CN216499341U - High-efficient sealed reation kettle - Google Patents

High-efficient sealed reation kettle Download PDF

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Publication number
CN216499341U
CN216499341U CN202123153252.2U CN202123153252U CN216499341U CN 216499341 U CN216499341 U CN 216499341U CN 202123153252 U CN202123153252 U CN 202123153252U CN 216499341 U CN216499341 U CN 216499341U
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reaction kettle
stirring
top surface
reation kettle
wall
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CN202123153252.2U
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何立新
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Wuxi Xinyoutong Equipment Technology Co ltd
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Wuxi Xinyoutong Equipment Technology Co ltd
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Abstract

The application discloses high-efficient sealed reation kettle, including workstation, fixing base, stabilizer bar, hot plate, the reation kettle jar body, filler, agitator motor, sealed bearing, puddler, actuating lever, stabilizing bearing, stirring leaf, row material pipe, solenoid valve, electric cabinet, manometer, receiver, bottom plate and backup pad. This application is through the top with agitator motor's output shaft tip fixed connection actuating lever, wall at the actuating lever sets up the puddler, make the puddler rotatory material to the inside of the reation kettle jar body mix the stirring when starting agitator motor, bottom through the top fixed connection actuating lever with the stirring leaf, thereby stir the interior bottom material of the reation kettle jar body through the stirring leaf when the actuating lever is rotatory, through the inside with the wall rotation connection sealed bearing of actuating lever, then inside the top surface with sealed bearing's wall embedding reation kettle jar body, thereby play sealed effect.

