CN216137259U - Distillation apparatus - Google Patents

Distillation apparatus Download PDF

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Publication number
CN216137259U
CN216137259U CN202121644369.8U CN202121644369U CN216137259U CN 216137259 U CN216137259 U CN 216137259U CN 202121644369 U CN202121644369 U CN 202121644369U CN 216137259 U CN216137259 U CN 216137259U
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container
heating
pipe
water outlet
water inlet
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CN202121644369.8U
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刘敬河
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Huizhou Huaboke Micro Semiconductor Equipment Co ltd
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Shenzhen Bodajing Technology Industry Co ltd
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Abstract

The present application relates to a distillation apparatus comprising a console, an installation box, a first container and a second container; the top of the installation box is fixedly provided with a heating element, the top of the heating element is provided with a nano heating layer, the first container is placed on the nano heating layer, and the nano heating layer is used for heating materials in the first container; the first container is provided with a condensing pipe which is communicated with the first container; a circulating device is arranged in the installation box and communicated with the condensing pipe so as to circulate condensed water in the condensing pipe; the control console is fixed at the side of the installation box, a controller is arranged in the control console, and the controller is electrically connected with the heating element and used for controlling the heating element to heat; the second container is placed on the top table surface of the console, and a water inlet of the second container is communicated with a water outlet of the condensation pipe. The nano heating technology is adopted, so that no electromagnetic field interference and damage exist in the heating process, the whole structure is compact, and the occupied space is reduced.

Description

Distillation apparatus
Technical Field
The application relates to the field of laboratory instruments, in particular to a distillation device.
Background
The distillation apparatus can be widely applied to various places needing distillation treatment in chemical laboratories such as environmental protection, disease control, aquatic products, water supply and drainage, universities, scientific research institutions, industrial and mining enterprises and the like, such as distillation treatment of volatile phenol, cyanide, ammonia nitrogen, Kjeldahl nitrogen, oil moisture and other items.
At present, a heating mode of a mechanical assembly is adopted in many chemical laboratories, and larger electromagnetic field interference and harm exist.
Disclosure of Invention
In view of the above, the present application provides a distillation apparatus, which employs a nano heating technology so that there is no electromagnetic field interference and damage during heating, and the whole structure is compact, and the occupied space is reduced.
According to an aspect of the present application, there is provided a distillation apparatus comprising a console, a mounting box, a first container and a second container;
the top of the mounting box is fixedly provided with a heating element, the top of the heating element is provided with a nano heating layer, the first container is placed on the nano heating layer, and the nano heating layer is used for heating materials in the first container;
a condensation pipe is arranged on the first container and is communicated with the first container;
a circulating device is arranged in the installation box and communicated with the condensing pipe, so that the condensed water circulates in the condensing pipe;
the control console is fixed on the side of the installation box, a controller is arranged in the control console, and the controller is electrically connected with the heating element and used for controlling the heating element to heat;
the second container is placed on the top table surface of the console, and a water inlet of the second container is communicated with a water outlet of the condensation pipe.
In a possible implementation manner, the number of the heating members is more than two, and the more than two heating members are sequentially arranged at the top of the installation box;
the number of the first containers is matched with that of the heating elements, and the first containers are placed on the nano heating layers of the heating elements in a one-to-one correspondence manner;
the number of the condensing pipes is matched with that of the first containers, and the condensing pipes are communicated with the first containers in a one-to-one correspondence manner;
the number of the second containers is matched with that of the condensation pipes, and the second containers are arranged in one-to-one correspondence with the condensation pipes.
In a possible implementation manner, the two heating members are sequentially arranged in a linear shape, and the circulating device is provided with a first water outlet and a first water inlet;
a first water outlet pipeline is arranged at the first water outlet, a first water inlet pipeline is arranged at the first water inlet, and the first water outlet pipeline and the first water inlet pipeline both extend out of the installation box;
the bottom of each condensing pipe is provided with a circulating water inlet, and the top of each condensing pipe is provided with a circulating water outlet;
the first water outlet pipe is communicated with a circulating water inlet of the condenser pipe at one end, and the first water inlet pipe is communicated with a circulating water outlet of the condenser pipe at the other end;
and the circulating water inlet and the circulating water outlet of the adjacent condensation pipe are communicated.
