achieve the purpose, the utility model provides the following technical scheme:
a temperature control device for sulfonation reaction comprises a temperature control box, wherein a temperature control cavity is formed in the temperature control box, the upper end face of the temperature control cavity is fixedly connected with a mixing box, the outer circumferential face of the mixing box is fixedly connected with a liquid outlet pipe, a mixing cavity is formed in the mixing box, the inner circumferential face of the mixing cavity is provided with a limiting groove, a limiting block is connected in the limiting groove in a sliding manner, the outer end face of the limiting block is fixedly connected with a separation plate, the lower end face of the separation plate is fixedly connected with a floating plate, the upper end face of the separation plate is provided with a gas outlet hole, the outer side of the mixing box is provided with an outer connecting plate, a water groove is formed between the outer connecting plate and the mixing box, the upper end face of the temperature control box is respectively connected with a first liquid adding pipe and a second liquid adding pipe in a penetrating manner, the tail ends of the first liquid adding pipe and the second liquid adding pipe are arranged in the mixing cavity, and the left end face of the temperature control box is fixedly connected with a water tank, the water tank is internally provided with a water pump, the front side of the right end face of the water tank is fixedly connected with a water inlet pipe, the tail end of the water inlet pipe is arranged in the water tank, the rear side of the inner end face of the water tank is fixedly connected with a water outlet pipe, the tail end of the water outlet pipe penetrates through the temperature control box, and the left end face of the water tank is fixedly connected with an external connecting pipe. The water pump in the water tank pumps the water in the water tank, and water reaches the basin through the inlet tube in, because sulfonation reaction can release a large amount of heats, water takes away the heat, and the water through the heating flows from the outlet pipe, and the action of supplying is carried out to the water in the water tank to the outer takeover lasts, has reached the effect that can prevent the product spill that the sulfonation reaction produced and then pollute external device.
As a further scheme of the utility model: the temperature control chamber lower extreme front side is opened and is equipped with the spout, sliding connection has the slider in the spout, slider up end fixedly connected with collects the box, is provided with spout, slider and collects the box and can reach the effect of collecting the mixed liquid after mixing.
As a still further scheme of the utility model: the outer diameter of the blocking plate is matched with the inner diameter of the mixing cavity, so that the effect that the mixture can not leak can be completely blocked by the blocking plate.
As a still further scheme of the utility model: the hinge is fixedly connected with the left side of the front end face of the temperature control box, the box door is fixedly connected with the outer circumferential face of the hinge, and the hinge and the box door are arranged, so that the effect of conveniently taking out the collecting box can be achieved.
As a still further scheme of the utility model: the size of the sliding block is matched with that of the sliding groove, so that the sliding block is prevented from interfering in the sliding groove.
As a still further scheme of the utility model: the support is fixedly connected with the lower end face of the temperature control box, and the support is provided with a plurality of supports which can achieve the effect of stably supporting the temperature control box.
Compared with the prior art, the utility model has the beneficial effects that:
in the utility model, a temperature control cavity is arranged in a temperature control box, the upper end surface of the temperature control cavity is fixedly connected with a mixing box, the outer circumferential surface of the mixing box is fixedly connected with a liquid outlet pipe, the inner circumferential surface of the mixing cavity is provided with a limit groove, the limit groove is internally connected with a limit block in a sliding way, the outer end surface of the limit block is fixedly connected with a baffle plate, the lower end surface of the baffle plate is fixedly connected with a floating plate, the upper end surface of the baffle plate is provided with a gas outlet hole, the outer side of the mixing box is provided with an outer connecting plate, a water tank is formed between the outer connecting plate and the mixing box, the upper end surface of the temperature control box is respectively connected with a first liquid feeding pipe and a second liquid feeding pipe in a penetrating way, the tail ends of the first liquid feeding pipe and the second liquid feeding pipe are arranged in the mixing cavity, the left end surface of the temperature control box is fixedly connected with a water tank, a water pump is arranged in the water tank, the front side of the right end surface of the water tank is fixedly connected with a water inlet pipe, the rear side of the inner end surface of the water tank is fixedly connected with a water outlet pipe and the water tank is fixedly connected with an outer end surface of the water tank, accomplish and carry out the liquid mixing of sulfonation reaction to two kinds of needs, add the mixed intracavity from first liquid feeding pipe and second liquid feeding pipe with first kind of liquid and second kind of liquid respectively, two kinds of liquids react in the mixed intracavity, it produces buoyancy to the kickboard to mix the liquid, the kickboard carries out the separation to the material that violent reaction produced, meanwhile herein, the water pump in the water tank pumps the water in the water tank, water reachs the basin through the inlet tube in, because the sulfonation reaction can release a large amount of heats, water is taken away the heat, water through the heating flows from the outlet pipe, the action that the water in the water tank was supplied is continuously carried out to the external pipe, the problem that the sulfonation reaction is violent in the reaction in-process has been solved, reached and can prevent that the product that the sulfonation reaction produced from spilling and then polluting the effect of external device.
