CN216630825U

CN216630825U - Low-temperature chemical nickel liquid medicine preparation equipment

Info

Publication number: CN216630825U
Application number: CN202123174007.XU
Authority: CN
Inventors: 高升; 仝羽
Original assignee: Dongguan Zhongrui Surface Treatment Co ltd
Current assignee: Dongguan Zhongrui Surface Treatment Co ltd
Priority date: 2021-12-15
Filing date: 2021-12-15
Publication date: 2022-05-31
Anticipated expiration: 2031-12-15

Abstract

The utility model discloses a low-temperature chemical nickel liquid medicine preparation device, relates to the technical field of chemical liquid medicine preparation, and comprises the following steps: cooler bin, fixed slot, reaction cup and blocking lid, the top at the cooler bin is seted up to the fixed slot, reaction cup and blocking lid all slide and peg graft in the fixed slot, just the blocking lid activity cup joints the top at the reaction cup, the both sides difference fixedly connected with in the blocking lid top annotates liquid pipe and tail gas exhaust pipe, the inside of cooler bin is provided with cooling body, be provided with automatic rabbling mechanism in the reaction cup. According to the utility model, through the matching of the cooling mechanism, the stirring mechanism and the tail gas treatment structure, the problem that chemical reaction is easy to explode is solved, the requirements of safe production, energy conservation and emission reduction are met, the liquid is automatically stirred, the safety is improved, and meanwhile, the tail gas is purified and treated, so that the pollution to the outside is reduced.

Description

Low-temperature chemical nickel liquid medicine preparation equipment

Technical Field

The utility model relates to the technical field of chemical liquid medicine preparation, in particular to low-temperature chemical nickel liquid medicine preparation equipment.

Background

Chemical agents refer to agents that have an inhibitory effect on bacteria (agents that are beneficial for bacterial growth are attributed to nutrients). Chemical agents can inhibit or kill microorganisms and are thus used for the control of microbial growth. The chemical agents can be divided into bactericides and bacteriostats according to the action property; bactericides are chemical agents which destroy the metabolic function of bacteria and have a lethal effect, such as heavy metal ions, certain strong oxidants and the like. The bacteriostatic agent does not destroy the protoplasm of the bacteria, but only suppresses the synthesis of new cell substances, so that the bacteria cannot proliferate, such as sulfonamides, antibiotics and the like. Chemical disinfectants are used primarily to inhibit or kill microorganisms on surfaces, appliances, excretions and the surrounding environment. The bacteriostatic agent is commonly used on the body surface, such as skin, mucous membrane, wound and the like to prevent infection, and is also used for the anticorrosion effect of food, beverage and medicine, wherein chemical nickel liquid medicine is commonly used on objects in life, and a nickel layer electroplated by the nickel liquid medicine is compact, smooth, clean, good in corrosion resistance, good in discoloration prevention performance and excellent in binding force. The plating layer does not contain any toxic heavy metal, so the plating layer is environment-friendly and nontoxic and completely meets the rohs instruction standard, and the nickel electroplating liquid medicine is mainly suitable for the decorative, anticorrosive and wear-resistant plating layer of metal products requiring the plating layer not to contain heavy metal.

In the prior art, when chemical nickel liquid medicine is prepared, 30-50G/L of nickel sulfate, 40-50G/L of trisodium citrate dihydrate, 30-60G/L of sodium chloride and 8-15G/L of sodium hypophosphite are needed, the pH value is 7-10, the chemical nickel liquid medicine is prepared by mixing, but 30-50G/L of nickel sulfate, 40-50G/L of trisodium citrate dihydrate, 30-60G/L of sodium chloride and 8-15G/L of sodium hypophosphite can generate higher temperature when being sequentially mixed, the stability of acidic liquid at high temperature is poorer, and the situation of easy explosion is generated, through research, the liquid medicine can reduce the accident rate of production at low temperature on safety, a low-temperature system can obviously reduce energy consumption and medicament consumption, and the prior chemical liquid medicine generally needs to be stirred by a glass rod manually during preparation, the device is convenient for making different liquids fully contact and fuse, but the stirring has the defect that acidic liquid is easy to splash to hands of people, so that the hands of people are easy to corrode, great potential safety hazards exist, and in order to meet the requirements of safe production, energy conservation and emission reduction, the device for preparing the low-temperature chemical nickel liquid medicine is specially provided for solving the problems.