In a possible implementation manner, a first clamping frame is further arranged on the installation box and arranged beside the heating element to clamp the first container.
In one possible implementation, the first clamping frame comprises a support rod, a clamp and an adjusting knob;
the supporting rod is vertically fixed at the top of the installation box and is positioned beside the heating element;
the clamp comprises a clamping jaw and a connecting column, a through hole is formed in the side wall of the connecting column and matched with the supporting rod, the clamping jaw is fixedly installed at one end of the connecting column, and the clamping jaw is used for clamping the first container;
the other end of the connecting column is provided with a threaded hole which is communicated with the through hole;
and a screw rod is arranged at one end of the adjusting knob and is matched with the threaded hole.
In a possible implementation manner, the clamping device further comprises a second clamping frame;
the second clamping frame is fixedly installed on one side, facing the console, of the installation box and used for clamping the bottom of the condensation pipe.
In one possible implementation manner, the second clamping frame comprises a fixed part, a movable clamping part and a fixed clamping part;
the fixing part is plate-shaped, and one end of the fixing part is fixedly connected with the installation box;
the fixed clamping part and the movable clamping part are both in omega-shaped structures matched with the tube body of the condensation tube, the movable clamping part and the fixed clamping part are detachably connected, and the opening of the movable clamping part and the opening of the fixed clamping part are oppositely arranged;
and one side of the fixed clamping part, which is not connected with the movable clamping part, is fixedly connected with the fixed part.
In a possible implementation manner, a groove for placing the first container is formed in the top of the heating element, and the groove is hemispherical;
the structure of nanometer zone of heating with the top structure phase-match of heating member.
In one possible implementation, the condensation duct is located at a position directly above the water inlet of the second container;
the water outlet of the condensation pipe is arranged downwards, a water outlet pipe is arranged at the water outlet of the condensation pipe, and the water inlet of the second container is penetrated through by the water outlet pipe and extends into the second container.
In one possible implementation manner, the console and the installation box are connected in an L shape;
the height of the control console is smaller than that of the installation box.
When distillation experiment is carried out to distillation plant in this application embodiment, at first heat the experimental material in the first container through the nanometer zone of heating in the control cabinet control heating piece. The nano heating layer adopts a nano heating technology without adopting a mechanical heating component, can be dried and burnt, and has no interference and harm of an electromagnetic field during heating. After the test material in the first vessel had been heated, the resulting vapor was passed to a condenser tube for condensation. And a circulating device for conveying condensed water to the condensing pipe is arranged in the installation box, so that heat can be taken away through the circulating device, and gas generated by experimental materials is always in a rapid condensing effect. Condensate generated after the gas generated by the experimental material is condensed can enter the second container through the water outlet of the condensation pipe to be collected. In summary, the distillation apparatus of the embodiment of the present application enables no electromagnetic field interference and damage during heating by adopting the nano heating technology, and the whole structure is compact, thereby reducing the occupied space.
Other features and aspects of the present application will become apparent from the following detailed description of exemplary embodiments, which proceeds with reference to the accompanying drawings.
Drawings
The accompanying drawings, which are incorporated in and constitute a part of this specification, illustrate exemplary embodiments, features, and aspects of the application and, together with the description, serve to explain the principles of the application.
FIG. 1 is a view showing a main structure of a distillation apparatus according to an embodiment of the present application;
FIG. 2 shows an isometric view of a distillation apparatus of an embodiment of the present application;
FIG. 3 is a view showing the structure of a first holding frame and a second holding frame of a distillation apparatus according to an embodiment of the present application;
FIG. 4 shows an isometric view of a first holder and a second holder of a distillation apparatus of an embodiment of the present application;
fig. 5 is a sectional view showing a heating element of a distillation apparatus according to an embodiment of the present application.
Detailed Description
Various exemplary embodiments, features and aspects of the present application will be described in detail below with reference to the accompanying drawings. In the drawings, like reference numbers can indicate functionally identical or similar elements. While the various aspects of the embodiments are presented in drawings, the drawings are not necessarily drawn to scale unless specifically indicated.
