CN216536966U

CN216536966U - Fractionating device is used in production and preparation of high-purity diphenyl alkali

Info

Publication number: CN216536966U
Application number: CN202122940785.9U
Authority: CN
Inventors: 周培良
Original assignee: Ningxia Huahao Biotechnology Co ltd
Current assignee: Ningxia Huahao Biotechnology Co ltd
Priority date: 2021-11-26
Filing date: 2021-11-26
Publication date: 2022-05-17
Anticipated expiration: 2031-11-26

Abstract

The utility model belongs to the field of diphenylalkali production, and particularly relates to a fractionating device for producing and preparing high-purity diphenylalkali, which comprises a heating cylinder, wherein a heating column penetrates through the front end of the heating cylinder, a conducting rod is arranged below the heating cylinder, a heating pin is attached to the front end of the bottom of the conducting rod, a conducting pipe is arranged below the heating pin, a distribution box is arranged below the conducting pipe, and a base is arranged at the bottom of the distribution box; through the cartridge heater, the post that heats, the conduction pole, the heating pin, the conduction pipe, the block terminal, the relation between the base, when using, can carry out the conduction through block terminal control conduction pipe, thereby control the heating pin and transmit the heating, then transmit through the conduction pole, and heat the processing through the diphenyl alkali liquid of cartridge heater to inside, and can control the device and carry out rapid heating evaporation, and is very convenient, and the heating post of heating post front end can carry out the concentrated heating, the later stage of being convenient for carries out rapid distillation.

Description

Fractionating device is used in production and preparation of high-purity diphenyl alkali

Technical Field

The utility model relates to the field of diphenyl alkali production, in particular to a fractionating device for producing and preparing high-purity diphenyl alkali.

Background

In the theory of acid-base ionization, base refers to a compound in which all anions ionized in an aqueous solution are OH < - >; base in acid-base proton theory refers to a compound capable of accepting a proton; in acid-base electron theory, base refers to an electron donor.

When the conventional fractionation device is used, the fractionation steam in the device cannot be well controlled to be rapidly cooled and collected, the fractionation device is not convenient and fast, and the integral energy supply device is inconvenient to rapidly disassemble and replace at the later stage;

therefore, a fractionating device for producing and preparing high-purity diphenyl alkali is provided aiming at the problems.

SUMMERY OF THE UTILITY MODEL

In order to make up the defects of the prior art and solve the problems that the fractionation steam in the device cannot be well controlled to be quickly cooled and collected, the device is not convenient and fast, and the integral energy supply device is inconvenient to quickly disassemble and replace in the later period when the device is used, the utility model provides the fractionation device for producing and preparing high-purity diphenyl alkali.

The technical scheme adopted by the utility model for solving the technical problems is as follows: the fractionating device for producing and preparing high-purity diphenyl alkali comprises a heating cylinder, wherein a heating column penetrates through the front end of the heating cylinder, a conducting rod is arranged below the heating cylinder, a heating pin is attached to the front end of the bottom of the conducting rod, a conducting pipe is arranged below the heating pin, a distribution box is arranged below the conducting pipe, and a base is arranged at the bottom of the distribution box.

Preferably, one side of cartridge heater is provided with the casing, the laminating of one side outer wall of casing has the filter screen, one side of filter screen is provided with the condenser pipe, one side screwed connection of condenser pipe has the valve, the bottom of condenser pipe is run through there is the constant temperature pipe, the bottom of constant temperature pipe is provided with the condensing engine.

Preferably, the top of casing is provided with the telescopic link, the top of telescopic link is provided with the rubber pad, the top block of rubber pad is connected with the apron.

Preferably, the front end of conduction pole is provided with the sleeve, telescopic bottom fixedly connected with bottom plate, one side fixedly connected with mount of bottom plate, fixing bolt has been run through to the front end of mount.

Preferably, the cover plate forms a telescopic structure through the telescopic rod and the shell, and the central axis of the cover plate coincides with the central axis of the shell.

Preferably, the condenser pipe passes through the casing and constitutes the structure that runs through, and is connected for the block between condenser pipe and the filter screen.

Preferably, the shell forms a detachable structure with the fixed frame through a fixing bolt, and the central axis of the shell coincides with the central axis of the fixed frame.

Preferably, the conduction pipe forms detachable construction through between heating pin and the conduction pole, and coincides between the axis of conduction pole and the axis of heating cylinder mutually.

