CN216538503U - Conical separation tower - Google Patents

Conical separation tower Download PDF

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CN216538503U
CN216538503U CN202122824894.4U CN202122824894U CN216538503U CN 216538503 U CN216538503 U CN 216538503U CN 202122824894 U CN202122824894 U CN 202122824894U CN 216538503 U CN216538503 U CN 216538503U
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pipe
tower body
partition plate
resin
material discharge
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CN202122824894.4U
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高康
陈琳媛
赵浩竹
张�浩
戎宇舟
孙霞
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China Electronics Innovation Environmental Technology Co ltd
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China Electronics Innovation Environmental Technology Co ltd
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Abstract

The embodiment of the utility model provides a conical separation tower for separating or regenerating anion and cation resins in polishing resins, which comprises: the tower body, the frustum, the partition plate and the cylinder body; the frustum comprises a large-diameter port and a small-diameter port; one end of the tower body is a closed end, and the other end of the tower body is fixedly connected with the large-diameter port; one side of the partition plate covers the small-diameter port, and the other side of the partition plate is fixedly connected with one end of the cylinder; a plurality of water caps are arranged on the partition plate; the other end of the cylinder body is provided with a backwashing port; the tower body is provided with a material inlet, a material outlet and a water inlet; the water inlet is provided with the water inlet pipe; the material discharge port is provided with a first material discharge pipe and a second material discharge pipe. The embodiment of the utility model provides a conical separation tower which can be suitable for separating different types and proportions of resin, and has wide adaptability and low cost.

