CN216473531U - Anode electrochemical oxidation preparation device of titanium dioxide nanotube - Google Patents
Anode electrochemical oxidation preparation device of titanium dioxide nanotube Download PDFInfo
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- CN216473531U CN216473531U CN202120883652.XU CN202120883652U CN216473531U CN 216473531 U CN216473531 U CN 216473531U CN 202120883652 U CN202120883652 U CN 202120883652U CN 216473531 U CN216473531 U CN 216473531U
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Abstract
The utility model discloses an anodic electrochemical oxidation preparation device of a titanium dioxide nanotube, which relates to the technical field of anodic electrochemical oxidation preparation, solves the problems that an electrode connector on a reaction vessel cannot be fixed and the electrode connector and a pure titanium sheet or a platinum sheet cannot be fixed, and has the technical scheme that: comprises a reactor, the upper end of the reactor is open, and a fixed plate is clamped at the upper end of the reactor; one side of the upper surface of the fixing plate is provided with placing grooves which are arranged at intervals in a penetrating way, and one end of the fixing plate, which passes through the inside of the placing grooves, is provided with a mounting groove in a penetrating way; the edge of the fixing plate passing through the mounting groove is provided with a slope, the fixing plate is provided with round holes arranged at intervals through the slope, the fixing plate is provided with a spring through the round holes, and the outer end of the spring is connected with a lapping rod; the purpose of avoiding the pure titanium sheet or the platinum sheet from falling off in the preparation process is achieved, the electrode connector can be fixed, and the smooth preparation of the anode of the titanium dioxide nanotube is facilitated.
Description
Technical Field
The utility model relates to the technical field of anodic electrochemical oxidation preparation, in particular to an anodic electrochemical oxidation preparation device of a titanium dioxide nanotube.
Background
The electrochemical oxidation is a method of putting solution or suspension of organic matters into an electrolytic bath, capturing electrons on an anode through direct current to oxidize the organic matters or oxidize low-valence metal into high-valence metal ions, and then oxidizing the organic matters again through the high-valence metal ions. Therefore, an anode electrochemical oxidation preparation device of the titanium dioxide nanotube is provided.
SUMMERY OF THE UTILITY MODEL
The utility model aims to provide an anodic electrochemical oxidation preparation device of a titanium dioxide nanotube, which achieves the aim of avoiding the falling of a pure titanium sheet or a platinum sheet in the preparation process, can complete the fixation of an electrode connector and is further beneficial to the smooth preparation of the anode of the titanium dioxide nanotube.
The technical purpose of the utility model is realized by the following technical scheme: the device comprises a reactor, wherein the reactor is cylindrical, the upper end of the reactor is open, and a fixing plate is clamped at the upper end of the reactor;
one side of the upper surface of the fixed plate is provided with placing grooves which are arranged at intervals in a penetrating way, and one end of the fixed plate passing through the inside of the placing grooves is provided with a mounting groove in a penetrating way;
the edge of the fixing plate passing through the mounting groove is provided with a slope, the fixing plate is provided with round holes arranged at intervals through the slope, the fixing plate is provided with a spring through the round holes, and the outer end of the spring is fixedly connected with an overlapping rod;
the electrode device comprises a fixed plate, a plurality of transverse power-on rods, a base, a plurality of clamping plates, electrode rods, a power-on rod and a plurality of plastic tubes, wherein the fixed plate is provided with the plastic tubes through a mounting groove, the lower ends of the plastic tubes are fixedly connected with the base, the lower ends of the base are fixedly connected with the clamping plates which are arranged at intervals, the inner sides of the clamping plates are fixedly provided with the plurality of transverse power-on rods, the electrode rods are jointly arranged between the plastic tubes and the clamping plates, the lower ends of the electrode rods are connected with the power-on rods, and the upper ends of the electrode rods extend to the upper parts of the clamping plates;
and a liquid discharge pipe penetrates through the middle part of the lower surface of the reactor, and a pipeline valve is arranged on the liquid discharge pipe, so that the reaction solution can be conveniently replaced and added.
The utility model is further configured to: the lower surface of the fixed plate is provided with an arc-shaped clamping groove corresponding to the upper end of the reactor, and the upper end of the reactor is matched with the top end of the inside of the clamping groove.