The utility model has the advantages that:

1. according to the utility model, through the relation among the heating cylinder, the heating column, the conduction rod, the heating pin, the conduction pipe, the distribution box and the base, when the device is used, the conduction pipe can be controlled by the distribution box to conduct, so that the heating pin is controlled to conduct transmission heating, then the conduction rod is used for transmitting, and the heating cylinder is used for heating and processing the diphenyl alkali liquid in the device, so that the device is very convenient and fast, the heating column at the front end of the heating column can be used for carrying out centralized heating, the later-stage rapid distillation is facilitated, the convenience is high, the base supports the distribution box body above the heating column, and the integral device is effectively prevented from being deviated left and right;

2. according to the utility model, through the relationship among the filter screen, the condenser pipe, the filter screen, the constant temperature pipe, the condenser and the valve, when the device is used, the device can be controlled to quickly condense and collect water vapor evaporated below the device, the device is very convenient and fast, impurities can be blocked through the filter screen, simultaneously, reverse osmosis of dirt in the external environment can be prevented, and the fractionation purity is ensured.

Drawings

In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings used in the description of the embodiments or the prior art will be briefly described below, and it is obvious that the drawings in the following description are only some embodiments of the present invention, and for those skilled in the art, other drawings can be obtained according to these drawings without inventive exercise.

FIG. 1 is a schematic front view of the present invention;

FIG. 2 is a schematic cross-sectional view of the present invention;

FIG. 3 is a schematic view of a heating cartridge according to the present invention;

FIG. 4 is an enlarged view of the structure of FIG. 2A according to the present invention;

fig. 5 is a schematic view of a structure of a condenser tube according to the present invention.

In the figure: 1. a rubber pad; 2. a cover plate; 3. a telescopic rod; 4. a housing; 5. fixing the bolt; 6. a fixed mount; 7. a sleeve; 8. a base plate; 9. a distribution box; 10. a base; 11. a valve; 12. a condenser tube; 13. a condenser; 14. filtering with a screen; 15. a heating cylinder; 16. heating the column; 17. a heating pin; 18. a conducting tube; 19. a thermostatic tube; 20. a conductive rod.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

Referring to fig. 1-5, a fractionating apparatus for producing and preparing high-purity diphenyl alkali comprises a heating cylinder 15, a heating column 16 is penetrated through the front end of the heating cylinder 15, a conducting rod 20 is disposed below the heating cylinder 15, a heating pin 17 is attached to the front end of the bottom of the conducting rod 20, a conducting tube 18 is disposed below the heating pin 17, a distribution box 9 is disposed below the conducting tube 18, and a base 10 is disposed at the bottom of the distribution box 9.

This embodiment, one side of cartridge heater 15 is provided with casing 4, the laminating of one side outer wall of casing 4 has filter screen 14, one side of filter screen 14 is provided with condenser pipe 12, one side screwed connection of condenser pipe 12 has valve 11, the bottom of condenser pipe 12 runs through there is constant temperature pipe 19, the bottom of constant temperature pipe 19 is provided with condenser 13, through the relation between constant temperature pipe 19 and condenser 13, when using, constant temperature pipe 19 can protect the cryogenic fluid of condenser 13 transmission of below, prevent to cause the frostbite to the user simultaneously.

This embodiment, the top of casing 4 is provided with telescopic link 3, and the top of telescopic link 3 is provided with rubber pad 1, and the top block of rubber pad 1 is connected with apron 2, and through the relation between casing 4 and telescopic link 3 and the rubber pad 1, when using, apron 2 wholly can carry out telescopic control to control rubber pad 1 seals up, and is very convenient to the 4 feed inlets of casing of below.

This embodiment, the front end of conduction pole 20 is provided with sleeve 7, the bottom fixedly connected with bottom plate 8 of sleeve 7, one side fixedly connected with mount 6 of bottom plate 8, fixing bolt 5 has been run through to the front end of mount 6, through the relation between conduction pole 20 and sleeve 7 and the bottom plate 8, when using, can control sleeve 7 and effectively protect inside conduction pole 20 is whole, prolongs the holistic life of conduction pole 20 simultaneously.

This embodiment, apron 2 passes through to constitute extending structure between telescopic link 3 and the casing 4, and coincides mutually between the axis of apron 2 and the axis of casing 4, through the relation between apron 2 and telescopic link 3 and the casing 4, when using, can control apron 2 through telescopic link 3 and carry out quick seal, and is very convenient, and telescopic link 3 plays to support spacing effect to apron 2, can prevent to lap the condition that 2 appearances dropped.

This embodiment, condenser pipe 12 constitutes through the structure through casing 4, and is connected for the block between condenser pipe 12 and the filter screen 14, through the relation between condenser pipe 12 and casing 4 and the filter screen 14, when using, can control the whole later stage of being convenient for of filter screen 14 and dismantle the change, and is very convenient, and condenser pipe 12 can control inside gas and liquefy, and is very convenient.

