CN216538481U - Device convenient to triazole recovery in famoxadone synthetic waste water - Google Patents
Device convenient to triazole recovery in famoxadone synthetic waste water Download PDFInfo
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- CN216538481U CN216538481U CN202123351314.0U CN202123351314U CN216538481U CN 216538481 U CN216538481 U CN 216538481U CN 202123351314 U CN202123351314 U CN 202123351314U CN 216538481 U CN216538481 U CN 216538481U
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Abstract
The utility model belongs to the technical field of triazole recovery equipment, and particularly relates to a device convenient for recovering triazole from famoxadone synthesis wastewater.
Description
Technical Field
The utility model relates to the technical field of triazole recovery equipment, in particular to a device convenient for recovering triazole from famoxadone synthesis wastewater.
Background
1,2, 4-triazole is a chemical substance, the molecular formula is C2H3N3, the molecular weight is 69.07, CAS No. 288-88-0, colorless acicular crystal, dissolve in water and ethanol, the product is used in the production of pesticide, medicine (fluconazole), dyestuff, rubber auxiliary agent, also used in the photoconductor of the replication system, the midbody of antifungal agent fluconazole, in the present chemical industry field, can contain more triazole in the famoxadone synthesis waste water, need to reclaim triazole in the waste water, utilize in different trades on one side, and the waste water containing triazole directly discharges and can cause serious influence to the environment.
The prior art has the following problems:
1. the existing recovery device generally separates triazole in wastewater containing triazole through crystallization treatment, and the crystallized triazole can be dug out of a water outlet of the recovery device, so that the wastewater in the device cannot be effectively discharged;
2. the existing triazole crystals adhere to the inner surface of the device, and the triazole crystals in the device cannot be effectively collected after the wastewater is discharged or are difficult to collect, so that the improvement point exists.
SUMMERY OF THE UTILITY MODEL
Aiming at the defects of the prior art, the utility model provides a device convenient for recovering triazole in famoxadone synthesis wastewater, and solves the problems of recovery efficiency and blockage existing at present.
In order to achieve the purpose, the utility model provides the following technical scheme: a device convenient for recycling triazole in famoxadone synthesis wastewater comprises a reaction kettle, a driving motor is fixedly arranged at the top of the reaction kettle, a water inlet pipe is arranged at the top end of the reaction kettle in a penetrating way, a transmission shaft is arranged at the bottom of the driving motor, the inner surface of the reaction kettle is provided with a thread surface, the bottom end of the transmission shaft is provided with a fixed block, the surface of the transmission shaft is provided with a fixed ring, a scraper is arranged outside the fixing ring, a water outlet is arranged at the bottom of the inner surface of the reaction kettle, an inner sliding groove is arranged at the bottom of the water outlet, a sealing plate is arranged in the inner sliding groove, a tooth groove is arranged at the bottom of the sealing plate, a thread taper groove is arranged at the bottom of the inner sliding groove, the screw thread awl inslot is provided with the rubber awl, the rubber awl top is provided with the driving tooth, rubber awl bottom is provided with the bellows, the bottom of reation kettle one side is run through and is provided with the discharge gate.
As a preferred technical scheme of the utility model, the transmission shaft is in transmission connection with the driving motor through a coupling, the transmission shaft penetrates through the reaction kettle and is in rotary connection with the reaction kettle, and the fixing block is fixedly connected with the transmission shaft.
As a preferred technical scheme of the utility model, the number of the fixing blocks is four, the four fixing blocks are arranged in an annular array relative to the horizontal surface of the transmission shaft, the outer diameter size of the transmission shaft is matched with the inner diameter size of a fixing ring, the fixing ring is connected with the transmission shaft in a sliding manner, and the transmission shaft is clamped with the fixing ring through the fixing blocks.
As a preferable technical scheme of the utility model, the number of the scrapers is three, the three groups of the scrapers are arranged in an annular array relative to the horizontal surface of the fixing ring, and one end of each scraper, which is far away from the fixing ring, is in threaded connection with the threaded surface.
As a preferable technical scheme of the utility model, the size of the inner surface of the inner sliding groove is matched with the size of the outer surface of the sealing plate, the sealing plate is connected with the inner sliding groove in a sliding mode, the tooth grooves are meshed with the driving teeth, and the sealing plate is in driving connection with the driving teeth through the tooth grooves.
As a preferable technical scheme of the utility model, the transmission teeth are fixedly connected with the rubber cone, the outer shape of the rubber cone is in a circular dune shape, the size of the outer surface of the rubber cone is matched with the size of the inner surface of the thread cone groove, and the rubber cone is in threaded connection with the thread cone groove.