Description

Conical separation tower
Technical Field
The utility model belongs to the field of polishing resin separation and regeneration, and particularly relates to a conical separation tower.
Background
In recent years, domestic polishing resin is mostly disposable, and basically is replaced regularly without regeneration and recovery treatment, a large amount of polishing resin is treated as hazardous waste every year, and a large amount of high-value recoverable resources are wasted.
Different from the common mixed bed resin for in vivo regeneration, the cation and anion resin in the polishing resin needs to be regenerated separately, so that the influence of the cross contamination of the cation and anion resin on the quality of the regenerated effluent is avoided. However, in the existing resin separation technology, a separation tower is used for outputting resin through a hole on the side surface, the method has the problem of large mixed resin amount, one set of separation device can only be suitable for fixed resin amount and proportion of positive and negative resin, and the replaced polishing resin is split charged by small barrels in the actual use process, so that the proportion of each barrel of resin is easily different. In the other separation tower, resin is output from a hole at the bottom of the tower, and in the method, the layered interfaces of the cation and anion resin can sink and disorder when the resin is output, so that the cation and anion resin can not be completely separated.
Disclosure of Invention
Aiming at the defects in the prior art, the embodiment of the utility model provides a conical separation tower device which can be suitable for separating and regenerating anion-cation resin in polishing resin of different types and proportions, and has wide adaptability and low cost. In order to achieve the technical purpose, the embodiment of the utility model adopts the technical scheme that:
the embodiment of the utility model provides a conical separation tower for separating or regenerating anion and cation resins in polishing resins, which comprises:
the tower body, the frustum, the partition plate and the cylinder body;
the frustum comprises a large-diameter port and a small-diameter port;
one end of the tower body is a closed end, and the other end of the tower body is fixedly connected with the large-diameter port;
one side of the partition plate covers the small-diameter port, and the other side of the partition plate is fixedly connected with one end of the cylinder; a plurality of water caps are arranged on the partition plate;
the other end of the cylinder body is provided with a backwashing port;
the tower body is provided with a material inlet, a material outlet and a water inlet;
the water inlet is provided with the inlet tube, through the inlet tube can be to leading to water in the tower body.
The material discharge port is provided with a first material discharge pipe and a second material discharge pipe;
the first material discharge pipe comprises a first end and a second end, and the first end extends out of the tower body through the material discharge port; the second end is arranged in the tower body;
the second material discharge pipe comprises at least one branch pipe, one end of any branch pipe is connected with the second end, the other end of the branch pipe extends towards the partition plate, and a gap A is formed between the other end of the branch pipe and the partition plate;
polishing resin enters the separation tower through the material inlet and falls on the partition plate, a layering agent enters the separation tower through the backwashing port and the water cap and contacts with the polishing resin, negative resin and positive resin in the polishing resin are layered, the positive resin is discharged through the second material discharge pipe and the first material discharge pipe, and the negative resin is regenerated in the separation tower.
Furthermore, the second material discharge pipe comprises four branch pipes, and the four branch pipes are distributed in a trumpet shape.
Further, the branch pipe is L type, includes:
the first pipe is parallel to the partition plate, and one end of the first pipe is connected with the first material discharge pipe;
the second pipe is perpendicular to the partition plate, one end of the second pipe is connected with the other end of the first pipe, and a gap A is formed between the other end of the second pipe and the partition plate;
the first material discharge pipe, the first pipe and the second pipe are communicated.
Further, a material inlet pipe is arranged on the material inlet, and at least part of the material inlet pipe is positioned in the tower body and bent towards the partition plate.
Furthermore, a hanging rod is arranged at the closed end of the tower body, a wire winding pipe is arranged on the hanging rod, and a plurality of gaps are formed in the wire winding pipe;
the one end of inlet tube is passed through the water inlet stretches out the tower body, the other end of inlet tube with the wire winding union coupling, the inlet tube with the wire winding pipe intercommunication.
Furthermore, an exhaust port is arranged at the closed end of the tower body.
Furthermore, be equipped with the tower body sight glass on the lateral wall of tower body, through inside the separation column can be observed to the tower body sight glass.
Furthermore, the frustum comprises a conical surface, a cone sight glass is arranged on the conical surface, and the inside of the separation tower can be observed through the cone sight glass.
Furthermore, an access hole is formed in the tower body.
The technical scheme provided by the embodiment of the utility model has the following beneficial effects:
the embodiment of the utility model provides a conical separation tower device which can be suitable for separating different types and proportions of resin, has wide adaptability, high resin separation efficiency and low cost, and can avoid cross contamination generated in the regeneration process after resin separation and improve the effluent quality after resin regeneration by using a conical separation method.
Drawings
FIG. 1 is a schematic view of a separation column in an embodiment of the present invention.
Fig. 2 is a schematic structural diagram of a separator in an embodiment of the present invention.
FIG. 3 is a top view of a frustum in an embodiment of the utility model.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention is described in further detail below with reference to the accompanying drawings and embodiments. It should be understood that the specific embodiments described herein are merely illustrative of the utility model and are not intended to limit the utility model.