Through adopting above-mentioned technical scheme, form fixedly between fixed plate and the reactor, avoid the in-process fixed plate skew of preparation reaction to lead to the condition of preparation failure.
The utility model is further configured to: the outer ring surface of the plastic pipe corresponding to the upper surface of the fixed plate is sleeved with a carrying seat, and the lower end of the outer ring surface of the carrying seat is provided with a slope corresponding to the mounting groove.
Through adopting above-mentioned technical scheme, carry on between the upper end of seat and mounting groove the phase-match, be convenient for form fixed, the connection form that agrees with.
The utility model is further configured to: the slope on the carrying seat is provided with a circular groove, the circular groove is annular, and the circular groove is matched with the carrying rod.
Through adopting above-mentioned technical scheme, further through the connected mode that pushes up between circular recess and the take pole mutually, the cooperation spring forms closely fixedly.
The utility model is further configured to: the clamping plate is provided with a threaded hole in a penetrating mode, the clamping plate is provided with a threaded rod through the threaded hole, and the clamping plate and the threaded rod are made of rubber materials.
By adopting the technical scheme, the clamping plate made of the rubber material can deform, so that the pure titanium sheet and the platinum sheet can be clamped conveniently.
The utility model is further configured to: the outer ring surfaces of the threaded rod corresponding to the two clamping plates are respectively provided with left-handed threads and right-handed threads, and the threaded rod is in threaded connection with the two clamping plates through the left-handed threads and the right-handed threads.
Through adopting above-mentioned technical scheme, be provided with the connected mode between the threaded rod of left-handed screw and right-handed screw and the grip block for when twisting the threaded rod, two grip blocks can form removal in opposite directions, and then accomplish the centre gripping or become flexible.
Compared with the prior art, the utility model has the following beneficial effects: the purpose of avoiding the pure titanium sheet or the platinum sheet from falling off in the preparation process is achieved, the electrode connector can be fixed, and the smooth preparation of the anode of the titanium dioxide nanotube is facilitated.
Drawings
The accompanying drawings, which are included to provide a further understanding of the embodiments of the utility model and are incorporated in and constitute a part of this application, illustrate embodiment(s) of the utility model and together with the description serve to explain the principles of the utility model. In the drawings:
FIG. 1 is a schematic structural view of the present invention;
FIG. 2 is a bottom view of the present invention;
FIG. 3 is a schematic structural diagram of a fixing plate according to the present invention;
FIG. 4 is an enlarged schematic view of the utility model at A;
FIG. 5 is a schematic view of the conductive rod of the present invention;
fig. 6 is a cut-away view of a conductive rod of the present invention.
Reference numbers and corresponding part names in the drawings:
1. a reactor; 2. a fixing plate; 3. an electrode rod; 4. plastic pipes; 5. a mounting seat; 6. a placement groove; 7. a liquid discharge pipe; 8. A pipeline valve; 9. a card slot; 10. mounting grooves; 11. building a rod; 12. a spring; 13. a circular groove; 14. a base; 15. a clamping plate; 16. a power-on pole; 17. a threaded rod.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention is further described in detail below with reference to examples and accompanying drawings, and the exemplary embodiments and descriptions thereof are only used for explaining the present invention and are not meant to limit the present invention.
It will be understood that when an element is referred to as being "secured to" or "disposed on" another element, it can be directly on the other element or be indirectly on the other element. When an element is referred to as being "connected to" another element, it can be directly or indirectly connected to the other element.
It will be understood that the terms "length," "width," "upper," "lower," "front," "rear," "left," "right," "vertical," "horizontal," "top," "bottom," "inner," "outer," and the like, as used herein, refer to an orientation or positional relationship indicated in the drawings that is solely for the purpose of facilitating the description and simplifying the description, and do not indicate or imply that the device or element being referred to must have a particular orientation, be constructed and operated in a particular orientation, and is therefore not to be construed as limiting the utility model.
Furthermore, the terms "first", "second" and "first" are used for descriptive purposes only and are not to be construed as indicating or implying relative importance or implicitly indicating the number of technical features indicated. Thus, a feature defined as "first" or "second" may explicitly or implicitly include one or more of that feature. In the description of the present invention, "a plurality" means two or more unless specifically defined otherwise.