SUMMERY OF THE UTILITY MODEL

The utility model provides a low-temperature chemical nickel liquid medicine preparation device, which solves the problem that liquid medicine is easy to explode due to high-temperature reaction, and simultaneously solves the problem that liquid medicine is easy to splash to hands and corrode because liquid medicine is mostly not manually stirred during preparation of the traditional liquid medicine.

In order to solve the technical problem, the utility model provides a low-temperature chemical nickel liquid medicine preparation device, which comprises: cooler bin, fixed slot, reaction cup and blocking lid, the top at the cooler bin is seted up to the fixed slot, reaction cup and blocking lid all slide and peg graft in the fixed slot, just the blocking lid activity cup joints the top at the reaction cup, the both sides difference fixedly connected with in the blocking lid top annotates liquid pipe and tail gas exhaust pipe, the inside of cooler bin is provided with cooling body, be provided with automatic rabbling mechanism in the reaction cup.

Preferably, the cooling mechanism comprises a plurality of circulation pipes, a plurality of micro circulation water pumps, a plurality of cooling chambers, two heat conduction blocks and a plurality of heat dissipation holes, the plurality of cooling chambers are respectively arranged inside four sides of the cooling box, the plurality of circulation pipes are respectively fixedly arranged in the plurality of cooling chambers, cooling liquid is filled in the circulation pipes, the plurality of micro circulation water pumps are respectively arranged in the plurality of circulation pipes, the two heat conduction blocks are symmetrically and fixedly connected to the bottom wall in the fixing groove, the plurality of heat dissipation holes are respectively arranged in the cooling box, one ends of the heat dissipation holes are communicated with the fixing groove, the other ends of the heat dissipation holes are communicated with the outside, firstly, a raw material for preparing chemical nickel liquid medicine is introduced into the reaction cup, then the micro circulation water pumps are started to make the micro circulation water pumps circulate the cooling liquid in the circulation pipes, and the cooling liquid transfers the temperature of the liquid to the mixed liquid in the circulation pipes in the process, the chemical nickel liquid medicine preparation device can reduce the heat generated in the mixing reaction of chemical liquid medicine, is beneficial to solving the problem that the chemical reaction is easy to explode, and meets the requirements of safe production, energy conservation and emission reduction.

Preferably, rabbling mechanism includes axis of rotation, carousel, driving motor and a plurality of stirring rod, the axis of rotation rotates the bottom of connecting at the shutoff lid, just the axis of rotation is located the reaction cup, carousel fixed connection is in the bottom of axis of rotation, and is a plurality of the equal fixed connection of stirring rod is in the bottom of carousel, the inside of shutoff lid is provided with fixed chamber, driving motor fixed connection is at fixed intracavity, just driving motor's drive shaft is connected with the one end transmission of axis of rotation, opens driving motor, makes the axis of rotation drive carousel and a plurality of stirring rod rotate and stir mixed reaction liquid, makes mixed liquid fully contact and react, has avoided artifical manual stirring to lead to the problem that the hand is corroded by the liquid that splashes, has improved the security.

Preferably, the top of the reaction cup outer ring is provided with threads, the bottom of the blocking cover is provided with a threaded hole, and the blocking cover is sleeved on the top of the reaction cup through the threads, so that the sealing property is improved.

Preferably, the heat conduction block is made of copper, the thickness of the heat conduction block is 10mm, and the heat absorption capacity of the copper is strong, so that the liquid is cooled.

Preferably, be provided with the purification stopper in the exhaust pipe, the purification stopper includes filter pulp and active carbon board, just filter pulp and active carbon board fixed connection, the gaseous entering exhaust pipe that the liquid reaction produced is filtered by the purification stopper simultaneously in, reduces the pollution to the environment.

