CN216727743U - Chemical reagent auxiliary agent ammonolysis centrifugal device - Google Patents
Chemical reagent auxiliary agent ammonolysis centrifugal device Download PDFInfo
- Publication number
- CN216727743U CN216727743U CN202220162268.5U CN202220162268U CN216727743U CN 216727743 U CN216727743 U CN 216727743U CN 202220162268 U CN202220162268 U CN 202220162268U CN 216727743 U CN216727743 U CN 216727743U
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- plate
- ammonolysis
- outer frame
- chemical reagent
- reagent auxiliary
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- 239000003153 chemical reaction reagent Substances 0.000 title claims abstract description 36
- 238000005915 ammonolysis reaction Methods 0.000 title claims abstract description 24
- 239000012752 auxiliary agent Substances 0.000 title claims abstract description 14
- 238000005119 centrifugation Methods 0.000 claims abstract description 8
- 238000003825 pressing Methods 0.000 claims abstract description 5
- 239000007788 liquid Substances 0.000 claims description 16
- 238000005192 partition Methods 0.000 claims description 13
- 238000000926 separation method Methods 0.000 abstract description 10
- 238000003756 stirring Methods 0.000 abstract description 4
- 238000006243 chemical reaction Methods 0.000 abstract description 2
- 238000007790 scraping Methods 0.000 abstract description 2
- 238000000034 method Methods 0.000 description 4
- 238000005576 amination reaction Methods 0.000 description 2
- 238000003466 welding Methods 0.000 description 2
- -1 amine compounds Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229910052729 chemical element Inorganic materials 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 125000000524 functional group Chemical group 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
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- Centrifugal Separators (AREA)
- Sampling And Sample Adjustment (AREA)
Abstract
The utility model belongs to the technical field of ammonolysis centrifugal devices, and particularly relates to a chemical reagent auxiliary agent ammonolysis centrifugal device which comprises an outer frame, wherein an air outlet pipe is inserted into the top of the outer frame, a clamping plate is inserted into the inner side of the outer frame, the bottom of the clamping plate is rotatably connected with an inner cylinder, a pressing plate is fixedly installed at the top of the clamping plate, a separation plate is fixedly installed on the inner side of the outer frame, a scraping plate is fixedly installed on the outer side of the inner cylinder, and a through hole is formed in the side face of the separation plate. This chemical reagent auxiliary agent ammonolysis centrifugal device through being provided with clamp plate, sloping block, driving lever, through stirring the driving lever, the driving lever drives the sloping block and breaks away from the joint groove, can realize the separation to inner tube and frame through picking up the clamp plate, and the follow-up fixed reagent of being convenient for takes out and clears up, improves the practicality and the stability of device, and in addition, the gaseous through-hole and the outlet duct discharge of reaction in the centrifugation process, subsequent gaseous processing of being convenient for.
Description
Technical Field
The utility model relates to the technical field of ammonolysis centrifugal devices, in particular to an ammonolysis centrifugal device for a chemical reagent auxiliary agent.
Background
With the continuous research on chemical elements, more and more functional chemical reagent assistants are developed for the subsequent research foundation of people and also applied to various fields in life, in the chemical research, part of chemical reagents need to be subjected to ammonolysis reaction, the ammonolysis reaction refers to the process that organic compounds containing various functional groups generate amine compounds under the action of aminating agents, and the ammonolysis is also sometimes called "amination" or "amination".
In the ammonolysis process of the chemical reagent auxiliary agent, solid-liquid separation needs to be carried out on the auxiliary agent, centrifugal equipment needs to be used, the solid-liquid separation can be achieved by the existing centrifugal equipment, but separated liquid can be adhered to the inner wall of a centrifugal machine and is difficult to clean and collect, meanwhile, a centrifugal cylinder of the existing centrifugal device is basically fixedly installed, the separated solid reagent is difficult to take out, the experimental efficiency is influenced, and the use is inconvenient.
SUMMERY OF THE UTILITY MODEL
Aiming at the defects of the prior art, the utility model provides a chemical reagent auxiliary agent ammonolysis centrifugal device, which solves the problems existing at present.