Example (b): an anodic electrochemical oxidation preparation device of a titanium dioxide nanotube comprises a reactor 1, wherein the reactor 1 is cylindrical, the upper end of the reactor 1 is open, and a fixing plate 2 is clamped at the upper end of the reactor 1;
one side of the upper surface of the fixed plate 2 is provided with placing grooves 6 which are arranged at intervals in a penetrating way, and one end of the fixed plate 2 passing through the inside of the placing grooves 6 is provided with a mounting groove 10 in a penetrating way;
the edge of the fixed plate 2 passing through the mounting groove 10 is provided with a slope, the fixed plate 2 passes through the slope and is provided with round holes arranged at intervals, the fixed plate 2 is provided with a spring 12 through the round hole, and the outer end of the spring 12 is fixedly connected with an overlapping rod 11;
the fixed plate 2 is provided with a plastic pipe 4 through an installation groove 10, the lower end of the plastic pipe 4 is fixedly connected with a base 14, the lower end of the base 14 is fixedly connected with clamping plates 15 arranged at intervals, a plurality of transversely arranged power-on rods 16 are fixedly arranged on the inner sides of the clamping plates 15, electrode rods 3 are jointly arranged between the plastic pipe 4 and the clamping plates 15, the lower ends of the electrode rods 3 are connected with the power-on rods 16, and the upper ends of the electrode rods 3 extend to the upper side of the clamping plates 15;
a liquid discharge pipe 7 penetrates through the middle part of the lower surface of the reactor 1, and a pipeline valve 8 is arranged on the liquid discharge pipe 7.
As shown in fig. 1, 2 and 4, an arc-shaped clamping groove 9 is formed in the lower surface of the fixing plate 2 corresponding to the upper end of the reactor 1, the upper end of the reactor 1 is matched with the top end of the inner part of the clamping groove 9, a carrying seat 5 is sleeved on the outer annular surface of the plastic pipe 4 corresponding to the upper surface of the fixing plate 2, and a slope corresponding to the mounting groove 10 is formed in the lower end of the outer annular surface of the carrying seat 5.
As shown in fig. 3, 4 and 5, a circular groove 13 is formed in the slope of the carrying seat 5, the circular groove 13 is annular, the circular groove 13 is matched with the carrying rod 11, a threaded hole is formed in the clamping plates 15 in a penetrating mode, a threaded rod 17 is installed on each clamping plate 15 through the threaded hole, the threaded rod 17 is respectively provided with a left-handed thread and a right-handed thread corresponding to the outer annular surfaces of the two clamping plates 15, and the clamping plates 15 and the threaded rod 17 are made of rubber materials, and the threaded rod 17 is respectively in threaded connection with the two clamping plates 15 through the left-handed thread and the right-handed thread.
The working principle is as follows: when the device is used, firstly, pure titanium and platinum sheets are respectively placed between the clamping plates 15, the threaded rod 17 is screwed, and the left-handed threads and the right-handed threads on the threaded rod 17 respectively enable the clamping plates 15 to move close to each other, so that the pure titanium sheets and the platinum sheets are respectively clamped and fixed;
then, the electrode rod 3 with the plastic tube 4 and the carrying seat 5 is placed in the mounting groove 10 through the placing groove 6, the electrode rod 3 is pressed downwards according to the mode that the circular groove 13 below the carrying seat 5 is matched with the lapping rod 11, the spring 12 below the lapping rod 11 is contracted, the lapping rod 11 and the circular groove 13 are mutually jacked under the action force of the spring 12 which is restored to the original state, and the effect of fixing the electrode rod 3 is achieved;
in conclusion: the device has reached the purpose of avoiding pure titanium piece or platinum piece to drop in the preparation process, and can accomplish the fixed of electrode connection head, and then is favorable to going on smoothly of the positive pole preparation of titanium dioxide nanotube.
The above-mentioned embodiments are intended to illustrate the objects, technical solutions and advantages of the present invention in further detail, and it should be understood that the above-mentioned embodiments are merely exemplary embodiments of the present invention, and are not intended to limit the scope of the present invention, and any modifications, equivalent substitutions, improvements and the like made within the spirit and principle of the present invention should be included in the scope of the present invention.