The embodiment of the utility model provides a conical separation tower for separating or regenerating anion and cation resins in polishing resins, which comprises: the tower body 1, the frustum 2, the partition plate 3 and the cylinder 4; the frustum 2 comprises a large-diameter port 21 and a small-diameter port 22; one end of the tower body 1 is a closed end, and the other end of the tower body 1 is fixedly connected with a large-diameter port 21; one side of the partition plate 3 covers the small-diameter port 22, and the other side of the partition plate 3 is fixedly connected with one end of the cylinder 4; a plurality of water caps 31 are arranged on the partition plate 3; the other end of the cylinder body 4 is provided with a backwashing port 40; the tower body 1 is provided with a material inlet 11, a material outlet 12 and a water inlet 13; the water inlet pipe 130 is arranged on the water inlet 13, and water can be introduced into the tower body 1 through the water inlet pipe 130; the material outlet 12 is provided with a first material outlet pipe 121 and a second material outlet pipe 122; the first material outlet pipe 121 comprises a first end 123 and a second end 124, and the first end 123 extends out of the tower body 1 through the material outlet 12; the second end 124 is arranged in the tower body 1; the second material discharge pipe 122 includes at least one branch pipe, one end of any branch pipe is connected to the second end 124, and the other end of the branch pipe extends toward the partition plate 3 and has a gap a with the partition plate 3; the polishing resin enters the separation tower through the material inlet port 11 and falls on the partition plate 3, the delaminating agent enters the separation tower through the backwashing port 40 and the water cap 31 and contacts with the polishing resin, the negative resin among the polishing resin is delaminated from the positive resin, the positive resin is discharged through the second material discharge pipe 122 and the first material discharge pipe 121, and the negative resin is regenerated in the separation tower.
In a specific embodiment, as shown in fig. 1, the tower body 1, the frustum 2 and the cylinder 4 are all arranged in the up-down direction; the tower comprises a tower body 1, a tower body 2, a partition plate 3, a barrel 4 and a back washing opening 40, wherein a closed arc-shaped cover is arranged above the tower body 1, the lower part of the tower body 1 is fixedly connected with a large-diameter port 21 of the frustum 2, a small-diameter port 22 is covered by the partition plate 3, the lower part of the partition plate 3 is the barrel 4, and the lower end of the barrel 4 is provided with the back washing opening 40.
The partition 3 is provided with a plurality of water caps 31, the water caps 31 allow fluid to pass but not resin, so that the polishing resin entering the separation tower from the material inlet 11 is gathered above the partition 3, water entering the separation tower from the water inlet 13 can enter the cylinder through the partition 3, and when fluid such as alkali liquor, water, carbon dioxide and the like is injected into the cylinder 4 through the backwashing port 40, the fluid can pass through the partition 3 to enter above the partition 3 and contact with the polishing resin. As can be easily understood, the number and the position distribution of the water caps 31 can be adaptively adjusted according to the size of the partition plate 3; specifically, as shown in fig. 2, when the fluid is a liquid such as an alkali solution and/or pure water, in order to ensure that the liquid can uniformly flow through the polishing resin, the water caps 31 need to be uniformly distributed on the partition plate 3, and the water caps 31 may be circularly distributed on a plurality of concentric circles according to the shape of the partition plate 3. At the moment, when the liquid in the cylinder 4 contacts with the materials through the partition plate 3, the liquid can be uniformly distributed, and the phenomenon that the water flow is not uniform when the liquid flows through the polishing resin is avoided.
More preferably, the water inlet 13, the material inlet 11 and the material outlet 12 are all disposed on the side wall of the tower body 1, wherein the water inlet 13 and the material inlet 11 are all disposed above the side wall of the tower body 1, and the material outlet 12 is disposed below the side wall of the tower body 1. At this time, the polishing resin entering from the material inlet port 11 falls downward by gravity and is accumulated above the partition plate 3.
The second material discharge pipe 122 includes at least one branched pipe, and the number and shape of the branched pipes in the second material discharge pipe 122 are not limited in this application, and the specific number and shape may be adaptively adjusted according to the process of separating the polishing resin. Since one end of any of the branch pipes is connected to the second end 124 of the first material discharge pipe 121 and the other end of the branch pipe extends toward the partition plate 3 and has a gap a with the partition plate 3, the polishing resin gathered above the partition plate 3 can enter the second material discharge pipe 122 through the gap a and be discharged out of the tower body 1 through the first material discharge pipe 121. In one embodiment, the second material discharging pipe 122 includes a branch pipe, one end of the branch pipe is connected to the second end 124, and the second material discharging pipe 122 is communicated with the first material discharging pipe 121, so that the material in the second material discharging pipe 122 can enter the first material discharging pipe 121 and then be discharged out of the separation tower. In another embodiment, as shown in fig. 3, the second material discharging pipe 122 includes four branch pipes, and one end of each branch pipe is fixedly connected to the second end 124, so that the positive resin can simultaneously enter the first material discharging pipe 121 from the four branch pipes, which is highly efficient in discharging the positive resin. In other embodiments, the second material discharge pipe 122 may be two symmetrically arranged branch pipes, and the arrangement and the function of the second material discharge pipe 122 are similar to those of the four branch pipes in the above embodiments, so detailed descriptions thereof are omitted.
When the polishing resin is separated, a pneumatic diaphragm pump is adopted to pump the polishing resin added with a proper amount of water into the tower body 1 from the material inlet 11, the polishing resin falls on the partition plate 3 under the action of gravity, at the moment, a layering agent is injected into the tower through the backwashing port 40, the layering agent is contacted with the polishing resin on the partition plate 3 through the partition plate 3, the negative resin and the positive resin in the polishing resin are promoted to be layered, and then the positive resin gradually falls to the lower part of the negative resin. The delaminating agent may be suitably adjusted according to the kind of the polishing resin, and for example, the delaminating agent may be pure water or an alkali solution. After the layering of the male resin and the female resin is completed, the male resin below can enter the second material discharge pipe at the moment because one end of the second material discharge pipe is close to the partition plate and is at a distance A from the partition plate. At this time, pure water is continuously injected into the tower through the water inlet 13 and the backwashing port 40, so that the lower positive resin continuously enters the second material discharge pipe 122 through the gap a and further enters the first material discharge pipe 121, and the positive resin can be discharged out of the tower body 1 and transferred to a positive resin regeneration device for regeneration; after the positive resin is discharged, a small amount of mixed resin at the layered interface of the positive resin and the negative resin can be discharged out of the tower body and put in a mixed resin storage device to wait for the separation of the next batch; the negative resin is left in the tower 1 to be regenerated. And (2) carrying out acid regeneration treatment on the positive resin discharged out of the tower body 1 and carrying out alkali regeneration treatment on the negative resin remained in the tower body, so that the positive resin and the negative resin recover the ion exchange performance, namely, the positive resin and the negative resin are regenerated.