In order to achieve the purpose, the utility model provides the following technical scheme: the utility model provides a chemical reagent auxiliary agent ammonolysis centrifugal device, includes the frame, it has the outlet duct to peg graft at the top of frame, it has the joint board to peg graft in the inboard of frame, the bottom of joint board is rotated and is connected with the inner tube, the top fixed mounting of joint board has the press plate, the inboard fixed mounting of frame has the division board, the outside fixed mounting of inner tube has the scraper blade, the through-hole has been seted up to the side of division board, the bottom fixed mounting of frame has the fixed plate, the inboard fixed mounting of fixed plate has extension spring, extension spring keeps away from the inboard one end welding of fixed plate and has the sloping block, the positive fixed mounting of sloping block has the driving lever, the bottom fixed mounting of inner tube has the frock board, the spout has been seted up in the outside of frame, the inboard top fixed mounting of frame has the lug.
As a preferable technical scheme of the utility model, one end of the scraper far away from the inner cylinder is connected with the partition plate in a sliding manner, and the through hole is positioned above the scraper.
As a preferable technical solution of the present invention, the inclined block is slidably connected to an inner side of the fixing plate, the shift lever penetrates through an inner wall of the outer frame to an outside of the outer frame, and the shift lever is slidably connected to an inner side of the sliding groove.
As a preferred technical scheme of the utility model, the bottom of the tooling plate is designed into an inclined plane and is matched with the inclined plane of the inclined block, the side surface of the tooling plate is provided with a clamping groove, and the inclined block can enter the clamping groove.
As a preferable technical scheme of the utility model, the outer side of the clamping and connecting plate is provided with a groove, and the groove is clamped with the bump.
As a preferable technical scheme of the utility model, the two scrapers are symmetrically distributed on the outer side of the inner cylinder.
As a preferable technical scheme of the utility model, a liquid outlet is formed in the bottom of the outer frame and between the inner cylinder and the partition plate.
Compared with the prior art, the utility model provides a chemical reagent auxiliary agent ammonolysis centrifugal device, which has the following beneficial effects:
1. the ammonolysis centrifugal device for the chemical reagent auxiliary agent is provided with the inclined block, the extension spring and the convex block, an operator presses the pressing plate downwards, the bottom of the tooling plate is contacted with the inclined block and pushes the inclined block to enter the inner side of the fixed plate, and the inclined block can extrude the extension spring along with the continuous movement of the inclined block, when the inclined block and the clamping groove on the side surface of the tooling plate are positioned on the same horizontal plane, the inclined block enters the clamping groove under the action of the extension spring to clamp the tooling plate, meanwhile, the convex block is clamped with the groove on the clamping plate to limit the inner cylinder, at the moment, the scraper blade is tightly attached to the inner wall of the partition plate, the tooling plate is driven to rotate and the inner cylinder is driven to rotate by external power, so that the separation of the reagent is realized, the scraper plate also rotates along with the reagent, and liquid reagent separated on the partition plate is scraped and flows out through the liquid outlet, so that the collection and the cleaning of the reagent of the liquid in the device are achieved.
2. This chemical reagent auxiliary agent ammonolysis centrifugal device through being provided with clamp plate, sloping block, driving lever, through stirring the driving lever, the driving lever drives the sloping block and breaks away from the joint groove, can realize the separation to inner tube and frame through picking up the clamp plate, and the follow-up fixed reagent of being convenient for takes out and clears up, improves the practicality and the stability of device, and in addition, the gaseous through-hole and the outlet duct discharge of reaction in the centrifugation process, subsequent gaseous processing of being convenient for.
Drawings
FIG. 1 is a schematic structural view of the present invention;
FIG. 2 is a schematic view of the internal structure of the outer frame of the present invention;
FIG. 3 is a top view of the position relationship between the inner barrel and the scraper according to the present invention;
FIG. 4 is an enlarged view of the structure at A in FIG. 2 according to the present invention.
