CN216755466U - Continuous water washing extraction device for D- (-) -alpha-hydroxy-beta, beta-dimethyl-gamma-butyrolactone intermediate - Google Patents
Continuous water washing extraction device for D- (-) -alpha-hydroxy-beta, beta-dimethyl-gamma-butyrolactone intermediate Download PDFInfo
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- CN216755466U CN216755466U CN202220261210.6U CN202220261210U CN216755466U CN 216755466 U CN216755466 U CN 216755466U CN 202220261210 U CN202220261210 U CN 202220261210U CN 216755466 U CN216755466 U CN 216755466U
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Abstract
The utility model discloses a continuous water washing extraction device for a D- (-) -alpha-hydroxy-beta, beta-dimethyl-gamma-butyrolactone intermediate, which comprises a water washing extraction tank, wherein a liquid inlet pipe, a first liquid outlet pipe and a second liquid outlet pipe are arranged on the water washing extraction tank, and the top end of the second liquid outlet pipe is provided with a liquid inlet hole. According to the utility model, the main shaft is driven to rotate by the driving motor, the main shaft drives the inner guide barrel to rotate, the inner guide barrel drives the fixed disc to rotate and the stirring blades in the fixed disc to rotate, so that liquid in the outer guide barrel is stirred, when the liquid in the outer guide barrel is full, the liquid is guided to the inner part of the outer guide barrel again through the liquid guide pipe to be stirred, meanwhile, under the action of the machine pump, the liquid is guided into the annular pipe through the circulating pipe and is sprayed through the spray head, and the liquid in the washing extraction tank can be rapidly and uniformly mixed by matching with the operation of the stirring assembly, so that the stirring efficiency is high, the time is saved, and the production efficiency is improved.
Description
Technical Field
The utility model relates to the technical field of water washing extraction, in particular to a continuous water washing extraction device for a D- (-) -alpha-hydroxy-beta, beta-dimethyl-gamma-butyrolactone intermediate.
Background
The water washing extraction is also called water washing liquid separation, and is generally used for organic experiments. When preparing liquid organic substances, several organic substances are often mixed at the same time. If the organic substances are difficult to extract by organic extraction, the organic substances can be separated by utilizing the difference of water solubility.
When the existing water-washing extraction device is used for extraction, the phenomenon of incomplete liquid reaction is easy to occur, so that the extraction efficiency is low and the extraction is incomplete.
SUMMERY OF THE UTILITY MODEL
The utility model aims to: in order to solve the problems, the device for continuously washing and extracting the D- (-) -alpha-hydroxy-beta, beta-dimethyl-gamma-butyrolactone intermediate by water is provided.
In order to achieve the purpose, the utility model adopts the following technical scheme:
the utility model provides a be used for D-alpha-hydroxyl-beta, beta-dimethyl-gamma-butyrolactone midbody continuous washing extraction device, includes washing extraction jar, be provided with feed liquor pipe and drain pipe one and drain pipe two on the washing extraction jar, the top of drain pipe two has the feed liquor hole, the inside of washing extraction jar is provided with the main shaft, the table wall is connected with driving motor in the top that the main shaft runs through washing extraction jar, the bottom of main shaft is connected with stirring component, still be provided with even liquid subassembly on the washing extraction jar.
Preferably, the stirring assembly comprises an outer guide flow barrel, the inner part of the outer guide flow barrel is rotatably connected with a fixed disc, stirring blades are arranged in the fixed disc, the upper end face of the fixed disc is provided with an inner guide flow barrel, and the outer guide flow barrel is further provided with a liquid guide pipe.
Preferably, the inner guide barrel is connected with the main shaft through a support rod.
Preferably, even liquid subassembly is including intercommunication water washing extraction jar and the circulating pipe and the injection subassembly of drain pipe two, the injection subassembly is including installing the machine pump on the circulating pipe and installing the annular pipe at the circulating pipe top, be provided with the shower nozzle on the annular pipe.
Preferably, the liquid inlet pipe, the first liquid outlet pipe, the second liquid outlet pipe and the circulating pipe are all provided with control valves.
In summary, due to the adoption of the technical scheme, the utility model has the beneficial effects that:
in this application, it rotates to drive the main shaft through driving motor, the main shaft drives interior water conservancy diversion bucket and rotates, interior water conservancy diversion bucket drives the fixed disk and rotates and its inside stirring vane rotates, thereby stir the inside liquid of external water conservancy diversion bucket, when the inside liquid of outer water conservancy diversion bucket is filled with, water conservancy diversion once more stirs to outer water conservancy diversion bucket inside through the catheter, simultaneously under the effect of machine pump, liquid passes through in the leading-in ring pipe of circulating pipe, and spray through the shower nozzle, the operation of cooperation stirring subassembly can carry out the homogeneous mixing to the liquid in the washing extraction jar fast, stirring efficiency is high, the time is saved, the production efficiency is improved.