Description

High-efficient sealed reation kettle
Technical Field
The application relates to the technical field of sealed reaction kettles, in particular to a high-efficiency sealed reaction kettle.
Background
The reaction kettle is a small reactor commonly used in a chemical laboratory and can be used for the synthesis reaction of small dosage; the purpose of rapidly digesting the indissolvable substances can be achieved by utilizing the environment of strong acid or strong base in the tank body and high-temperature high-pressure sealing.
The barrel and the sealing cover of the existing hydrothermal synthesis reaction kettle are tightly connected together by a bolt or a tooth lock to form a three-in-one body, namely the barrel, the rubber ring and the sealing cover, and the sealing method can cause the problem of air leakage due to the aging and hardening deformation of the rubber ring due to the deformation of the barrel and the sealing cover, so that the reaction kettle cannot be normally used, the stirring of materials in the reaction kettle is not uniform, and the standard of material mixing and stirring cannot be met. Therefore, a high-efficiency sealed reaction kettle is provided for solving the problems.
Disclosure of Invention
The utility model provides a high-efficient sealed reation kettle is used for solving sealed reation kettle's among the prior art mixing problem in this embodiment.
According to one aspect of the application, a high-efficiency sealed reaction kettle is provided, and comprises a workbench, a filling opening, a discharge pipe, an electric cabinet and a stirring mechanism;
rabbling mechanism includes stabilizer bar, the reactor tank body, agitator motor, sealed bearing, puddler, actuating lever, stabilizing bearing and stirring leaf, the inner wall surface of the tip fixed connection reactor tank body of stabilizer bar, the other end fixed connection stabilizing bearing's of stabilizer bar wall, stabilizing bearing's inside rotates the wall of connecting the actuating lever, the bottom fixed connection stirring leaf's of actuating lever top, the inside of connecting sealed bearing is rotated to the wall of actuating lever, sealed bearing's wall embedding reactor tank body's top surface is inside, the top fixed connection agitator motor's of actuating lever output shaft tip, agitator motor's the top surface of the base fixed connection reactor tank body, the wall of the tip fixed connection actuating lever of puddler.
Furthermore, the bottom surface of the electric cabinet is fixedly connected with the top surface of the workbench.
Further, the bottom surface avris fixed connection backup pad's of workstation top surface, the bottom surface fixed connection bottom plate's of backup pad top surface avris, the top surface of bottom plate sets up the receiver.
Further, the top surface of workstation fixed connection fixing base's bottom surface, the inside of fixing base sets up the hot plate, the inner wall of hot plate closely laminates the wall of the reactor tank body, the top surface that should the reactor tank body sets up the manometer.
Further, the bottom end of the filling port is connected with the top surface of the tank body of the reaction kettle in a penetrating manner.
Furthermore, the top end of the discharge pipe penetrates through the bottom surface of the reaction kettle tank body, and the wall surface of the discharge pipe is provided with an electromagnetic valve.
Through the above-mentioned embodiment of this application, adopted rabbling mechanism, solved high-efficient sealed reation kettle's stirring problem, gained high-efficient sealed reation kettle's stirring effect.
Drawings
In order to more clearly illustrate the embodiments of the present application or the technical solutions in the prior art, the drawings needed to be used in the description of the embodiments or the prior art will be briefly introduced below, and it is obvious that the drawings in the following description are only some embodiments of the present application, and it is obvious for those skilled in the art that other drawings can be obtained according to the drawings without inventive exercise.
FIG. 1 is a schematic perspective view of one embodiment of the present application;
FIG. 2 is a schematic cross-sectional view of one embodiment of the present application;
fig. 3 is a schematic front view of an embodiment of the present application.
In the figure: 1. a work table; 2. a fixed seat; 3. a stabilizer bar; 4. heating plates; 5. a reaction kettle tank body; 6. a filling port; 7. a stirring motor; 8. sealing the bearing; 9. a stirring rod; 10. a drive rod; 11. stabilizing the bearing; 12. stirring blades; 13. a discharge pipe; 14. an electromagnetic valve; 15. an electric cabinet; 16. a pressure gauge; 17. a storage box; 18. a base plate; 19. and a support plate.
Detailed Description
In order to make the technical solutions better understood by those skilled in the art, the technical solutions in the embodiments of the present application will be clearly and completely described below with reference to the drawings in the embodiments of the present application, and it is obvious that the described embodiments are only partial embodiments of the present application, but not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the scope of the adjustment of the present application.
It should be noted that the terms "first," "second," and the like in the description and claims of this application and in the drawings described above are used for distinguishing between similar elements and not necessarily for describing a particular sequential or chronological order. It should be understood that the data so used may be interchanged under appropriate circumstances such that embodiments of the application described herein may be used. Furthermore, the terms "comprises," "comprising," and "having," and any variations thereof, are intended to cover a non-exclusive inclusion, such that a process, method, system, article, or apparatus that comprises a list of steps or elements is not necessarily limited to those steps or elements expressly listed, but may include other steps or elements not expressly listed or inherent to such process, method, article, or apparatus.