Preferably, the number of the circulating pipes, the micro circulating water pumps and the cooling cavities is four, and the number of the heat dissipation holes is six.

Preferably, the top of the liquid injection pipe is movably sleeved with a cover cap, the cover cap and the stirring rod are made of glass materials, and the acidic liquid is not easy to react with the glass, so that the service lives of the stirring rod and the cover cap can be prolonged.

Preferably, the front side of cooler bin is provided with electromagnetic control board, electromagnetic control board and the equal electric connection of miniature circulating water pump and driving motor help personnel to control miniature circulating water pump and driving motor.

Preferably, the both sides of cooler bin all fixedly connected with handle, the catching groove has all been seted up at both ends around the shutoff lid, the reaction cup of conveniently taking.

Compared with the related art, the low-temperature chemical nickel liquid medicine preparation equipment provided by the utility model has the following beneficial effects:

1. according to the chemical nickel liquid medicine preparation device, the raw materials for preparing the chemical nickel liquid medicine are firstly introduced into the reaction cup, then the micro circulating water pump is started to enable the micro circulating water pump to enable cooling liquid to flow in a circulating pipe in a circulating mode, the cooling liquid transfers the liquid temperature of the cooling liquid to the mixed liquid in the process, the liquid temperature is reduced, meanwhile, the temperature generated by the reaction liquid is transferred to the heat conduction block through the bottom of the reaction cup, finally, the heat conduction block absorbs the heat and then discharges the heat to the outside through the heat dissipation holes, the reaction liquid in the reaction cup can be controlled to be 40-50 ℃, and the chemical nickel liquid medicine preparation device can cool the heat generated in the mixing reaction of the chemical liquid medicine, is beneficial to solving the problem that the chemical reaction is easy to explode, and meets the requirements of safe production, energy conservation and emission reduction.

2. According to the utility model, the driving motor is started, the rotating shaft drives the rotating disc and the stirring rods to rotate and stir the mixed reaction liquid, so that the mixed liquid is fully contacted and reacted, finally, gas generated by liquid reaction enters the tail gas exhaust pipe and is filtered by the purification plug, the problem that liquid medicine is easy to splash to hands and corrode because liquid medicine is not manually stirred mostly in the existing liquid medicine preparation process is solved, the liquid is automatically stirred, the safety is improved, and meanwhile, the tail gas is purified and treated.

Drawings

FIG. 1 is a schematic perspective view of an external device for preparing a low-temperature chemical nickel solution;

FIG. 2 is a schematic plan view of the interior of a cryogenic chemical nickel solution preparation apparatus;

FIG. 3 is a schematic view of a plan view of the interior of a cooling chamber of a cryogenic chemical nickel solution preparation apparatus;

fig. 4 is an enlarged view of a portion a in fig. 2.

Reference numbers in the figures: 1. a cooling tank; 2. fixing grooves; 3. a reaction cup; 4. a blocking cover; 5. a circulation pipe; 6. a micro circulating water pump; 7. a cooling chamber; 8. a heat conducting block; 9. heat dissipation holes; 10. a liquid injection pipe; 11. a tail gas exhaust pipe; 12. a purge plug; 13. a rotating shaft; 14. a turntable; 15. a stirring rod; 16. the motor is driven.

Detailed Description

Reference will now be made in detail to embodiments of the present invention, examples of which are illustrated in the accompanying drawings, wherein like reference numerals refer to the same or similar elements or elements having the same or similar function throughout. The embodiments described below with reference to the accompanying drawings are illustrative only for the purpose of explaining the present invention and are not to be construed as limiting the present invention.

