CN216604057U - Concentration device for calcium glucarate crystallization mother liquor - Google Patents

Concentration device for calcium glucarate crystallization mother liquor Download PDF

Info

Publication number
CN216604057U
CN216604057U CN202123235224.5U CN202123235224U CN216604057U CN 216604057 U CN216604057 U CN 216604057U CN 202123235224 U CN202123235224 U CN 202123235224U CN 216604057 U CN216604057 U CN 216604057U
Authority
CN
China
Prior art keywords
pipe
concentration kettle
concentration
fixedly connected
wall
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN202123235224.5U
Other languages
Chinese (zh)
Inventor
毕建华
柴炯
赵新宇
陈宁存
李刚
宋晴
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shandong Huishengtang Biomedical Co ltd
Original Assignee
Shandong Huishengtang Biomedical Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shandong Huishengtang Biomedical Co ltd filed Critical Shandong Huishengtang Biomedical Co ltd
Priority to CN202123235224.5U priority Critical patent/CN216604057U/en
Application granted granted Critical
Publication of CN216604057U publication Critical patent/CN216604057U/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/10Process efficiency

Landscapes

  • Mixers Of The Rotary Stirring Type (AREA)

Abstract

The utility model relates to the field of crystallization mother liquor concentration, in particular to a concentration device of calcium glucarate crystallization mother liquor, which comprises a concentration kettle, wherein the lower part of the concentration kettle is fixedly sleeved with a steam sleeve, and the bottom of the steam sleeve is fixedly connected with a discharge pipe valve communicated with the bottom of the concentration kettle inside the steam sleeve. This kind of enrichment facility of calcium gluconate crystallization mother liquor, setting through the cooling jacket, intercept rising steam, the cooperation of rethread water pump connecting pipe, can carry the outside coolant liquid to the tube seat in the cooling jacket, make it condense into the drop of water to steam cooling rapidly, and converge with the water receiving tank along the slope of cooling jacket inner wall in, discharge by the drain pipe again, avoid the drop of condensation to drip and dilute the material, the effectual concentration efficiency that has improved, can stir the material from top to bottom through setting up of hob, improve heating efficiency, strike off its inner wall through the scraper blade with concentration cauldron inner wall matched with again, can effectually avoid remaining of inner wall.