In this application, the terms "upper", "lower", "left", "right", "front", "rear", "top", "bottom", "inner", "outer", "middle", "vertical", "horizontal", "lateral", "longitudinal", and the like indicate orientations or positional relationships based on the orientations or positional relationships shown in the drawings. These terms are used primarily to better describe the present application and its embodiments, and are not used to limit the indicated devices, elements or components to a particular orientation or to be constructed and operated in a particular orientation.
Moreover, some of the above terms may be used to indicate other meanings besides the orientation or positional relationship, for example, the term "on" may also be used to indicate some kind of attachment or connection relationship in some cases. The specific meaning of these terms in this application will be understood by those of ordinary skill in the art as appropriate.
Furthermore, the terms "mounted," "disposed," "provided," "connected," and "sleeved" are to be construed broadly. For example, it may be a fixed connection, a removable connection, or a unitary construction; can be a mechanical connection, or an electrical connection; may be directly connected, or indirectly connected through intervening media, or may be in internal communication between two devices, elements or components. The specific meaning of the above terms in the present application can be understood by those of ordinary skill in the art as appropriate.
It should be noted that the embodiments and features of the embodiments in the present application may be combined with each other without conflict. The present application will be described in detail below with reference to the embodiments with reference to the attached drawings.
The reation kettle heating device of high-efficient sealed reation kettle in this embodiment can be used for reation kettle's heating, for example, the high-efficient sealed reation kettle who like taking rabbling mechanism of reation kettle heating device is provided in this embodiment, and what the high-efficient sealed reation kettle's of taking the stirring structure reation kettle heating device in this embodiment can be used for heating reation kettle.
The utility model provides a reaction kettle heating device, includes the cauldron body, the outside of the cauldron body is equipped with outer heating device, and the inside of the cauldron body is equipped with interior heating device, is equipped with two-way agitating unit on the interior heating device.
The external heating device comprises a jacket, an oil inlet pipe and an oil outlet pipe, the jacket is fixedly arranged outside the kettle body, a heating cavity is formed between the jacket and the kettle body, and the oil inlet pipe and the oil outlet pipe are fixedly arranged on the jacket and communicated with the heating cavity; the oil inlet pipe is fixedly arranged at the lower part of the jacket and is communicated with an oil outlet of the hot oil pump through a pipeline, and the oil outlet pipe is fixedly arranged at the upper part of the jacket and is communicated with an oil inlet of the hot oil pump through a pipeline; high-temperature hot oil enters the heating cavity from an oil inlet pipe at the lower part of the jacket through an oil outlet of the hot oil pump and a pipeline to heat the kettle body; the cold oil with reduced temperature flows back to the hot oil pump from the oil outlet pipe and the pipeline on the upper part of the jacket for circular heating after flowing through the whole kettle body, thereby ensuring the temperature of the hot oil in the jacket, fully heating the kettle body and enabling the materials in the reaction kettle to be heated more uniformly.
The bottom of the kettle body is provided with a heating rod inserted in the heating cavity, the heating rod carries out auxiliary heating on hot oil in the heating cavity, the cooling speed of the hot oil is reduced, and the heating effect is improved.
The outside of pressing from both sides the cover sets firmly insulating layer, plays the heat preservation effect to the whole cauldron body, prevents to carry out the heat transfer because of the heat that interior heating device and outer heating device produced and external environment, and leads to heating efficiency to reduce.
The bidirectional stirring device comprises a driving component, a stirring shaft and stirring blades, wherein the driving component comprises a driving motor, a first bevel gear, a second bevel gear and a third bevel gear; the driving motor is fixedly connected to the top of the kettle body, and an output shaft of the driving motor is fixedly connected with the third bevel gear; the first bevel gear is vertical to the third bevel gear and meshed at the lower end of the third bevel gear; the second bevel gear is vertical to the third bevel gear and meshed at the upper end of the third bevel gear; and starting the driving motor, driving the third bevel gear to rotate by the driving motor, and driving the first bevel gear and the second bevel gear to reversely rotate by the third bevel gear.
The stirring shaft comprises an inner shaft and an outer shaft, the outer shaft is sleeved on the inner shaft and is rotatably connected with the inner shaft, and the upper ends of the inner shaft and the outer shaft extend out of the top of the kettle body and are rotatably connected with the top of the kettle body; the upper end of the outer shaft is fixedly connected with the first bevel gear, and the upper end of the inner shaft extends out of the outer shaft and is fixedly connected with the second bevel gear; and the first bevel gear and the second bevel gear rotate reversely, so that the outer shaft and the inner shaft rotate reversely.
The stirring blades comprise an upper stirring blade and a lower stirring blade, the upper stirring blade is fixedly arranged on the outer shaft and is positioned on the upper layer of the kettle body, and the lower stirring blade is fixedly arranged on the inner shaft and is positioned on the lower layer of the kettle body; the outer shaft and the inner shaft rotate reversely, so that the upper stirring blade and the lower stirring blade rotate reversely.