In the description of the present invention, it should be understood that if the terms "center", "longitudinal", "lateral", "length", "width", "thickness", "upper", "lower", "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outer", "clockwise", "counterclockwise", etc. are referred to, they refer to the orientation or positional relationship shown in the drawings, and are used for convenience of description and simplicity of description, but do not indicate or imply that the device or element referred to must have a particular orientation, be constructed and operated in a particular orientation, and thus should not be construed as limiting the present invention. Furthermore, the terms "first", "second" and "first" are used for descriptive purposes only and are not to be construed as indicating or implying relative importance or implicitly indicating the number of technical features indicated. Thus, features defined as "first", "second", may explicitly or implicitly include one or more of the described features. In the description of the present invention, "a plurality" means two or more unless specifically defined otherwise.

In the description of the present invention, it should be noted that the terms "mounted," "connected," and "connected" are to be construed broadly and may be, for example, fixedly connected, detachably connected, or integrally connected unless otherwise explicitly stated or limited. Either mechanically or electrically. Either directly or indirectly through intervening media, either internally or in any other relationship. The specific meanings of the above terms in the present invention can be understood by those skilled in the art according to specific situations.

In a first embodiment, as shown in fig. 1-4, a low temperature chemical nickel solution manufacturing apparatus comprises: the reaction device comprises a cooling box 1, a fixing groove 2, a reaction cup 3 and a blocking cover 4, wherein the fixing groove 2 is formed in the top of the cooling box 1, the reaction cup 3 and the blocking cover 4 are both slidably inserted into the fixing groove 2, the blocking cover 4 is movably sleeved on the top of the reaction cup 3, a liquid injection pipe 10 and a tail gas exhaust pipe 11 are fixedly connected to two sides of the top of the blocking cover 4 respectively, a cooling mechanism is arranged inside the cooling box 1, and an automatic stirring mechanism is arranged in the reaction cup 3;

the cooling mechanism comprises a plurality of circulating pipes 5, a plurality of micro circulating water pumps 6, a plurality of cooling cavities 7, two heat-conducting blocks 8 and a plurality of radiating holes 9, wherein the plurality of cooling cavities 7 are respectively arranged inside four sides of the cooling box 1, the plurality of circulating pipes 5 are respectively and fixedly arranged in the plurality of cooling cavities 7, cooling liquid is filled in the circulating pipes 5, the plurality of micro circulating water pumps 6 are respectively arranged in the plurality of circulating pipes 5, the two heat-conducting blocks 8 are symmetrically and fixedly connected to the bottom wall in the fixing groove 2, the plurality of radiating holes 9 are respectively arranged in the cooling box 1, one end of each radiating hole 9 is communicated with the fixing groove 2, the other end of each radiating hole 9 is communicated with the outside, firstly, 30-50G/L nickel sulfate, 40-50G/L trisodium citrate dihydrate, 30-60G/L sodium chloride and 8-15G/L sodium hypophosphite are mixed according to a proper proportion, and acid and alkali are introduced into the liquid injection pipe 10 with PH7-10, then the liquid falls into the reaction cup 3, then the micro circulating water pump 6 is started to make the micro circulating water pump 6 circularly flow the cooling liquid in the circulating pipe 5, the cooling liquid transfers the liquid temperature to the reaction cup 3 through the side wall of the cooling box 1 in the process, then the liquid temperature is transferred to the mixed liquid at low temperature, the temperature generated by the reaction liquid in the previous process is transferred to the heat conduction block 8 through the bottom of the reaction cup 3, finally the heat conduction block 8 absorbs the heat and then discharges the heat to the outside through the heat dissipation holes 9, the cooling structure can control the reaction liquid in the reaction cup 3 at 40-50 ℃, and the safety of preparing the chemical nickel liquid medicine is improved.

Embodiment two, on the basis of embodiment one, the rabbling mechanism includes axis of rotation 13, carousel 14, driving motor 16 and a plurality of stirring rod 15, axis of rotation 13 rotates the bottom of connecting at shutoff lid 4, and axis of rotation 13 is located reaction cup 3, carousel 14 fixed connection is in the bottom of axis of rotation 13, the equal fixed connection of a plurality of stirring rod 15 is in the bottom of carousel 14, the inside of shutoff lid 4 is provided with fixed chamber, driving motor 16 fixed connection is in fixed intracavity, and driving motor 16's drive shaft is connected with the one end transmission of axis of rotation 13, open driving motor 16, make axis of rotation 13 drive carousel 14 rotate, make stirring rod 15 follow the rotation and stir liquid in reaction cup 3, make mixed liquid fully contact and react.