In the figure: 1. an outer frame; 2. an air outlet pipe; 3. a clamping and connecting plate; 4. pressing a plate; 5. a partition plate; 6. a squeegee; 7. a fixing plate; 8. an extension spring; 9. a sloping block; 10. assembling a plate; 11. a deflector rod; 12. a chute; 13. a through hole; 14. a bump; 15. an inner cylinder.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring to fig. 1-4, in the present embodiment: the utility model provides a chemical reagent auxiliary agent ammonolysis centrifugal device, including frame 1, it has outlet duct 2 to peg graft at the top of frame 1, it has joint board 3 to peg graft in the inboard of frame 1, the bottom of joint board 3 is rotated and is connected with inner tube 15, the top fixed mounting of joint board 3 has press plate 4, the inboard fixed mounting of frame 1 has division board 5, the outside fixed mounting of inner tube 15 has scraper blade 6, through-hole 13 has been seted up to division board 5's side, the bottom fixed mounting of frame 1 has fixed plate 7, the inboard fixed mounting of fixed plate 7 has extension spring 8, extension spring 8 keeps away from the inboard one end welding of fixed plate 7 and has sloping block 9, the positive fixed mounting of sloping block 9 has driving lever 11, the bottom fixed mounting of inner tube 15 has frock board 10, spout 12 has been seted up in the outside of frame 1, the inboard top fixed mounting of frame 1 has lug 14.
In the embodiment, one end of the scraper 6, which is far away from the inner cylinder 15, is slidably connected with the partition plate 5, the through hole 13 is positioned above the scraper 6, so that the liquid reagent on the partition plate 5 can be conveniently scraped and cleaned, the sloping block 9 is slidably connected to the inner side of the fixing plate 7, the deflector rod 11 penetrates through the inner wall of the outer frame 1 to the outer side of the outer frame 1, the deflector rod 11 is slidably connected to the inner side of the chute 12, so that the tooling plate 10 can be conveniently limited and released by stirring the deflector rod 11, the inner cylinder 15 can be conveniently taken out, so that the fixing reagent can be conveniently taken out and cleaned, the bottom of the tooling plate 10 is designed to be an inclined plane and is matched with the inclined plane of the sloping block 9, the side surface of the tooling plate 10 is provided with a clamping groove, the sloping block 9 can enter the clamping groove, so that the tooling plate 10 can be conveniently fixed, the outer side of the clamping plate 3 is provided with a groove, the groove is clamped with the lug 14, so that the clamping plate 3 can be conveniently fixed, the scraper 6 is provided with two symmetrical parts which are distributed on the outer side of the inner cylinder 15, improve scraping efficiency of liquid reagent, the liquid outlet has been seted up just to the bottom of frame 1 between being located inner tube 15 and division board 5, and the liquid reagent of being convenient for flows and collects from the liquid outlet.
The working principle and the using process of the utility model are as follows: an operator presses the pressing plate 4 downwards to enable the bottom of the tooling plate 10 to be in contact with the inclined block 9 and push the inclined block 9 to enter the inner side of the fixing plate 7, the inclined block 9 can extrude the extension spring 8 along with the continuous movement of the inclined block 9, when the inclined block 9 and a clamping groove on the side face of the tooling plate 10 are positioned on the same horizontal plane, the inclined block 9 enters the clamping groove under the action of the extension spring 8 to clamp the tooling plate 10, meanwhile, the lug 14 is clamped with a groove on the clamping plate 3 to limit the inner cylinder 15, the scraper 6 is tightly attached to the inner wall of the partition plate 5 at the moment, the tooling plate 10 is driven to rotate by external power and drives the inner cylinder 15 to rotate, so that the separation of a reagent is realized, the scraper 6 can also rotate along with the inclined block, the liquid reagent separated on the partition plate 5 is scraped and flows out through a liquid outlet to collect and clean the reagent in the liquid in the device, in addition, the gas reacted in the centrifugal process is discharged from the gas outlet pipe 2 through the through hole 13, subsequent gaseous processing of being convenient for, after the separation is accomplished, through stirring driving lever 11, driving lever 11 drives sloping block 9 and breaks away from the joint groove, can realize the separation to inner tube 15 and frame 1 through picking up clamp plate 4, and follow-up fixed reagent of being convenient for takes out and clears up, improves the practicality and the stability of device.
Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that changes may be made in the embodiments and/or equivalents thereof without departing from the spirit and scope of the utility model. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (7)
1. The utility model provides a chemical reagent auxiliary agent ammonolysis centrifugal device, includes frame (1), its characterized in that: the top of the outer frame (1) is spliced with an air outlet pipe (2), the inner side of the outer frame (1) is spliced with a clamping plate (3), the bottom of the clamping plate (3) is rotatably connected with an inner tube (15), the top of the clamping plate (3) is fixedly provided with a pressing plate (4), the inner side of the outer frame (1) is fixedly provided with a partition plate (5), the outer side of the inner tube (15) is fixedly provided with a scraper (6), the side surface of the partition plate (5) is provided with a through hole (13), the bottom of the outer frame (1) is fixedly provided with a fixed plate (7), the inner side of the fixed plate (7) is fixedly provided with a tension spring (8), one end of the tension spring (8) far away from the inner side of the fixed plate (7) is welded with an inclined block (9), the front of the inclined block (9) is fixedly provided with a shift lever (11), the bottom of the inner tube (15) is fixedly provided with a tooling plate (10), the outer side of the outer frame (1) is provided with a sliding groove (12), and the top of the inner side of the outer frame (1) is fixedly provided with a convex block (14).
2. The chemical reagent auxiliary ammonolysis centrifugation apparatus according to claim 1, wherein: one end, far away from the inner cylinder (15), of the scraper (6) is connected with the partition plate (5) in a sliding mode, and the through hole (13) is located above the scraper (6).
3. The chemical reagent auxiliary ammonolysis centrifugation apparatus according to claim 1, wherein: the inclined block (9) is connected to the inner side of the fixing plate (7) in a sliding mode, the shifting rod (11) penetrates through the inner wall of the outer frame (1) to the outside of the outer frame (1), and the shifting rod (11) is connected to the inner side of the sliding groove (12) in a sliding mode.
4. The chemical reagent auxiliary ammonolysis centrifugation apparatus according to claim 1, wherein: the bottom of the tooling plate (10) is designed to be an inclined plane and is matched with the inclined plane of the inclined block (9), a clamping groove is formed in the side face of the tooling plate (10), and the inclined block (9) can enter the clamping groove.
5. The chemical reagent auxiliary ammonolysis centrifugation apparatus according to claim 1, wherein: the outer side of the clamping plate (3) is provided with a groove, and the groove is clamped with the bump (14).
6. The chemical reagent auxiliary ammonolysis centrifugation apparatus according to claim 1, wherein: the two scrapers (6) are symmetrically distributed on the outer side of the inner cylinder (15).
7. The chemical reagent auxiliary ammonolysis centrifugation apparatus according to claim 6, wherein: and a liquid outlet is formed in the bottom of the outer frame (1) and positioned between the inner cylinder (15) and the partition plate (5).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202220162268.5U CN216727743U (en) | 2022-01-21 | 2022-01-21 | Chemical reagent auxiliary agent ammonolysis centrifugal device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202220162268.5U CN216727743U (en) | 2022-01-21 | 2022-01-21 | Chemical reagent auxiliary agent ammonolysis centrifugal device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN216727743U true CN216727743U (en) | 2022-06-14 |
Family
ID=81913981
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202220162268.5U Active CN216727743U (en) | 2022-01-21 | 2022-01-21 | Chemical reagent auxiliary agent ammonolysis centrifugal device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN216727743U (en) |
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2022
- 2022-01-21 CN CN202220162268.5U patent/CN216727743U/en active Active
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20240318 Address after: No. 3001, 30th Floor, Building 1, No. 138 Tianfu Second Street, Chengdu High tech Zone, China (Sichuan) Pilot Free Trade Zone, Chengdu City, Sichuan Province, 610000 Patentee after: Chengdu Taibo Ruisi Technology Co.,Ltd. Country or region after: China Address before: 200120 Room 202, second floor, building 6, No. 1-28, Lane 588, Tianxiong Road, Pudong New Area, Shanghai Patentee before: Shanghai Feiyue Pharmaceutical Technology Co.,Ltd. Country or region before: China |
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| TR01 | Transfer of patent right |