The inner heating device comprises an inner heating rod, an outer heating ring, an upper heating sheet and a lower heating sheet, the inner heating rod is fixedly arranged inside the inner shaft, the outer heating ring is fixedly arranged on the inner surface of the outer shaft and is rotationally connected with the inner shaft, the upper heating sheet is fixedly arranged on the upper stirring blade, and the lower heating sheet is fixedly arranged on the lower stirring blade; go up stirring vane and stirring vane's antiport down, finally realize the antiport of going up heating plate and heating plate down to realized carrying out abundant antiport and heating to the material simultaneously, improved the mobility of material, be favorable to the heat exchange between the material, can make the material in the reation kettle be heated evenly, improved heating efficiency.
The upper stirring blade and the lower stirring blade are different in size, and the upper heating sheet and the lower heating sheet are different in size; stirring vane is different to the stirring degree of material with stirring vane down on the messenger, improves the mobility of material, goes up the heating plate simultaneously and heats the material with lower heating plate, helps the heat exchange between the material, makes the material in the reation kettle be heated more evenly.
The outer epaxial scraper blade frame that has set firmly with the internal wall of cauldron laminating mutually, the scraper blade frame rotates along the internal wall of cauldron under the drive of outer axle, can scrape the material that adheres on the internal wall of cauldron down, and the external heating device of being convenient for gets into the internal portion of cauldron with heat transfer, improves heating efficiency.
The implementation principle of the embodiment is as follows: when the reaction kettle heating device is used for heating materials, the driving motor is started, the driving motor drives the third bevel gear to rotate, and the third bevel gear drives the first bevel gear and the second bevel gear to rotate reversely; the first bevel gear drives the outer shaft to rotate, and the second bevel gear drives the inner shaft to rotate; thereby realize outer axle and interior reverse rotation of axle to and go up stirring vane and stirring vane's reverse rotation down, finally realize going up the reverse rotation of heating plate and heating plate down, thereby realized carrying out reverse stirring and heating fully to the material simultaneously, improved the mobility of material, be favorable to the heat exchange between the material, can make the material in the reation kettle be heated evenly, improve heating efficiency. Meanwhile, the scraping plate frame rotates along with the outer shaft, so that materials adhered to the inner wall of the kettle body can be scraped, and an external heating device can conveniently transfer heat into the kettle body. Meanwhile, high-temperature hot oil enters the heating cavity from an oil inlet pipe at the lower part of the jacket through an oil outlet of the hot oil pump and a pipeline to heat the kettle body; the cold oil with reduced temperature flows through the whole kettle body and flows back to the hot oil pump from the oil outlet pipe and the pipeline on the upper part of the jacket for circulating heating, thereby ensuring the temperature of the hot oil in the jacket. Meanwhile, the heating rod in the heating cavity carries out auxiliary heating on hot oil in the heating cavity, and the cooling speed of the hot oil is reduced. Simultaneously, insulating heat preservation plays the heat preservation effect to whole cauldron body, prevents to carry out the heat transfer because of heat and external environment, and leads to heating efficiency to reduce.
The heating device of the reaction kettle is a Chinese utility model patent (application number: CN 211800844U). Wherein, the reaction kettle in the above patent of the reaction kettle heating device in the application can be used.
Of course, the present embodiment can also be used for stirring the reaction kettle heating device of the high-efficiency sealed reaction kettle with other structures. The details are not repeated here, and the stirring mechanism of the high-efficiency sealed reaction kettle of the reaction kettle heating device of the embodiment of the present application is introduced below.
Referring to fig. 1-3, a high-efficiency sealed reaction kettle comprises a workbench 1, a filling opening 6, a discharge pipe 13, an electric cabinet 15 and a stirring mechanism;
the stirring mechanism comprises a stabilizer bar 3, a reaction kettle tank body 5, a stirring motor 7, a sealing bearing 8, a stirring rod 9, a driving rod 10, a stabilizing bearing 11 and a stirring blade 12, wherein the end part of the stabilizer bar 3 is fixedly connected with the inner wall surface of the reaction kettle tank body 5, the other end of the stabilizer bar 3 is fixedly connected with the wall surface of the stabilizing bearing 11, the inner part of the stabilizing bearing 11 is rotatably connected with the wall surface of the driving rod 10, the bottom end of the driving rod 10 is fixedly connected with the top end of the stirring blade 12, the wall surface of the driving rod 10 is rotatably connected with the inner part of the sealing bearing 8, the wall surface of the sealing bearing 8 is embedded into the top surface of the reaction kettle tank body 5, the top end of the driving rod 10 is fixedly connected with the end part of an output shaft of the stirring motor 7, the base of the stirring motor 7 is fixedly connected with the top surface of the reaction kettle tank body 5, and the end part of the stirring rod 9 is fixedly connected with the wall surface of the driving rod 10, the end part of an output shaft of the stirring motor 7 is fixedly connected with the top end of the driving rod 10, the stirring rod 9 is arranged on the wall surface of the driving rod 10, when the stirring motor 7 is started, the stirring rod 9 rotates to mix and stir materials in the reaction kettle tank body 5, the top end of the stirring blade 12 is fixedly connected with the bottom end of the driving rod 10, when the driving rod 10 rotates, the materials at the inner bottom of the reaction kettle tank body 5 are stirred through the stirring blade 12, the wall surface of the driving rod 10 is rotatably connected with the inner part of the sealing bearing 8, and then the wall surface of the sealing bearing 8 is embedded into the top surface of the reaction kettle tank body 5, so that the sealing effect is achieved;