Drawings
FIG. 1 is a schematic perspective view of the present invention;
FIG. 2 is a schematic cross-sectional view of a limiting groove according to the present invention;
FIG. 3 is an enlarged view of the structure of FIG. 2 at A according to the present invention;
FIG. 4 is a schematic cross-sectional view of a water tank according to the present invention;
FIG. 5 is a schematic view of the external connection tube of the present invention.
In the figure: 1. a temperature control box; 2. a support; 3. a temperature control cavity; 4. a hinge; 5. a box door; 6. a chute; 7. a slider; 8. a collection box; 9. a mixing box; 10. an outer connecting plate; 11. a water tank; 12. a liquid outlet pipe; 13. a first liquid adding pipe; 14. a second liquid adding pipe; 15. a water tank; 16. an external connection pipe; 17. a water outlet pipe; 18. a water inlet pipe; 19. a mixing chamber; 20. a limiting groove; 21. a limiting block; 22. a barrier plate; 23. a floating plate; 24. and an air outlet.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring to fig. 1-5, in the embodiment of the present invention, a temperature control device for sulfonation reaction includes a temperature control box 1, a temperature control cavity 3 is formed in the temperature control box 1, a mixing box 9 is fixedly connected to an upper end surface of the temperature control cavity 3, a liquid outlet pipe 12 is fixedly connected to an outer circumferential surface of the mixing box 9, a mixing cavity 19 is formed in the mixing box 9, a limiting groove 20 is formed on an inner circumferential surface of the mixing cavity 19, a limiting block 21 is slidably connected to the limiting groove 20, a blocking plate 22 is fixedly connected to an outer end surface of the limiting block 21, a floating plate 23 is fixedly connected to a lower end surface of the blocking plate 22, an air outlet hole 24 is formed on an upper end surface of the blocking plate 22, an outer connecting plate 10 is disposed outside the mixing box 9, a water tank 11 is formed between the outer connecting plate 10 and the mixing box 9, a first liquid adding pipe 13 and a second liquid adding pipe 14 are respectively connected to an upper end surface of the temperature control box 1, tail ends of the first liquid adding pipe 13 and the second liquid adding pipe 14 are disposed in the mixing cavity 19, the utility model can mix two liquids needing sulfonation reaction by arranging a mixing box 9, a liquid outlet pipe 12, a mixing cavity 19, a limiting groove 20, a limiting block 21, a baffle plate 22, a floating plate 23, a gas outlet hole 24, an outer connecting plate 10, a water tank 11, a first liquid adding pipe 13, a second liquid adding pipe 14, a water tank 15 and the outer connecting pipe 16, respectively add the first liquid and the second liquid into the mixing cavity 19 from the first liquid adding pipe 13 and the second liquid adding pipe 14, and react the two liquids in the mixing cavity 19, the mixed liquid produces buoyancy to kickboard 23, and separation board 22 carries out the separation to the material that violent reaction produced, and here simultaneously, the water pump in the water tank 15 pumps the water in the water tank 15, and water is in advancing water pipe 18 arrival basin 11, because sulfonation reaction can release a large amount of heats, and water is taken away the heat, and the water through the heating flows out from outlet pipe 17, and outer takeover 16 lasts the action of carrying out the supply to the water in the water tank 15, has reached the effect that can prevent the product spill that the sulfonation reaction produced and then pollute external device.
The front side of the lower end face of the temperature control cavity 3 is provided with a sliding chute 6, the sliding chute 6 is connected with a sliding block 7 in a sliding mode, the upper end face of the sliding block 7 is fixedly connected with a collection box 8, and the sliding chute 6, the sliding block 7 and the collection box 8 are arranged to achieve the effect of collecting mixed liquid after mixing;
the outer diameter of the blocking plate 22 is matched with the inner diameter of the mixing cavity 19, so that the effect that the mixture can not leak out can be completely blocked by the blocking plate 22;
the hinge 4 is fixedly connected to the left side of the front end face of the temperature control box 1, the box door 5 is fixedly connected to the outer circumferential face of the hinge 4, and the hinge 4 and the box door 5 are arranged to achieve the effect of conveniently taking out the collecting box 8;
the size of the sliding block 7 is matched with that of the sliding groove 6, so that the sliding block 7 is ensured not to generate an interference phenomenon in the sliding groove 6;
end face fixedly connected with support 2 under temperature control box 1, support 2 is provided with a plurality ofly, is provided with support 2 and can reaches the effect of carrying out stable support to temperature control box 1.