Drawings
FIG. 1 illustrates a schematic three-dimensional front view structure provided according to an embodiment of the present invention;
FIG. 2 illustrates a schematic three-dimensional cross-sectional structure provided in accordance with an embodiment of the present invention;
fig. 3 is a schematic structural diagram of a stirring assembly provided according to an embodiment of the utility model.
Illustration of the drawings:
1. washing the extraction tank with water; 2. a liquid inlet pipe; 3. a main shaft; 4. a drive motor; 5. a second liquid outlet pipe; 6. a circulation pipe; 7. a machine pump; 8. a first liquid outlet pipe; 9. an annular tube; 10. a spray head; 11. an outer guide barrel; 12. a catheter; 13. a liquid inlet hole; 14. a stirring blade; 15. an inner guide barrel; 16. fixing the disc; 17. a support bar; 18. and (4) controlling the valve.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring to fig. 1-3, the present invention provides a technical solution:
a continuous water washing extraction device for D- - -alpha-hydroxyl-beta, beta-dimethyl-gamma-butyrolactone intermediates comprises a water washing extraction tank 1, wherein a liquid inlet pipe 2, a first liquid outlet pipe 8 and a second liquid outlet pipe 5 are arranged on the water washing extraction tank 1, a add and derive for control liquid, the top of drain pipe two 5 has feed liquor hole 13, make the inside liquid of washing extraction jar 1 flow in the inside of drain pipe two 5 through feed liquor hole 13, the inside of washing extraction jar 1 is provided with main shaft 3, the table wall connection has driving motor 4 in the main shaft 3 runs through the top of washing extraction jar 1, driving motor 4 provides drive power for main shaft 3's rotation, main shaft 3's bottom is connected with the stirring subassembly, the stirring subassembly can be with higher speed liquid mixing efficiency, still be provided with even liquid subassembly on the washing extraction jar 1, even liquid subassembly can improve the even effect of liquid mixing.
Specifically, as shown in fig. 2, the stirring assembly includes an outer guide flow barrel 11, the inner portion of the outer guide flow barrel 11 is rotatably connected with a fixed disk 16, stirring blades 14 are arranged inside the fixed disk 16, an inner guide flow barrel 15 is arranged on the upper end face of the fixed disk 16, and a liquid guide tube 12 is further arranged on the outer guide flow barrel 11, so that the liquid is sufficiently mixed by the rotation of the stirring blades 14, and the liquid in the outer guide flow barrel 11 is guided to the inner portion of the inner guide flow barrel 15 again by the liquid guide tube 12 and enters the outer guide flow barrel 11 through the inner guide flow barrel 15.
Specifically, as shown in fig. 3, the inner guide flow barrel 15 is connected to the main shaft 3 through a support rod 17, so that the rotation of the main shaft 3 drives the inner guide flow barrel 15 to rotate.
Specifically, as shown in fig. 1 to 2, the liquid homogenizing assembly comprises a circulating pipe 6 and a spraying assembly, the circulating pipe 6 is communicated with the water washing extraction tank 1 and the liquid outlet pipe two 5, the spraying assembly comprises a pump 7 mounted on the circulating pipe 6 and a ring pipe 9 mounted at the top end of the circulating pipe 6, a spray head 10 is arranged on the ring pipe 9, under the action of the pump 7, liquid is guided into the ring pipe 9 through the circulating pipe 6 and is sprayed through the spray head 10, and the liquid in the water washing extraction tank 1 can be quickly mixed in cooperation with the operation of the stirring assembly.
Specifically, as shown in fig. 2, the liquid inlet pipe 2, the first liquid outlet pipe 8, the second liquid outlet pipe 5 and the circulating pipe 6 are all provided with control valves 18, which are convenient for controlling the on-off of each pipeline.
In conclusion, the continuous water washing and extracting device for the D- - -alpha-hydroxy-beta, beta-dimethyl-gamma-butyrolactone intermediate provided by the embodiment, the main shaft 3 is driven to rotate by the driving motor 4, the inner guide flow barrel 15 is driven to rotate by the main shaft 3, the fixed disc 16 and the stirring blades 14 in the fixed disc are driven to rotate by the inner guide flow barrel 15, so as to stir the liquid in the outer guide flow barrel 11, when the liquid in the outer guide flow barrel 11 is full, the liquid is guided to the inner part of the outer guide flow barrel 11 again through the liquid guide pipe 12 to be stirred, simultaneously under the effect of pump 7, liquid leads to in the ring pipe 9 through circulating pipe 6 to spray through shower nozzle 10, the operation of cooperation stirring subassembly can be fast to the liquid homogeneous mixing in the washing extraction jar 1, stir efficiently, save time, improved production efficiency.