Claims (6)
1. The device for preparing the titanium dioxide nanotube by anodic electrochemical oxidation comprises a reactor (1) and is characterized in that the reactor (1) is cylindrical, the upper end of the reactor (1) is open, and a fixing plate (2) is clamped at the upper end of the reactor (1);
one side of the upper surface of the fixed plate (2) is provided with placing grooves (6) which are arranged at intervals in a penetrating way, and one end of the fixed plate (2) passing through the inside of the placing grooves (6) is provided with a mounting groove (10) in a penetrating way;
the edge of the fixing plate (2) passing through the mounting groove (10) is provided with a slope, the fixing plate (2) is provided with round holes arranged at intervals through the slope, the fixing plate (2) is provided with a spring (12) through the round hole, and the outer end of the spring (12) is fixedly connected with an overlapping rod (11);
the plastic pipe (4) is arranged on the fixing plate (2) through a mounting groove (10), a base (14) is fixedly connected to the lower end of the plastic pipe (4), clamping plates (15) arranged at intervals are fixedly connected to the lower end of the base (14), a plurality of power-on rods (16) transversely arranged are fixedly arranged on the inner sides of the clamping plates (15), electrode rods (3) are jointly arranged between the plastic pipe (4) and the clamping plates (15), the lower ends of the electrode rods (3) are connected with the power-on rods (16), and the upper ends of the electrode rods (3) extend to the upper portions of the clamping plates (15);
the middle part of the lower surface of the reactor (1) is provided with a liquid discharge pipe (7) in a penetrating way, and the liquid discharge pipe (7) is provided with a pipeline valve (8).
2. The device for preparing the titanium dioxide nanotube by the anodic electrochemical oxidation as claimed in claim 1, wherein the lower surface of the fixing plate (2) is provided with an arc-shaped clamping groove (9) corresponding to the upper end of the reactor (1), and the upper end of the reactor (1) is matched with the inner top end of the clamping groove (9).
3. The device for preparing titanium dioxide nanotubes by anodic electrochemical oxidation as claimed in claim 1, wherein the plastic tube (4) is sleeved with a carrying seat (5) corresponding to the outer circumferential surface of the upper surface of the fixing plate (2), and the lower end of the outer circumferential surface of the carrying seat (5) is provided with a slope corresponding to the mounting groove (10).
4. The device for preparing the titanium dioxide nano tube by the anodic electrochemical oxidation as claimed in claim 3, wherein the slope of the carrying seat (5) is provided with a circular groove (13), the circular groove (13) is annular, and the circular groove (13) is matched with the lapping rod (11).
5. The device for preparing the titanium dioxide nano tube by the anodic electrochemical oxidation is characterized in that threaded holes are formed between the clamping plates (15) in a penetrating mode, threaded rods (17) are installed on the clamping plates (15) through the threaded holes, and the clamping plates (15) and the threaded rods (17) are made of rubber materials.
6. The device for preparing the titanium dioxide nanotubes by the anodic electrochemical oxidation as claimed in claim 5, wherein the threaded rod (17) has left-handed threads and right-handed threads corresponding to the outer annular surfaces of the two clamping plates (15), and the threaded rod (17) is in threaded connection with the two clamping plates (15) through the left-handed threads and the right-handed threads.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202120883652.XU CN216473531U (en) | 2021-04-27 | 2021-04-27 | Anode electrochemical oxidation preparation device of titanium dioxide nanotube |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202120883652.XU CN216473531U (en) | 2021-04-27 | 2021-04-27 | Anode electrochemical oxidation preparation device of titanium dioxide nanotube |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN216473531U true CN216473531U (en) | 2022-05-10 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202120883652.XU Active CN216473531U (en) | 2021-04-27 | 2021-04-27 | Anode electrochemical oxidation preparation device of titanium dioxide nanotube |
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| Country | Link |
|---|---|
| CN (1) | CN216473531U (en) |
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2021
- 2021-04-27 CN CN202120883652.XU patent/CN216473531U/en active Active
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