Third, on the basis of the first embodiment, the top of the outer ring of the reaction cup 3 is provided with a thread, the bottom of the blocking cover 4 is provided with a threaded hole, and the blocking cover 4 is sleeved on the top of the reaction cup 3 through the thread, so that the sealing performance is improved.

In the fourth embodiment, on the basis of the first embodiment, the heat conducting block 8 is made of copper, and the thickness of the heat conducting block 8 is 10mm, so that the heat absorbing capacity of the copper is strong, thereby being beneficial to cooling the liquid.

Fifth embodiment, on the basis of first embodiment, be provided with purification plug 12 in the exhaust gas pipe 11, purification plug 12 includes filter pulp and active carbon plate, and filter pulp and active carbon plate fixed connection, and the gaseous entering exhaust gas pipe 11 that the liquid reaction produced is filtered by purification plug 12 simultaneously in, reduces the pollution to the environment.

In the sixth embodiment, on the basis of the first embodiment, the number of the circulating pipes 5, the micro circulating water pumps 6 and the cooling cavities 7 is four, and the number of the heat dissipation holes 9 is six.

In the seventh embodiment, on the basis of the second embodiment, the cap is movably sleeved on the top of the liquid injection pipe 10, and the cap and the stirring rod 15 are made of glass, so that the acidic liquid is not easy to react with the glass, and the service lives of the stirring rod 15 and the cap can be prolonged.

Eighth embodiment, on the basis of second embodiment, the front side of cooling box 1 is provided with electromagnetic control board, and electromagnetic control board and miniature circulating water pump 6 and driving motor 16 all electric connection help personnel to control miniature circulating water pump 6 and driving motor 16.

Ninth, on the basis of the first embodiment, the handles are fixedly connected to both sides of the cooling box 1, and the front end and the rear end of the blocking cover 4 are provided with fastening grooves, so that the reaction cup 3 can be conveniently taken.

The working principle is as follows:

when the temperature of the chemical agent in the reaction cup 3 needs to be reduced:

the first step is as follows: firstly, 30-50G/L of nickel sulfate, 40-50G/L of trisodium citrate dihydrate, 30-60G/L of sodium chloride and 8-15G/L of sodium hypophosphite are introduced into a liquid injection pipe 10 according to a proper proportion, the acid-base pH is 7-10, and then the liquid falls into a reaction cup 3;

the second step is that: then, the micro circulating water pump 6 is started, so that the micro circulating water pump 6 enables cooling liquid to circularly flow in the circulating pipe 5, the cooling liquid transmits the liquid temperature of the cooling liquid to the reaction cup 3 through the side wall of the cooling box 1 in the process, and then the low temperature is transmitted into the mixed liquid, so that the liquid temperature is reduced;

the third step: in the process, the temperature generated by the reaction liquid is transferred to the heat conducting block 8 through the bottom of the reaction cup 3, and finally the heat conducting block 8 absorbs the heat and then discharges the heat to the outside through the heat dissipation holes 9, and the cooling structure can control the temperature of the reaction liquid in the reaction cup 3 to be 40-50 ℃.

When the mixture in the reaction cup 3 needs to be stirred:

the first step is as follows: starting a driving motor 16 to enable a rotating shaft 13 to drive a rotating disc 14 to rotate, so that a stirring rod 15 rotates and stirs liquid in the reaction cup 3, and the mixed liquid is fully contacted and reacted;

the second step is that: finally, gas generated by liquid reaction enters the tail gas exhaust pipe 11 and is filtered by the purifying plug 12, so that harmful substances in the gas are adsorbed and blocked by the activated carbon plate and the filter cotton.

It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.

Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the utility model, the scope of which is defined in the appended claims and their equivalents.