Further, the second material discharge pipe 122 includes four branch pipes, and the four branch pipes are distributed in a trumpet shape.
The four branch pipes are distributed in a trumpet shape, so that the efficiency of discharging the cation resin out of the separation tower can be improved; on the other hand, the four branch pipes can enable the interface of the male resin and the female resin to be uniformly reduced along with the discharge of the male resin, so that the phenomenon that the polishing resin layering interface is partially sunk due to the fact that the male resin is reduced too fast is avoided, the male resin and the female resin are disordered and cannot be completely separated, and the structural design can greatly reduce the mixed grease amount.
Further, the branch pipe is L type, includes: a first pipe 125 parallel to the partition plate 3, one end of the first pipe 125 being connected to the first material discharge pipe 121; a second tube 126 perpendicular to the separator 3, one end of the second tube 126 being connected to the other end of the first tube 125, and a gap a being provided between the other end of the second tube 126 and the separator 3; the first material discharge pipe 121, the first pipe 125, and the second pipe 126 are communicated.
In a specific embodiment, as shown in fig. 1 and 3, the second material discharging pipe is an L-shaped branched pipe, wherein the first pipe 125 is transversely disposed, one end of the first pipe 125 is connected to the first material discharging pipe 121, the second pipe 126 is vertically disposed, the upper end of the second pipe 126 is connected to the other end of the first pipe 125, the lower end of the second pipe 126 is close to the partition plate 3, and the distance between the lower end of the second pipe 126 and the partition plate 3 is a. Further, since the first material discharge pipe 121, the first pipe 125, and the second pipe 126 are communicated with each other, the male resin on the partition plate 3 can enter the second pipe 126 through the gap a, enter the first pipe 125, enter the first material discharge pipe 121, and be discharged out of the tower body 1.
Further, a material inlet pipe 110 is arranged on the material inlet 11, and at least a part of the material inlet pipe 110 is located in the tower body 1 and is bent towards the partition plate 3.
In a specific embodiment, as shown in fig. 1, a part of the material inlet pipe 110 extends out of the tower body 1, a part of the material inlet pipe 110 is disposed in the separation tower and bent downward, and when the polishing resin is driven into the separation tower from the material inlet pipe 110 by using an air operated diaphragm pump, the material falls downward on the partition plate 3.
Furthermore, a hanging rod 14 is arranged at the closed end of the tower body 1, a wire winding pipe 15 is arranged on the hanging rod 14, and a plurality of gaps are formed in the wire winding pipe 15; the one end of inlet tube 130 is passed through the water inlet stretches out tower body 1, the other end of inlet tube with wire winding pipe 15 is connected, inlet tube 130 with wire winding pipe 15 intercommunication.
In a specific embodiment, as shown in fig. 1, the top end of the tower body 1 is a closed end, the top end of the tower body 1 is provided with a suspension rod 14, by arranging the wire winding pipe 15 on the suspension rod 14, and because the wire winding pipe 15 has a plurality of gaps, when water is fed from the water inlet 13, the water can uniformly flow out of the plurality of gaps of the wire winding pipe 15, and when the layering agent is injected from the backwashing port 40, the resin cannot be discharged out of the tower body from the water inlet 13.
Further, an exhaust port 16 is arranged at the closed end of the tower body 1.
In a specific embodiment, as shown in fig. 1, the gas outlet 16 is disposed at the top end of the tower body 1, so that the gas in the tower body can escape from the top of the tower body 1, and the liquid or solid in the separation tower can be prevented from blocking the gas outlet 16. In the process of separating the polishing resin as described above, when the liquid is injected from the water inlet 13 and the backwash opening 40, the gas in the column is discharged from the gas discharge opening 16, thereby preventing the excessive pressure in the separation column.
Furthermore, a tower body view mirror 17 is arranged on the side wall of the tower body 1, and the inside of the separation tower can be observed through the tower body view mirror 17.
In a specific embodiment, as shown in fig. 1, a tower view mirror 17 is disposed on a side wall of the tower body 1, and the tower view mirror 17 may be disposed on an upper portion, a middle portion, or a lower portion of the tower body 1, such that when the polishing resin is delaminated in the above process of separating the polishing resin, whether the delamination of the positive resin and the negative resin in the tower body 1 is completed can be observed according to the tower view mirror 17.
Further, the frustum 2 comprises a conical surface 23, a cone sight glass 24 is arranged on the conical surface 23, and the inside of the separation tower can be observed through the cone sight glass 24.
In a specific embodiment, as shown in fig. 1, in the process of separating the polishing resin as described above, after the positive and negative resins in the polishing resin are layered, carbon dioxide gas is introduced from the backwashing port 40 while the positive resin is transferred, and since the absorption capacities of the positive and negative resins to carbon dioxide are different, the carbon dioxide reaches the interface between the positive and negative resins, the conductivity between the positive and negative resins is rapidly decreased, and whether the positive resin separation is completed is determined by detecting whether the conductivity of the positive and negative resins is suddenly decreased and observing the inside of the separation tower in combination with the cone lens 24.
Further, an access hole 18 is formed in the tower body 1.
In a specific embodiment, as shown in fig. 1, the access opening 18 is arranged on the side wall of the tower body 1, and the access opening 18 is normally covered with a cover, so that when the separation tower is out of order, a worker can access the separation tower through the access opening 18.
Finally, it should be noted that the above embodiments are only for illustrating the technical solutions of the present invention and not for limiting, and although the present invention has been described in detail with reference to examples, it should be understood by those skilled in the art that modifications or equivalent substitutions may be made on the technical solutions of the present invention without departing from the spirit and scope of the technical solutions of the present invention, which should be covered by the claims of the present invention.