It will be understood, however, that the terms "central," "longitudinal," "lateral," "length," "width," "upper," "lower," "front," "rear," "left," "right," "vertical," "horizontal," "top," "bottom," "inner," "outer," "clockwise," "counterclockwise," "axial," "radial," "circumferential," and the like are used in an orientation or positional relationship indicated in the drawings for convenience in describing or simplifying the description, and do not indicate or imply that the device or element so referred to must have a particular orientation, be constructed and operated in a particular orientation, and thus should not be considered as limiting the utility model.
Furthermore, the terms "first", "second" and "first" are used for descriptive purposes only and are not to be construed as indicating or implying relative importance or implicitly indicating the number of technical features indicated. Thus, a feature defined as "first" or "second" may explicitly or implicitly include one or more of that feature. In the description of the present invention, "a plurality" means two or more unless specifically defined otherwise.
The word "exemplary" is used exclusively herein to mean "serving as an example, embodiment, or illustration. Any embodiment described herein as "exemplary" is not necessarily to be construed as preferred or advantageous over other embodiments.
Furthermore, in the following detailed description, numerous specific details are set forth in order to provide a better understanding of the present application. It will be understood by those skilled in the art that the present application may be practiced without some of these specific details. In some instances, methods, means, elements and circuits that are well known to those skilled in the art have not been described in detail so as not to obscure the present application.
Fig. 1 is a main structure diagram of a distillation apparatus according to an embodiment of the present application. Fig. 2 shows an isometric view of a distillation apparatus of an embodiment of the present application. Fig. 3 shows a configuration diagram of a first holding frame and a second holding frame of a distillation apparatus according to an embodiment of the present application. Fig. 4 shows an isometric view of a first and second holder of a distillation apparatus of an embodiment of the present application. Fig. 5 is a sectional view showing a heating element of a distillation apparatus according to an embodiment of the present application. As shown in fig. 1, fig. 2, fig. 3, fig. 4, or fig. 5, the distillation apparatus includes: control cabinet 100, install bin 200, first container 300 and second container 400, the top fixed mounting of install bin 200 has heating member 500, and the top of heating member 500 is provided with the nanometer zone of heating, and first container 300 is placed on the nanometer zone of heating, and the nanometer zone of heating is used for heating the material in the first container 300. The condensation duct 600 is installed on the first container 300, and the condensation duct 600 communicates with the first container 300. A circulation device is arranged in the installation box 200 and communicated with the condensation pipe 600, so that the condensed water circulates in the condensation pipe 600. The control console 100 is fixed at the side of the installation box 200, a controller is arranged in the control console 100, and the controller is electrically connected with the heating member 500 and used for controlling the heating member 500 to heat. The second container 400 is placed on the top table of the console 100, and the water inlet of the second container 400 is communicated with the water outlet of the condensation duct 600.
Here, it should be noted that the nano heating layer may be implemented by a nano ceramic heating element, and details are not described here. The control program that the controller can control the nano-heating layer of the heating member 500 to heat the first container 300 can be implemented by the conventional technical means of those skilled in the art, and will not be described in detail herein.
When the distillation apparatus according to the embodiment of the present application performs a distillation experiment, the nano heating layer in the heating member 500 is first controlled by the console 100 to heat the experimental material in the first container 300. The nano heating layer adopts a nano heating technology without adopting a mechanical heating component, can be dried and burnt, and has no interference and harm of an electromagnetic field during heating. After the test material in the first container 300 is heated, the generated steam flows to the condensation pipe 600 to be condensed. And a circulating device for conveying condensed water to the condensing pipe 600 is arranged in the installation box 200, so that heat can be taken away through the circulating device, and gas generated by experimental materials is always in a rapid condensing effect. Condensed liquid generated after the gas generated from the experimental material is condensed may enter the second container 400 through the water outlet of the condensation pipe 600 to be collected. In summary, the distillation apparatus of the embodiment of the present application enables no electromagnetic field interference and damage during heating by adopting the nano heating technology, and the whole structure is compact, thereby reducing the occupied space.