Description

Concentration device for calcium glucarate crystallization mother liquor
Technical Field
The utility model relates to the field of crystallization mother liquor concentration, in particular to a concentration device of calcium glucarate crystallization mother liquor.
Background
The calcium glucarate has wide functions and application, can be used for preparing biodegradable detergents and metal complexing agents, can also be used for preparing biodegradable high-tensile-strength fibers, films, adhesives and plant fertilizers, and is newly researched and found that the glucaric acid also has the functions of resisting tumors and reducing cholesterol, and the main action mechanism of the glucaric acid is probably to enhance the detoxification capability of organisms to toxins and carcinogens.
The following problems in the prior art are not well solved: 1. most of the existing concentration devices remove redundant water in a heating and evaporating mode, but the existing device has low steam discharge efficiency, so that water drops condensed by steam remained in the device can drip into materials again, and the concentration efficiency is low; 2. and after the material is concentrated, the consistency becomes high, and the material is easy to adhere to the inner wall of the tank body, so that the cleaning is inconvenient.
SUMMERY OF THE UTILITY MODEL
The utility model aims to provide a concentration device of calcium glucarate crystallization mother liquor, which solves the problems that condensed water drops drop into a material and are mixed with the material when steam is not discharged in time, the concentration efficiency is low, and the material is adhered to the inner wall of a tank body, so that the cleaning is inconvenient. In order to achieve the purpose, the utility model provides the following technical scheme: a concentration device of calcium glucarate crystallization mother liquor, which comprises a concentration kettle, wherein the lower part of the concentration kettle is fixedly sleeved with a steam sleeve, and the bottom of the steam sleeve is fixedly connected with a discharge pipe valve communicated with the bottom of the concentration kettle inside the steam sleeve, the two sides of the outer wall of the steam sleeve are respectively and fixedly connected with an air inlet pipe valve and an exhaust pipe valve communicated with the inside of the steam sleeve, two sides of the concentration kettle are respectively and fixedly connected with a feed pipe valve and a drain pipe which are communicated with the interior of the concentration kettle, a top cover is movably clamped at the top of the concentration kettle, a motor is fixedly connected at the top of the top cover, a scraper is movably lapped in the concentration kettle, the middle part of the scraper is fixedly connected with a screw rod, the top of the screw rod is movably inserted with a connecting rod, the output end of the motor penetrates through the top cover and is fixedly connected with the top of the connecting rod below the top cover, and a cooling mechanism is movably lapped in the concentration kettle;
cooling body includes the cooling jacket, and cooling jacket activity overlap joint is in concentrated cauldron, the pipe box has been seted up in the cooling jacket, and the edge fixedly connected with water receiving tank of cooling jacket bottom, and one side of water receiving tank set up and run through to its inside through-hole, the top activity of cooling jacket is pegged graft and is had the water pump connecting pipe that runs through to its inside pipe box both ends, and the top of water pump connecting pipe runs through the top cap and extends to its avris.
Preferably, the inner wall of the concentration kettle is provided with an inner step matched with the cooling cover, and one side of the inner step is provided with a notch matched with the scraper.
Preferably, the bottom of the inner wall of the concentration kettle is arc-shaped, and the side section of the scraper is of a U-shaped structure matched with the arc at the bottom of the inner wall of the concentration kettle.
Preferably, the horizontal height of the drain pipe is matched with the water receiving tank, and the top end of the drain pipe is communicated with the through hole.
Preferably, the water pump connecting pipe consists of a water conveying pipe and a water return pipe, and the top ends of the water conveying pipe and the water return pipe are respectively and fixedly connected with an output pipe and an input pipe of the cooling water pump.
Preferably, the outer wall of the connecting rod is fixedly connected with a convex block matched with the concave slot at the top end of the spiral rod, and the cooling cover is movably sleeved on the spiral rod.
Compared with the prior art, the utility model has the beneficial effects that:
according to the utility model, the cooling cover is arranged to intercept rising steam, and then the outside cooling liquid can be conveyed into the pipe groove in the cooling cover through the matching of the water pump connecting pipe, so that the steam is rapidly cooled and condensed into water drops, and the water drops are converged along the gradient of the inner wall of the cooling cover and are discharged from the water receiving groove and the water discharging pipe, so that the condensed water drops are prevented from dropping and diluting materials, and the concentration efficiency is effectively improved.
According to the utility model, the material can be stirred up and down through the arrangement of the screw rod, the heating efficiency is improved, the inner wall of the concentration kettle is scraped through the scraper matched with the inner wall of the concentration kettle, the residue of the inner wall can be effectively avoided, the cooling mechanism, the screw rod and the scraper can be easily detached through arranging the inner step with the notch on the inner wall of the concentration kettle, the cleaning is convenient, meanwhile, the replacement of parts is convenient, the structure is simple, the occupied area is small, and the mechanical cost is low.
Drawings
FIG. 1 is a perspective view of the structure of the present invention;
FIG. 2 is a front cross-sectional view of the structure of the present invention;
FIG. 3 is a perspective cross-sectional view of a cooling mechanism of the present invention;
FIG. 4 is a top cross-sectional view of a structural duct of the present invention;
fig. 5 is a side view of the water pump connecting pipe of the present invention.
In the figure: 1. a concentration kettle; 2. a steam sleeve; 3. a discharge tube valve; 4. an intake pipe valve; 5. an exhaust pipe valve; 6. a feed pipe valve; 7. a drain pipe; 8. a top cover; 9. a motor; 10. a squeegee; 11. a screw rod; 12. a connecting rod; 13. a cooling mechanism; 1301. a cooling jacket; 1302. a pipe groove; 1303. a water receiving tank; 1304. a through hole; 1305. and a water pump connecting pipe.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be obtained by workers skilled in the art without any inventive work based on the embodiments of the present invention, are within the scope of the present invention.