As a preferred technical scheme of the utility model, the corrugated pipe is fixedly connected with the rubber cone, and the discharge hole is fixedly connected with the reaction kettle through the sealing ring.
Compared with the prior art, the utility model provides a device convenient for recovering triazole in famoxadone synthesis wastewater, and the device has the following beneficial effects:
1. the device convenient for recycling triazole in famoxadone synthetic wastewater comprises an inner sliding groove formed at the bottom of a water outlet, and a slidable sealing plate arranged in the inner sliding groove, so that in the normal crystallization process of the wastewater in the device, the sealing plate is matched with the water outlet, the wastewater in a reaction kettle is sealed, when the sealing plate needs to be opened to remove the wastewater, the tightness is improved through the thread tightening effect between a rubber cone and a thread cone groove, the rotation of the rubber cone drives a top transmission gear to rotate along with the rubber cone, the transmission gear is meshed with a tooth groove, the rotation of the transmission gear drives the sealing plate to slide in the inner sliding groove, thus the opening effect of a port of the water outlet can be completed, the crystallization of the port of the water outlet can crack along with the sliding between the sealing plate and the inner sliding groove, the removal of the wastewater is finally realized, even if the port of the water outlet is crystallized, the removal of the crystals can be completed by rotating the rubber cone, and the problem that waste water cannot be discharged due to the blockage of a water outlet is prevented.
2. The device for conveniently recovering the triazole in the famoxadone synthesis wastewater comprises a driving motor arranged at the top of a reaction kettle, a transmission shaft driven to rotate in the reaction kettle under the control, four groups of fixed blocks on the surface of the transmission shaft and fixed rings clamped with each other, so that the transmission shaft can normally drive the fixed rings and three groups of scrapers fixed on the outer sides of the fixed rings to rotate, the scraping effect on the inner wall of the reaction kettle is realized, thus the inner wall crystallization can be broken, the thread surfaces arranged on the inner surface of the reaction kettle are meshed with the scrapers, the fixed rings drive the scrapers to rotate and simultaneously slide up and down on the surface of the transmission shaft, the crystallization breaking work on the whole inner surface of the reaction kettle can be realized, finally, the scrapers rotate on the bottom surface of the reaction kettle, a derivation effect is performed on the crystallization, and the crystallization is convenient to be sent out from a discharge port, and the collection of crystals is realized.
Drawings
FIG. 1 is a front sectional view of the overall structure of the present invention;
FIG. 2 is a schematic top view of the overall structure of the present invention;
FIG. 3 is a disassembled view showing the structure of the seal connecting member according to the present invention;
fig. 4 is a schematic view of a drain port according to the present invention.
In the figure: 1. a reaction kettle; 2. a drive motor; 3. a water inlet pipe; 4. a drive shaft; 5. a thread face; 6. a fixed block; 7. a fixing ring; 8. a squeegee; 9. a water outlet; 10. an inner chute; 11. a sealing plate; 12. a tooth socket; 13. a thread taper groove; 14. a rubber cone; 15. a transmission gear; 16. a bellows; 17. and (4) a discharge port.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring to fig. 1-4, in this embodiment: a device convenient for recycling triazole in famoxadone synthesis wastewater comprises a reaction kettle 1, namely a recycling device whole; a driving motor 2 with the model number of HM3500 is fixedly arranged at the top of the reaction kettle 1 and is used for driving; a water inlet pipe 3 is arranged at the top end of the reaction kettle 1 in a penetrating way and is used for conveying wastewater into the reaction kettle 1; the bottom of the driving motor 2 is provided with a transmission shaft 4 for transmission; the inner surface of the reaction kettle 1 is provided with a thread surface 5 for realizing the stable descending effect of a subsequent device; the bottom end of the transmission shaft 4 is provided with a fixed block 6 for fixing a subsequent device and driving the subsequent device to rotate; the surface of the transmission shaft 4 is provided with a fixed ring 7 which is used for connecting a subsequent device and is matched with the transmission shaft 4 to generate a moving effect; a scraper 8 is arranged outside the fixed ring 7 and used for scraping the inner wall of the reaction kettle 1; a water outlet 9 is formed at the bottom of the inner surface of the reaction kettle 1 and used for discharging waste water; the bottom of the water outlet 9 is provided with an inner chute 10 for providing a sliding space; a sealing plate 11 is arranged inside the inner chute 10 and used for closing or opening the port of the water outlet 9; the bottom of the sealing plate 11 is provided with a tooth groove 12 for transmission; the bottom of the inner chute 10 is provided with a threaded conical groove 13 for threaded sealing; a rubber cone 14 is arranged in the thread cone groove 13 and is used for sealing in cooperation with the thread cone groove 13; the top of the rubber cone 14 is provided with a transmission gear 15 which is used for matching with the tooth groove 12 to drive the sealing plate 11 to slide; the bottom of the rubber cone 14 is provided with a corrugated pipe 16 for guiding flow; the bottom of one side of the reaction kettle 1 is provided with a discharge hole 17 for discharging.