The previous description of the embodiments is provided to enable any person skilled in the art to make or use the present invention. Various modifications to these embodiments will be readily apparent to those skilled in the art, and the generic principles defined herein may be applied to other embodiments without departing from the spirit or scope of the utility model. Thus, the present invention is not intended to be limited to the embodiments shown herein but is to be accorded the widest scope consistent with the principles and novel features disclosed herein.
Claims (5)
1. The utility model provides a be used for D- (-) -alpha-hydroxyl-beta, beta-dimethyl-gamma-butyrolactone midbody to wash extraction device with water in succession, includes washing extraction jar (1), its characterized in that, be provided with feed liquor pipe (2) and drain pipe (8) and drain pipe two (5) on washing extraction jar (1), the top of drain pipe two (5) has feed liquor hole (13), the inside of washing extraction jar (1) is provided with main shaft (3), surface wall connection has driving motor (4) in main shaft (3) runs through the top of washing extraction jar (1), the bottom of main shaft (3) is connected with stirring component, still be provided with even liquid subassembly on washing extraction jar (1).
2. The continuous water washing extraction device for the D- (-) -alpha-hydroxy-beta, beta-dimethyl-gamma-butyrolactone intermediate according to claim 1, wherein the stirring component comprises an outer guide barrel (11), a fixed disk (16) is rotatably connected to the inside of the outer guide barrel (11), stirring blades (14) are arranged inside the fixed disk (16), an inner guide barrel (15) is arranged on the upper end face of the fixed disk (16), and a liquid guide tube (12) is further arranged on the outer guide barrel (11).
3. The continuous water washing extraction device for the D- (-) -alpha-hydroxy-beta, beta-dimethyl-gamma-butyrolactone intermediate according to claim 2, characterized in that the inner guide barrel (15) is connected with the main shaft (3) through a support rod (17).
4. The continuous water washing extraction device for the D- (-) -alpha-hydroxy-beta, beta-dimethyl-gamma-butyrolactone intermediate according to claim 1, wherein the liquid homogenizing assembly comprises a circulating pipe (6) communicating the water washing extraction tank (1) and the second liquid outlet pipe (5), and a spraying assembly, the spraying assembly comprises a pump (7) mounted on the circulating pipe (6) and a ring pipe (9) mounted at the top end of the circulating pipe (6), and a spray head (10) is arranged on the ring pipe (9).
5. The continuous water washing and extracting device for the D- (-) -alpha-hydroxy-beta, beta-dimethyl-gamma-butyrolactone intermediate according to claim 4, characterized in that control valves (18) are arranged on the liquid inlet pipe (2), the liquid outlet pipe I (8), the liquid outlet pipe II (5) and the circulating pipe (6).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202220261210.6U CN216755466U (en) | 2022-02-09 | 2022-02-09 | Continuous water washing extraction device for D- (-) -alpha-hydroxy-beta, beta-dimethyl-gamma-butyrolactone intermediate |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202220261210.6U CN216755466U (en) | 2022-02-09 | 2022-02-09 | Continuous water washing extraction device for D- (-) -alpha-hydroxy-beta, beta-dimethyl-gamma-butyrolactone intermediate |
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| CN216755466U true CN216755466U (en) | 2022-06-17 |
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| CN202220261210.6U Active CN216755466U (en) | 2022-02-09 | 2022-02-09 | Continuous water washing extraction device for D- (-) -alpha-hydroxy-beta, beta-dimethyl-gamma-butyrolactone intermediate |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116422007A (en) * | 2023-05-12 | 2023-07-14 | 江苏东宝农化股份有限公司 | Extraction device and application thereof in extraction of azadirachtin |
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2022
- 2022-02-09 CN CN202220261210.6U patent/CN216755466U/en active Active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116422007A (en) * | 2023-05-12 | 2023-07-14 | 江苏东宝农化股份有限公司 | Extraction device and application thereof in extraction of azadirachtin |
| CN116422007B (en) * | 2023-05-12 | 2023-11-07 | 江苏东宝农化股份有限公司 | Extraction device and application thereof in extraction of azadirachtin |
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Address after: 115000, Liaoning Yingkou immortal Island energy chemical industry zone Patentee after: Liaoning Xinhe Biochemical Technology Co.,Ltd. Address before: 115000, Liaoning Yingkou immortal Island energy chemical industry zone Patentee before: Liaoning Xinhe new energy material technology Co.,Ltd. |
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| CP01 | Change in the name or title of a patent holder |