Referring to fig. 1 to 5, the present invention provides a technical solution: a concentration device of calcium glucarate crystallization mother liquor, which comprises a concentration kettle 1, wherein the lower part of the concentration kettle 1 is fixedly sleeved with a steam sleeve 2, and the bottom of the steam sleeve 2 is fixedly connected with a discharge pipe valve 3 communicated with the bottom of the concentration kettle 1 inside the steam sleeve, the two sides of the outer wall of the steam sleeve 2 are respectively and fixedly connected with an air inlet pipe valve 4 and an air exhaust pipe valve 5 communicated with the inside of the steam sleeve, the two sides of the concentration kettle 1 are respectively and fixedly connected with a feed pipe valve 6 and a drain pipe 7 communicated with the inside of the concentration kettle, a top cover 8 is movably clamped at the top of the concentration kettle 1, the top of the top cover 8 is fixedly connected with a motor 9, a scraper 10 is movably lapped in the concentration kettle 1, a screw rod 11 is fixedly connected to the middle part of the scraper 10, a connecting rod 12 is movably inserted and connected to the top of the screw rod 11, the output end of the motor 9 penetrates through the top cover 8 and is fixedly connected with the top of the connecting rod 12 below the top cover, and a cooling mechanism 13 is movably lapped in the concentration kettle 1;
cooling body 13 includes cooling jacket 1301, and cooling jacket 1301 activity overlap joint is in concentrated cauldron 1, has seted up tub 1302 in the cooling jacket 1301, and the marginal fixedly connected with water receiving tank 1303 of cooling jacket 1301 bottom, and the through-hole 1304 that runs through to its inside is seted up to one side of water receiving tank 1303, and the top activity of cooling jacket 1301 is pegged graft and is had the water pump connecting pipe 1305 that runs through to its inside tub 1302 both ends, and the top of water pump connecting pipe 1305 runs through top cap 8 and extends to its avris.
In this embodiment, as shown in fig. 1, fig. 2, fig. 3, fig. 4, and fig. 5, an inner wall of the concentration kettle 1 is provided with an inner step which is engaged with the cooling jacket 1301, and one side of the inner step is provided with a notch which is engaged with the scraper 10.
In this embodiment, as shown in fig. 1, fig. 2, circular arc processing is done to the bottom of 1 inner wall of concentrated cauldron, the side cross-section of scraper blade 10 is the U type structure of the circular arc of 1 inner wall bottom of concentrated cauldron of cooperation, can stir the material from top to bottom through setting up of hob 11, improve heating efficiency, rethread strikes off its inner wall with 1 inner wall matched with scraper blade 10 of concentrated cauldron, can effectually avoid remaining of inner wall, set up the interior step that has the breach through 1 inner wall of concentrated cauldron, can easily dismantle cooling body 13, hob 11 and scraper blade 10, when being convenient for wash, also be convenient for change spare part, moreover, the steam generator is simple in structure, and area is less, mechanical cost is lower.
In this embodiment, as shown in fig. 1, fig. 2, fig. 3, fig. 4, and fig. 5, the horizontal height of the drain pipe 7 is matched with the water receiving tank 1303, and the top end of the drain pipe 7 is communicated with the through hole 1304, the rising steam is intercepted by the arrangement of the cooling cover 1301, and then the external cooling liquid is conveyed to the pipe channel 1302 in the cooling cover 1301 by matching with the 1305 of the water pump connecting pipe, so that the steam is rapidly cooled and condensed into water drops, and the water drops are converged and discharged from the water receiving tank 1303 along the slope of the inner wall of the cooling cover 1301 and then discharged by the drain pipe 7, thereby preventing the condensed water drops from dropping and diluting the material, and effectively improving the concentration efficiency.
In this embodiment, as shown in fig. 2 and 5, the water pump connecting pipe 1305 is composed of a water pipe and a water return pipe, and the top ends of the water pipe and the water return pipe are respectively and fixedly connected to the output pipe and the input pipe of the cooling water pump.
In this embodiment, as shown in fig. 2 and 3, the outer wall of the connecting rod 12 is fixedly connected with a convex block matched with the concave slot at the top end of the spiral rod 11, and the cooling cover 1301 is movably sleeved on the spiral rod 11.
The use method and the advantages of the utility model are as follows: when the concentration device of the calcium glucarate crystallization mother liquor is used, the working process is as follows:
as shown in fig. 1, fig. 2, fig. 3, fig. 4 and fig. 5, firstly, the solution enters the concentration kettle 1 through the feed pipe valve 6, and at the same time, the high temperature steam enters the gap between the steam sleeve 2 and the concentration kettle 1 through the air inlet pipe valve 4 to be heated, the starting motor 9 drives the screw rod 11 and the scraper 10 to synchronously rotate through the connecting rod 12, the material can be stirred up, down, left and right, the heating efficiency is improved, after the solution is heated, the rising steam is intercepted by the cooling cover 1301, and simultaneously, under the cooperation of the water pump connecting pipe 1305, the external cooling liquid can be conveyed to the pipe channel 1302 in the cooling cover 1301, the cooling cover 1301 is wholly and circularly cooled, the steam adhered to the inner wall is cooled and condensed into water drops, and converged to the water receiving channel along the slope of the inner wall of the cooling cover 1301, and then is intensively discharged through the water discharge pipe 7, so that a large amount of condensed water drops can be effectively prevented from dropping and diluting the material, the scraper 10 adhered to the inner wall of the concentration kettle 1 can scrape the residual material, and through the concentrated cauldron 1 inner wall set up the interior step that has the breach, can easily dismantle cooling body 13, hob 11 and scraper blade 10, when being convenient for wash, also be convenient for change spare part, simple structure, and area is less, and mechanical cost is lower.
The foregoing shows and describes the general principles, essential features, and advantages of the utility model. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, and the preferred embodiments of the present invention are described in the above embodiments and the description, and are not intended to limit the present invention. The scope of the utility model is defined by the appended claims and equivalents thereof.