This embodiment, casing 4 passes through to constitute detachable construction between 5 and the mount 6 of fixing bolt, and coincides mutually between the axis of casing 4 and the axis of mount 6, through the relation between

casing

4 and 5 and the mount 6 of fixing bolt, when using, can control casing 4 and remain stable, and the later stage of being convenient for simultaneously is dismantled casing 4 and is changed.

In this embodiment, the conduction pipe 18 forms detachable construction through between heating pin 17 and the conduction pole 20, and coincides mutually between the axis of conduction pole 20 and the axis of heating cylinder 15, through the relation between conduction pipe 18 and heating pin 17 and the conduction pole 20, when using, can control the whole change of dismantling of conduction pipe 18, and is very convenient.

Theory of operation, with the device before the use, the diphenyl alkali stoste that will carry out the fractionation at first drops into through 4 tops of casing, then presses apron 2 control rubber pad 1 and casing 4 to seal, then conducts to transfer pipe 18 through block terminal 9 of bottom, then control heating cylinder 15 carries out the heating function, then control inside diphenyl alkali stoste and heat, the inside steam of final control evaporates, cool off through condenser pipe 12 at last, discharge through 11 control of valve at last, this is exactly the theory of operation of the device.

In the description herein, references to the description of "one embodiment," "an example," "a specific example" or the like are intended to mean that a particular feature, structure, material, or characteristic described in connection with the embodiment or example is included in at least one embodiment or example of the utility model. In this specification, the schematic representations of the terms used above do not necessarily refer to the same embodiment or example. Furthermore, the particular features, structures, materials, or characteristics described may be combined in any suitable manner in any one or more embodiments or examples.

The foregoing shows and describes the general principles, essential features, and advantages of the utility model. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, which are described in the specification and illustrated only to illustrate the principle of the present invention, but that various changes and modifications may be made therein without departing from the spirit and scope of the present invention, which fall within the scope of the utility model as claimed.

Claims

1. The utility model provides a fractionating device is used in production and preparation of high-purity diphenyl alkali which characterized in that: including a heating cylinder (15), the front end of a heating cylinder (15) runs through and has heating post (16), the below of a heating cylinder (15) is provided with conduction pole (20), the laminating of the bottom front end of conduction pole (20) has heating pin (17), the below of heating pin (17) is provided with conduction pipe (18), the below of conduction pipe (18) is provided with block terminal (9), the bottom of block terminal (9) is provided with base (10).

2. The fractionating apparatus for producing and preparing high-purity diphenyl alkali according to claim 1, wherein: one side of cartridge heater (15) is provided with casing (4), one side outer wall laminating of casing (4) has filter screen (14), one side of filter screen (14) is provided with condenser pipe (12), one side screwed connection of condenser pipe (12) has valve (11), the bottom of condenser pipe (12) is run through and is had constant temperature pipe (19), the bottom of constant temperature pipe (19) is provided with condensing engine (13).

3. The fractionating apparatus for producing and preparing high-purity diphenyl alkali according to claim 2, wherein: the top of casing (4) is provided with telescopic link (3), the top of telescopic link (3) is provided with rubber pad (1), the top block of rubber pad (1) is connected with apron (2).

4. The fractionating apparatus for producing and preparing high-purity diphenyl alkali according to claim 1, wherein: the front end of conduction pole (20) is provided with sleeve (7), the bottom fixedly connected with bottom plate (8) of sleeve (7), one side fixedly connected with mount (6) of bottom plate (8), fixing bolt (5) have been run through to the front end of mount (6).

5. The fractionating apparatus for producing and preparing high-purity diphenyl alkali according to claim 3, wherein: the cover plate (2) forms a telescopic structure with the shell (4) through the telescopic rod (3), and the central axis of the cover plate (2) coincides with the central axis of the shell (4).

6. The fractionating apparatus for producing and preparing high-purity diphenyl alkali according to claim 2, wherein: the condensation pipe (12) forms a penetrating structure through the shell (4), and the condensation pipe (12) is connected with the filter screen (14) in a clamping manner.

7. The fractionating apparatus for producing and preparing high-purity diphenyl alkali according to claim 2, wherein: the shell (4) forms a detachable structure with the fixing frame (6) through the fixing bolt (5), and the central axis of the shell (4) coincides with the central axis of the fixing frame (6).

8. The fractionating apparatus for producing and preparing high-purity diphenyl alkali according to claim 1, wherein: the conduction pipe (18) forms a detachable structure through the heating pin (17) and the conduction rod (20), and the central axis of the conduction rod (20) coincides with the central axis of the heating cylinder (15).