Claims

1. A low-temperature chemical nickel liquid medicine preparation device comprises: cooler bin (1), fixed slot (2), reaction cup (3) and shutoff lid (4), its characterized in that, the top at cooler bin (1) is seted up in fixed slot (2), reaction cup (3) and shutoff lid (4) are all slided and are pegged graft in fixed slot (2), just shutoff lid (4) activity is cup jointed at the top of reaction cup (3), liquid pipe (10) and tail gas exhaust pipe (11) are annotated to the both sides difference fixedly connected with at shutoff lid (4) top, the inside of cooler bin (1) is provided with cooling body, be provided with automatic rabbling mechanism in reaction cup (3).

2. The apparatus for preparing low-temperature chemical nickel solution according to claim 1, wherein the cooling mechanism comprises a plurality of circulation pipes (5), a plurality of micro circulation water pumps (6), a plurality of cooling chambers (7), two heat conduction blocks (8) and a plurality of heat dissipation holes (9), the plurality of cooling chambers (7) are respectively disposed inside four sides of the cooling tank (1), the plurality of circulation pipes (5) are respectively and fixedly disposed in the plurality of cooling chambers (7), the circulation pipes (5) are filled with cooling liquid, the plurality of micro circulation water pumps (6) are respectively disposed in the plurality of circulation pipes (5), the two heat conduction blocks (8) are symmetrically and fixedly connected to the bottom wall of the fixing groove (2), the plurality of heat dissipation holes (9) are all disposed in the cooling tank (1), one end of the heat conduction blocks (9) is communicated with the fixing groove (2), and the other end of the heat dissipation hole (9) is communicated with the outside.

3. The cryogenic chemical nickel liquid preparation equipment according to claim 1, wherein the stirring mechanism comprises a rotating shaft (13), a rotating disc (14), a driving motor (16) and a plurality of stirring rods (15), the rotating shaft (13) is rotatably connected to the bottom of the blocking cover (4), the rotating shaft (13) is located in the reaction cup (3), the rotating disc (14) is fixedly connected to the bottom end of the rotating shaft (13), the stirring rods (15) are fixedly connected to the bottom of the rotating disc (14), a fixed cavity is arranged inside the blocking cover (4), the driving motor (16) is fixedly connected to the fixed cavity, and a driving shaft of the driving motor (16) is in transmission connection with one end of the rotating shaft (13).

4. The low-temperature chemical nickel liquid medicine preparation equipment as claimed in claim 1, wherein the top of the outer ring of the reaction cup (3) is provided with threads, the bottom of the blocking cover (4) is provided with threaded holes, and the blocking cover (4) is in threaded sleeve connection with the top of the reaction cup (3).

5. The apparatus for preparing the chemical nickel reagent solution at low temperature according to claim 2, wherein the heat conducting block (8) is made of copper, and the thickness of the heat conducting block (8) is 10 mm.

6. The low-temperature chemical nickel liquid medicine preparation equipment according to claim 1, characterized in that a purification plug (12) is arranged in the tail gas exhaust pipe (11), the purification plug (12) comprises filter cotton and an activated carbon plate, and the filter cotton is fixedly connected with the activated carbon plate.

7. The apparatus for preparing chemical nickel reagent solution at low temperature according to claim 2, wherein the number of the circulation pipe (5), the micro circulation water pump (6) and the cooling chamber (7) is four, and the number of the heat dissipation holes (9) is six.

8. The equipment for preparing the low-temperature chemical nickel liquid medicine is characterized in that a cover cap is movably sleeved on the top of the liquid injection pipe (10), and the cover cap and the stirring rod (15) are made of glass materials.

9. The apparatus for preparing nickel reagent solution for low temperature chemical according to claim 3, wherein the front side of the cooling tank (1) is provided with an electromagnetic control board, and the electromagnetic control board is electrically connected with the micro circulating water pump (6) and the driving motor (16).

10. The low-temperature chemical nickel liquid medicine preparation equipment as claimed in claim 1, wherein handles are fixedly connected to both sides of the cooling tank (1), and catching grooves are formed in both the front and rear ends of the blocking cover (4).