the bottom surface of the electric cabinet 15 is fixedly connected with the top surface of the workbench 1, the bottom surface side of the workbench 1 is fixedly connected with the top surface of the supporting plate 19, the bottom surface of the supporting plate 19 is fixedly connected with the top surface side of the bottom plate 18, the top surface of the bottom plate 18 is provided with the storage box 17, the top surface of the workbench 1 is fixedly connected with the bottom surface of the fixed seat 2, the inside of the fixed seat 2 is provided with the heating plate 4, the inner wall of the heating plate 4 is tightly attached to the wall surface of the reaction kettle tank body 5, the top surface of the reaction kettle tank body 5 is provided with the pressure gauge 16, the heating plate 4 is arranged inside the fixed seat 2, then the inner wall of the heating plate 4 is tightly attached to the wall surface of the reaction kettle tank body 5, when the heating plate 4 is opened, the wall surface of the reaction kettle tank body 5 is heated, the stirring reaction of the materials inside is accelerated, and the pressure inside is observed by arranging the pressure gauge 16 on the top surface of the reaction kettle tank body 5, the bottom through connection reation kettle jar body 5's of filler 6 top surface through connection reation kettle jar body 5 with the bottom through connection reation kettle jar body 5's of filler 6 top surface to be convenient for toward the inside filling material of reation kettle jar body 5 the top through connection reation kettle jar body 5's of row material pipe 13 bottom surface, the wall of arranging material pipe 13 sets up solenoid valve 14, through the bottom surface with the top through connection reation kettle jar body 5 of row material pipe 13, sets up solenoid valve 14 at the wall of arranging material pipe 13, makes the inside material discharge that mixes the stirring of reation kettle jar body 5 when opening solenoid valve 14.
When the stirring device is used, the end part of an output shaft of a stirring motor 7 is fixedly connected with the top end of a driving rod 10, a stirring rod 9 is arranged on the wall surface of the driving rod 10, when the stirring motor 7 is started, the stirring rod 9 rotates to mix and stir materials in the reaction kettle tank body 5, the top end of a stirring blade 12 is fixedly connected with the bottom end of the driving rod 10, when the driving rod 10 rotates, the materials at the inner bottom of the reaction kettle tank body 5 are stirred through the stirring blade 12, the wall surface of the driving rod 10 is rotatably connected with the inside of a sealing bearing 8, then the wall surface of the sealing bearing 8 is embedded into the top surface of the reaction kettle tank body 5, so that the sealing effect is achieved, a heating plate 4 is arranged in a fixing seat 2, then the inner wall surface of the heating plate 4 is tightly attached to the wall surface of the reaction kettle tank body 5, when the heating plate 4 is opened, so that the wall surface of the reaction kettle tank body 5 is heated, accelerate the stirring reaction of its inside material, thereby observe its internal pressure through set up manometer 16 at the top surface that should the cauldron jar body 5, through the top surface with the bottom through connection reation kettle jar body 5 of filler 6 to be convenient for toward the inside filling material of the reation kettle jar body 5, through the bottom surface with the top through connection reation kettle jar body 5 of arranging row material pipe 13, arrange the wall of material pipe 13 and set up solenoid valve 14, make the inside material discharge that mixes the stirring of the reation kettle jar body 5 when opening solenoid valve 14.
The application has the advantages that:
1. through the top with agitator motor's output shaft tip fixed connection actuating lever, set up the puddler at the wall of actuating lever, make the puddler rotatory material to the inside of the reation kettle jar body mix the stirring when starting agitator motor, through the bottom with the top fixed connection actuating lever of stirring leaf, thereby stir the interior bottom material of the reation kettle jar body through the stirring leaf when the actuating lever is rotatory, through the inside with the wall rotation connection sealed bearing of actuating lever, then inside with sealed bearing's wall embedding reation kettle jar body's top surface, thereby play sealed effect.
2. Set up the hot plate through the inside at the fixing base, then the wall of the reation kettle jar body of closely laminating with the inner wall of hot plate, thereby heat the wall of the reation kettle jar body when opening the hot plate, thereby accelerate the stirring reaction of its inside material, thereby it observes its internal pressure to set up the manometer through the top surface that should the cauldron jar body, through the top surface with the bottom through connection reation kettle jar body of filler, thereby be convenient for toward the inside filling material of the reation kettle jar body, through the bottom surface with the top through connection reation kettle jar body of row material pipe, wall at row material pipe sets up the solenoid valve, make the good material of the internal portion mixing stirring of reation kettle jar discharge when opening the solenoid valve.
It is well within the skill of those in the art to implement, without undue experimentation, the present application is not directed to software and process improvements, as they relate to circuits and electronic components and modules.
The above description is only a preferred embodiment of the present application and is not intended to limit the present application, and various modifications and changes may be made by those skilled in the art. Any modification, equivalent replacement, improvement and the like made within the spirit and principle of the present application shall be included in the scope of the adjustment of the present application.