The working principle of the utility model is as follows: when the sulfonation reaction is carried out, two liquids to be subjected to the sulfonation reaction can be mixed, the first liquid and the second liquid are respectively added into the mixing cavity 19 from the first liquid adding pipe 13 and the second liquid adding pipe 14, the two liquids react in the mixing cavity 19, the mixed liquid generates buoyancy on the floating plate 23, the separation plate 22 separates substances generated by violent reaction, meanwhile, the water in the water tank 15 is pumped out by the water pump in the water tank 15, the water reaches the water tank 11 through the water inlet pipe 18, a large amount of heat is released due to the sulfonation reaction, the water takes away the heat, the heated water flows out from the water outlet pipe 17, the external connecting pipe 16 continuously supplies the water in the water tank 15, the effect of preventing products generated by the sulfonation reaction from splashing to pollute an external device is achieved, and after the reaction is finished, the liquid outlet pipe 12 is controlled through the electromagnetic valve, the mixed solution flows out of the outlet pipe 12 to the collection box 8.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and equivalent alternatives or modifications according to the technical solution of the present invention and the inventive concept thereof should be covered by the scope of the present invention.
Claims (6)
1. A temperature control device for sulfonation reaction, which comprises a temperature control box (1), and is characterized in that: a temperature control cavity (3) is formed in the temperature control box (1), a mixing box (9) is fixedly connected to the upper end face of the temperature control cavity (3), a liquid outlet pipe (12) is fixedly connected to the outer circumferential face of the mixing box (9), a mixing cavity (19) is formed in the mixing box (9), a limiting groove (20) is formed in the inner circumferential face of the mixing cavity (19), a limiting block (21) is connected in the limiting groove (20) in a sliding manner, a blocking plate (22) is fixedly connected to the outer end face of the limiting block (21), a floating plate (23) is fixedly connected to the lower end face of the blocking plate (22), an air outlet hole (24) is formed in the upper end face of the blocking plate (22), an outer connecting plate (10) is arranged on the outer side of the mixing box (9), a water groove (11) is formed between the outer connecting plate (10) and the mixing box (9), a first liquid adding pipe (13) and a second liquid adding pipe (14) are respectively connected to the upper end face of the temperature control box (1) in a penetrating manner, first liquid feeding pipe (13) with second liquid feeding pipe (14) tail end sets up in hybrid chamber (19), control by temperature change case (1) left end face fixedly connected with water tank (15), be provided with the water pump in water tank (15), water tank (15) right-hand member face front side fixedly connected with inlet tube (18), inlet tube (18) tail end sets up in basin (11), terminal surface rear side fixedly connected with outlet pipe (17) in basin (11), outlet pipe (17) tail end runs through control by temperature change case (1) and sets up, water tank (15) left end face fixedly connected with is external to manage (16).
2. The temperature control device for sulfonation according to claim 1, wherein: the temperature control chamber (3) lower extreme front side is opened and is equipped with spout (6), sliding connection has slider (7) in spout (6), slider (7) up end fixedly connected with collects box (8).
3. The temperature control device for sulfonation according to claim 1, wherein: the outer diameter of the baffle plate (22) is matched with the inner diameter of the mixing cavity (19).
4. The temperature control device for sulfonation according to claim 1, wherein: the temperature control box is characterized in that a hinge (4) is fixedly connected to the left side of the front end face of the temperature control box (1), and a box door (5) is fixedly connected to the outer circumferential face of the hinge (4).
5. The temperature control device for sulfonation according to claim 2, wherein: the size of the sliding block (7) is matched with that of the sliding groove (6).
6. The temperature control device for sulfonation according to claim 1, wherein: the lower end face of the temperature control box (1) is fixedly connected with a support (2), and the support (2) is provided with a plurality of parts.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202123413120.9U CN216792759U (en) | 2021-12-30 | 2021-12-30 | Temperature control device for sulfonation reaction |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202123413120.9U CN216792759U (en) | 2021-12-30 | 2021-12-30 | Temperature control device for sulfonation reaction |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN216792759U true CN216792759U (en) | 2022-06-21 |
Family
ID=82010313
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202123413120.9U Expired - Fee Related CN216792759U (en) | 2021-12-30 | 2021-12-30 | Temperature control device for sulfonation reaction |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN216792759U (en) |
-
2021
- 2021-12-30 CN CN202123413120.9U patent/CN216792759U/en not_active Expired - Fee Related
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| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20220621 |
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| CF01 | Termination of patent right due to non-payment of annual fee |