Claims (6)

1. The utility model provides a enrichment facility of calcium glucarate crystallization mother liquor, includes concentrated cauldron (1), its characterized in that: the lower part of the concentration kettle (1) is fixedly sleeved with a steam sleeve (2), the bottom of the steam sleeve (2) is fixedly connected with a discharge pipe valve (3) communicated with the bottom of the concentration kettle (1) inside the concentration kettle, two sides of the outer wall of the steam sleeve (2) are respectively fixedly connected with an air inlet pipe valve (4) and an air exhaust pipe valve (5) communicated with the inside of the steam sleeve, two sides of the concentration kettle (1) are respectively fixedly connected with an air inlet pipe valve (6) and an air exhaust pipe (7) communicated with the inside of the concentration kettle, the top of the concentration kettle (1) is movably clamped with a top cover (8), the top of the top cover (8) is fixedly connected with a motor (9), a scraper (10) is movably lapped in the concentration kettle (1), the middle part of the scraper (10) is fixedly connected with a screw rod (11), the top of the screw rod (11) is movably spliced with a connecting rod (12), the output end of the motor (9) penetrates through the top cover (8) and is fixedly connected with the top of the connecting rod (12) below the top of the concentration kettle, a cooling mechanism (13) is movably lapped in the concentration kettle (1);
cooling body (13) are including cooling cover (1301), and cooling cover (1301) activity overlap joint is in concentrated cauldron (1), pipe box (1302) have been seted up in cooling cover (1301), and the edge fixedly connected with water receiving tank (1303) of cooling cover (1301) bottom, and water receiving tank (1303) one side set up run through to its inside through-hole (1304), the top activity of cooling cover (1301) is pegged graft and is had water pump connecting pipe (1305) that run through to its inside pipe box (1302) both ends, and the top of water pump connecting pipe (1305) runs through top cap (8) and extends to its avris.
2. The apparatus for concentrating a mother liquor for calcium glucarate crystallization according to claim 1, characterized in that: the inner wall of the concentration kettle (1) is provided with an inner step matched with the cooling cover (1301), and one side of the inner step is provided with a notch matched with the scraper (10).
3. The apparatus for concentrating a mother liquor for calcium glucarate crystallization according to claim 1, characterized in that: the bottom of the inner wall of the concentration kettle (1) is processed into an arc shape, and the side section of the scraper (10) is of a U-shaped structure matched with the arc shape at the bottom of the inner wall of the concentration kettle (1).
4. The apparatus for concentrating a mother liquor for calcium glucarate crystallization according to claim 1, characterized in that: the horizontal height of the drain pipe (7) is matched with the water receiving tank (1303), and the top end of the drain pipe (7) is communicated with the through hole (1304).
5. The apparatus for concentrating a mother liquor for calcium glucarate crystallization according to claim 1, characterized in that: the water pump connecting pipe (1305) is composed of a water conveying pipe and a water return pipe, and the top ends of the water conveying pipe and the water return pipe are fixedly connected with an output pipe and an input pipe of the cooling water pump respectively.
6. The apparatus for concentrating a mother liquor for calcium glucarate crystallization according to claim 1, characterized in that: the outer wall fixedly connected with of connecting rod (12) and hob (11) top concave slot matched with lug, cooling cover (1301) activity cup joints on hob (11).
CN202123235224.5U 2021-12-21 2021-12-21 Concentration device for calcium glucarate crystallization mother liquor Active CN216604057U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202123235224.5U CN216604057U (en) 2021-12-21 2021-12-21 Concentration device for calcium glucarate crystallization mother liquor