Claims (6)

1. The utility model provides a high-efficient sealed reation kettle which characterized in that: comprises a workbench (1), a filling port (6), a discharging pipe (13), an electric cabinet (15) and a stirring mechanism;
the stirring mechanism comprises a stabilizer bar (3), a reaction kettle tank body (5), a stirring motor (7), a sealing bearing (8), a stirring rod (9), a driving rod (10), a stabilizing bearing (11) and a stirring blade (12), wherein the end part of the stabilizer bar (3) is fixedly connected with the inner wall surface of the reaction kettle tank body (5), the other end of the stabilizer bar (3) is fixedly connected with the wall surface of the stabilizing bearing (11), the inner part of the stabilizing bearing (11) is rotatably connected with the wall surface of the driving rod (10), the bottom end of the driving rod (10) is fixedly connected with the top end of the stirring blade (12), the wall surface of the driving rod (10) is rotatably connected with the inner part of the sealing bearing (8), the wall surface of the sealing bearing (8) is embedded into the top surface of the reaction kettle tank body (5), and the top end part of the driving rod (10) is fixedly connected with the end part of an output shaft of the stirring motor (7), the base of the stirring motor (7) is fixedly connected with the top surface of the reaction kettle tank body (5), and the end part of the stirring rod (9) is fixedly connected with the wall surface of the driving rod (10).
2. The high-efficiency sealed reaction kettle according to claim 1, wherein: the bottom surface of the electric cabinet (15) is fixedly connected with the top surface of the workbench (1).
3. The high-efficiency sealed reaction kettle according to claim 1, wherein: the top surface of bottom surface avris fixed connection backup pad (19) of workstation (1), the top surface avris of bottom surface fixed connection bottom plate (18) of backup pad (19), the top surface of bottom plate (18) sets up receiver (17).
4. The high-efficiency sealed reaction kettle according to claim 1, wherein: the bottom surface of top surface fixed connection fixing base (2) of workstation (1), the inside of fixing base (2) sets up hot plate (4), the wall of the reation kettle jar body (5) is closely laminated to the inner wall of hot plate (4), the top surface of answering the cauldron jar body (5) sets up manometer (16).
5. The high-efficiency sealed reaction kettle according to claim 1, wherein: the bottom end of the filling port (6) is connected with the top surface of the reaction kettle tank body (5) in a penetrating way.
6. The high-efficiency sealed reaction kettle according to claim 1, wherein: the top end of the discharge pipe (13) is connected with the bottom surface of the reaction kettle tank body (5) in a penetrating way, and the wall surface of the discharge pipe (13) is provided with an electromagnetic valve (14).
CN202123153252.2U 2021-12-14 2021-12-14 High-efficient sealed reation kettle Active CN216499341U (en)

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CN202123153252.2U CN216499341U (en) 2021-12-14 2021-12-14 High-efficient sealed reation kettle

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115922944A (en) * 2023-03-15 2023-04-07 苏州汇博塑化有限公司 PVC material preparation facilities for optical cable

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115922944A (en) * 2023-03-15 2023-04-07 苏州汇博塑化有限公司 PVC material preparation facilities for optical cable

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