Claims (9)

1. A conical separation column for separating or regenerating cation and anion resins from a polishing resin, comprising:
the tower body (1), the frustum (2), the partition plate (3) and the cylinder body (4);
the frustum (2) comprises a large-diameter port (21) and a small-diameter port (22);
one end of the tower body (1) is a closed end, and the other end of the tower body (1) is fixedly connected with the large-diameter port (21);
one side of the partition plate (3) covers the small-diameter port, and the other side of the partition plate (3) is fixedly connected with one end of the cylinder (4); a plurality of water caps (31) are arranged on the partition plate (3);
the other end of the cylinder body (4) is provided with a backwashing port (40);
the tower body is provided with a material inlet (11), a material outlet (12) and a water inlet (13);
a water inlet pipe (130) is arranged on the water inlet (13), and water can be introduced into the tower body (1) through the water inlet pipe (130);
the material discharge port (12) is provided with a first material discharge pipe (121) and a second material discharge pipe (122);
the first material discharge pipe (121) comprises a first end (123) and a second end (124), and the first end (123) extends out of the tower body (1) through the material discharge port (12); the second end (124) is arranged in the tower body (1);
the second material discharge pipe (122) comprises at least one branch pipe, one end of any branch pipe is connected with the second end (124), the other end of the branch pipe extends towards the partition plate (3), and a gap A is formed between the other end of the branch pipe and the partition plate (3).
2. The conical separation column of claim 1,
the second material discharge pipe (122) comprises four branch pipes, and the four branch pipes are distributed in a trumpet shape.
3. The conical separation column of claim 1,
the branch pipe is the L type, includes:
a first pipe (125) parallel to the partition (3), one end of the first pipe (125) being connected to the first material discharge pipe (121);
a second tube (126) perpendicular to the separator (3), one end of the second tube (126) being connected to the other end of the first tube (125), a gap a being present between the other end of the second tube (126) and the separator (3);
the first material discharge pipe (121), the first pipe (125) and the second pipe (126) are communicated.
4. The conical separation column of claim 1,
the material inlet (11) is provided with a material inlet pipe (110), and at least part of the material inlet pipe (110) is positioned in the tower body (1) and is bent towards the partition plate (3).
5. The conical separation column of claim 1,
a hanging rod (14) is arranged at the closed end of the tower body (1), a wire winding pipe (15) is arranged on the hanging rod (14), and a plurality of gaps are formed in the wire winding pipe (15);
the one end of inlet tube (130) is passed through water inlet (13) stretch out tower body (1), the other end of inlet tube (130) with wire winding pipe (15) are connected, inlet tube (130) with wire winding pipe (15) intercommunication.
6. The conical separation column of claim 1,
an air outlet (16) is arranged on the closed end of the tower body (1).
7. The conical separation column of claim 1,
be equipped with tower body sight glass (17) on the lateral wall of tower body (1), through inside tower body sight glass (17) can observe the knockout tower.
8. The conical separation column of claim 1,
the frustum (2) comprises a conical surface (23), a cone viewing mirror (24) is arranged on the conical surface (23), and the inside of the separation tower can be observed through the cone viewing mirror (24).
9. The conical separation column of claim 1,
an access hole (18) is arranged on the tower body (1).
CN202122824894.4U 2021-11-18 2021-11-18 Conical separation tower Active CN216538503U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202122824894.4U CN216538503U (en) 2021-11-18 2021-11-18 Conical separation tower

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202122824894.4U CN216538503U (en) 2021-11-18 2021-11-18 Conical separation tower

Publications (1)

Publication Number Publication Date
CN216538503U true CN216538503U (en) 2022-05-17

Family

ID=81573395

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202122824894.4U Active CN216538503U (en) 2021-11-18 2021-11-18 Conical separation tower

Country Status (1)

Country Link
CN (1) CN216538503U (en)

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