In the embodiment, the transmission shaft 4 is in transmission connection with the driving motor 2 through a coupling, the transmission shaft 4 penetrates through the reaction kettle 1 and is in rotational connection with the reaction kettle, the fixing block 6 is fixedly connected with the transmission shaft 4, the transmission shaft 4 rotates under the transmission effect of the driving motor 2, and the fixing block 6 is clamped with a subsequent device to drive the subsequent device to rotate; the number of the fixing blocks 6 is four, the four fixing blocks 6 are arranged in an annular array relative to the horizontal surface of the transmission shaft 4, the outer diameter of the transmission shaft 4 is matched with the inner diameter of the fixing ring 7, the fixing ring 7 is connected with the transmission shaft 4 in a sliding mode, the transmission shaft 4 is connected with the fixing ring 7 in a clamping mode through the fixing blocks 6, and the four fixing blocks 6 improve the rotating effect; the fixing ring 7 is clamped with the fixing block 6 to rotate along with the transmission shaft 4; the number of the scrapers 8 is three, the three groups of scrapers 8 are arranged in an annular array relative to the horizontal plane of the fixing ring 7, one end, far away from the fixing ring 7, of each scraper 8 is in threaded connection with the threaded surface 5, the three groups of scrapers 8 scrape the inner surface of the reaction kettle 1, the scrapers 8 can move up and down while rotating due to threaded connection with the threaded surfaces 5, and the function is realized by the sliding effect between the fixing ring 7 and the transmission shaft 4; the size of the inner surface of the inner sliding groove 10 is matched with the size of the outer surface of the sealing plate 11, the sealing plate 11 is in sliding connection with the inner sliding groove 10, the tooth grooves 12 are meshed with the transmission teeth 15, the sealing plate 11 is in transmission connection with the transmission teeth 15 through the tooth grooves 12, and the sealing plate 11 can move in the inner sliding groove 10 under the meshing action between the tooth grooves 12 and the transmission teeth 15, so that the opening and closing of the port of the water outlet 9 are realized; the transmission teeth 15 are fixedly connected with the rubber cone 14, the rubber cone 14 is in a circular dune shape, the size of the outer surface of the rubber cone 14 is matched with the size of the inner surface of the thread cone groove 13, the rubber cone 14 is in threaded connection with the thread cone groove 13, and the circular dune-shaped rubber cone 14 is in threaded connection with the thread cone groove 13, so that the sealing performance is improved, and wastewater leakage is prevented; the corrugated pipe 16 is fixedly connected with the rubber cone 14, the discharge port 17 is fixedly connected with the reaction kettle 1 through a sealing ring, and the discharge port 17 discharges crystals.
The working principle and the using process of the utility model are as follows: an operator injects waste water into the reaction kettle 1 through the water inlet pipe 3 and performs chemical crystallization reaction, after the reaction is completed, the rubber cone 14 and the thread taper groove 13 are screwed tightly, at the moment, the rotation of the rubber cone 14 drives the transmission gear 15 to rotate, the transmission gear 15 is meshed with the tooth groove 12 to drive the sealing plate 11 to slide in the inner chute 10, and the crystal at the port of the water outlet 9 is broken, when the sealing plate 11 slides to a certain area, the port of the water outlet 9 discharges the waste water, the waste water is collected by the corrugated pipe 16 for further treatment, when the waste water in the reaction kettle 1 is discharged completely, the driving motor 2 at the top of the reaction kettle 1 is opened, so that the driving motor 2 drives the transmission shaft 4 to rotate in the reaction kettle 1, the transmission shaft 4 is clamped with the fixing rings 7 through the four groups of fixing blocks 6 on the surface, and the fixing rings drive the fixing rings 7 to rotate, solid fixed ring 7 then drives three group's scrapers 8 and carry out a effect of striking off to 1 internal surface of reation kettle, the crystallization to adhering to the internal surface can be abolished like this, afterwards, because of the screw thread relation between scraper blade 8 and the helicoid 5, scraper blade 8 drives solid fixed ring 7 and slides about 4 surfaces of transmission shaft are gone on in solid fixed ring 7 pivoted simultaneously, can carry out a effect of striking off to the inner wall whole like this, scraper blade 8 rotates 4 bottoms of transmission shaft at last, and open discharge gate 17 this moment, carry out a collection effect to the crystal under scraper blade 8's boosting effect, it is relatively convenient, the problem of crystal adhesion and 9 port blockages in outlet is solved.
Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that changes may be made in the embodiments and/or equivalents thereof without departing from the spirit and scope of the utility model. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (7)
1. The utility model provides a device convenient to triazole is retrieved in famoxadone synthetic waste water, includes reation kettle (1), its characterized in that: the top of the reaction kettle (1) is fixedly provided with a driving motor (2), the top end of the reaction kettle (1) is provided with a water inlet pipe (3) in a penetrating manner, the bottom of the driving motor (2) is provided with a transmission shaft (4), the inner surface of the reaction kettle (1) is provided with a thread face (5), the bottom end of the transmission shaft (4) is provided with a fixed block (6), the surface of the transmission shaft (4) is provided with a fixed ring (7), the outer side of the fixed ring (7) is provided with a scraper (8), the bottom of the inner surface of the reaction kettle (1) is provided with a water outlet (9), the bottom of the water outlet (9) is provided with an inner sliding groove (10), a sealing plate (11) is arranged in the inner sliding groove (10), the bottom of the sealing plate (11) is provided with a tooth groove (12), the bottom of the inner sliding groove (10) is provided with a thread taper groove (13), and a rubber taper (14) is arranged in the thread taper groove (13), the top of the rubber cone (14) is provided with a transmission gear (15), the bottom of the rubber cone (14) is provided with a corrugated pipe (16), and the bottom end of one side of the reaction kettle (1) is provided with a discharge hole (17) in a penetrating manner.
2. The device for facilitating recovery of triazole in famoxadone synthesis wastewater according to claim 1, characterized in that: the transmission shaft (4) is in transmission connection with the driving motor (2) through a coupling, the transmission shaft (4) penetrates through the reaction kettle (1) and is rotatably connected with the reaction kettle, and the fixing block (6) is fixedly connected with the transmission shaft (4).
3. The device for facilitating recovery of triazole in famoxadone synthesis wastewater according to claim 1, characterized in that: the quantity of fixed block (6) is four groups, four groups annular array arrangement is personally submitted about the level of transmission shaft (4) in fixed block (6), the external diameter size of transmission shaft (4) and the internal diameter size phase-match of solid fixed ring (7), gu fixed ring (7) and transmission shaft (4) sliding connection, transmission shaft (4) are through fixed block (6) and solid fixed ring (7) joint.
4. The device for facilitating recovery of triazole in famoxadone synthesis wastewater according to claim 1, characterized in that: the quantity of scraper blade (8) is three groups, three groups scraper blade (8) are personally submitted annular array and are arranged about the level of solid fixed ring (7), scraper blade (8) keep away from the one end and the screw thread face (5) threaded connection of solid fixed ring (7).
5. The device for facilitating recovery of triazole in famoxadone synthesis wastewater according to claim 1, which is characterized in that: the inner surface size of the inner sliding groove (10) is matched with the outer surface size of the sealing plate (11), the sealing plate (11) is connected with the inner sliding groove (10) in a sliding mode, the tooth grooves (12) are meshed with the transmission teeth (15), and the sealing plate (11) is in transmission connection with the transmission teeth (15) through the tooth grooves (12).
6. The device for facilitating recovery of triazole in famoxadone synthesis wastewater according to claim 1, characterized in that: the transmission gear (15) is fixedly connected with the rubber cone (14), the rubber cone (14) is in a circular dune shape, the size of the outer surface of the rubber cone (14) is matched with the size of the inner surface of the thread cone groove (13), and the rubber cone (14) is in threaded connection with the thread cone groove (13).
7. The device for facilitating recovery of triazole in famoxadone synthesis wastewater according to claim 1, characterized in that: the corrugated pipe (16) is fixedly connected with the rubber cone (14), and the discharge hole (17) is fixedly connected with the reaction kettle (1) through a sealing ring.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202123351314.0U CN216538481U (en) | 2021-12-29 | 2021-12-29 | Device convenient to triazole recovery in famoxadone synthetic waste water |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202123351314.0U CN216538481U (en) | 2021-12-29 | 2021-12-29 | Device convenient to triazole recovery in famoxadone synthetic waste water |
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| CN216538481U true CN216538481U (en) | 2022-05-17 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN202123351314.0U Active CN216538481U (en) | 2021-12-29 | 2021-12-29 | Device convenient to triazole recovery in famoxadone synthetic waste water |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116120247A (en) * | 2022-12-27 | 2023-05-16 | 如东众意化工有限公司 | Method for recycling triazole in famoxadone synthesis wastewater |
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2021
- 2021-12-29 CN CN202123351314.0U patent/CN216538481U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116120247A (en) * | 2022-12-27 | 2023-05-16 | 如东众意化工有限公司 | Method for recycling triazole in famoxadone synthesis wastewater |
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