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202123235224.5U CN216604057U (en) 2021-12-21 2021-12-21 Concentration device for calcium glucarate crystallization mother liquor

Publications (1)

Publication Number Publication Date
CN216604057U true CN216604057U (en) 2022-05-27

Family

ID=81704601

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202123235224.5U Active CN216604057U (en) 2021-12-21 2021-12-21 Concentration device for calcium glucarate crystallization mother liquor

Country Status (1)

Country Link
CN (1) CN216604057U (en)

Similar Documents

Publication Publication Date Title
CN211169934U (en) Miniature evaporation crystallization equipment
CN108479477A (en) A kind of liquid waste mixing apparatus with cleaning function
EP1749086B1 (en) Facility parts cleaning solution for processing of (meth)acrylic acid and/or (meth)acrylic esters and cleaning method using said cleaning solution
CN212680091U (en) High-efficient rotatory wiped film evaporator
CN216604057U (en) Concentration device for calcium glucarate crystallization mother liquor
CN220237775U (en) Three-effect evaporation system reaction tank
CN212395933U (en) Spiral stirring formula crystallization kettle
CN210751328U (en) Aminoacetic acid by-product ammonium chloride recovery device
CN202778541U (en) Anti-foam vacuum rotary evaporator
CN218841744U (en) Water receiving tank device for treating m-benzene resin wastewater
CN216571585U (en) Constant-temperature circulating distillation device for producing beer
CN207679752U (en) A kind of sterilization cleaning device of food pipeline
CN205933523U (en) High salt organic wastewater of EDTA and resources recovery system
CN213643168U (en) Evaporative crystallization device for sodium molybdate production
CN212741286U (en) Distilling machine for processing selenium-rich lake wine
CN204848706U (en) Device of multiple amino acid is prepared to feather
CN207774989U (en) A kind of waste liquid materializing strategy system
CN209464976U (en) A kind of bath of glass Preparation equipment
CN209098287U (en) A kind of chemical waste liquid specification recovery processing device
CN108794301A (en) A kind of refining plant of biological diesel oil byproduct crude glycerine
CN208029436U (en) A kind of intelligence wine-growing Irrigation and fertilization system
CN216062095U (en) Miniature evaporation crystallization equipment with stable operation
CN110368878A (en) A kind of gas liquid phase reactor being used to prepare sulphite
CN201744193U (en) Waste-liquid cleaning recycling device
CN217818346U (en) Liquid ammonia evaporimeter coil pipe belt cleaning device

Legal Events

Date Code Title Description
GR01 Patent grant
GR01 Patent grant