In one possible implementation, the heating members 500 are provided in two or more, and the two or more heating members 500 are sequentially arranged on the top of the installation case 200. The number of the first containers 300 is matched with the number of the heating members 500, and the first containers 300 are disposed on the nano-heating layers of the heating members 500 in a one-to-one correspondence. The number of the condensation pipes 600 is matched with the number of the first containers 300, and the condensation pipes 600 are communicated with the first containers 300 in a one-to-one correspondence manner. The number of the second containers 400 is matched with the number of the condensation pipes 600, and the second containers 400 are arranged in one-to-one correspondence with the condensation pipes 600. Therefore, multi-line heating can be performed, and heating efficiency is improved.
Further, in a possible implementation manner, the two heating members 500 are arranged in a linear shape in sequence, and the circulating device is provided with a first water outlet and a first water inlet. A first water outlet 1010 is formed in the first water outlet, a first water inlet pipe 1020 is formed in the first water inlet, and the first water outlet 1010 and the first water inlet pipe 1020 extend out of the installation box 200. The bottom of every condenser pipe 600 all is equipped with the circulation water inlet, and the top of every condenser pipe 600 all is equipped with the circulation delivery port. The first water outlet pipe 1010 is communicated with a circulation water inlet of the condensation pipe 600 at one end, and the first water inlet pipe 1020 is communicated with a circulation water outlet of the condensation pipe 600 at the other end. The circulation water inlet and the circulation water outlet of the adjacent condensation pipe 600 are communicated. Therefore, the structure of the embodiment of the application is further optimized.
Here, it should be noted that, in one possible implementation, the circulating means can be implemented by conventional technical means of those skilled in the art, and the details are not described here.
In one possible implementation, the mounting box 200 is further provided with a first clamping frame 700, and the first clamping frame 700 is disposed beside the heating element 500 for clamping the first container 300. Thereby, the first container 300 is more stabilized.
Further, in one possible implementation, the first clamping frame 700 includes a supporting rod 710, a clamp 720 and an adjusting knob 730, the supporting rod 710 is vertically fixed on the top of the mounting box 200, and the supporting rod 710 is located beside the heating member 500. The clamp 720 comprises a clamping jaw 721 and a connecting column 722, a through hole is arranged on the side wall of the connecting column 722, the through hole is matched with the supporting rod 710, the clamping jaw 721 is fixedly arranged at one end of the connecting column 722, and the clamping jaw 721 is used for clamping the first container 300. The other end of the connecting column 722 is provided with a threaded hole which is communicated with the through hole, one end of the adjusting knob 730 is provided with a screw rod, and the screw rod is matched with the threaded hole. Therefore, the first container 300 can be clamped by the clamping jaws 721, and the screw abuts against the supporting rod 710 by rotating the adjusting knob 730, so as to fix the clamping jaws 721. When the height of the clamping jaw 721 is adjusted, the adjusting knob 730 is rotated to separate the screw from the supporting rod 710, and the clamping jaw 721 is moved.
In a possible implementation manner, a second clamping frame 800 is further included, the second clamping frame 800 is fixedly installed on a side of the installation box 200 facing the console 100, and the second clamping frame 800 is used for clamping the bottom of the condensation duct 600. Thereby, the installation of the condensation duct 600 may be more stable.
Further, in a possible implementation manner, the second clamping frame 800 includes a fixing portion 830, a movable clamping portion 810 and a fixed clamping portion 820, the fixing portion 830 is plate-shaped, and one end of the fixing portion 830 is fixedly connected with the mounting box 200. Decide joint portion 820 and move joint portion 810 and all be "omega" column structure with the pipe shaft assorted of condenser pipe 600, move joint portion 810 and decide joint portion 820 and can dismantle the connection, move the opening of joint portion 810 and decide the opening of joint portion 820 and set up relatively. The side of the fixed clamping part 820 not connected with the movable clamping part 810 is fixedly connected with the fixed part 830. Therefore, the structure of the embodiment of the application is further optimized.
Here, it should be noted that in one possible implementation, a fixed column 821 is provided at a side of the fixed clamping part 820 not connected to the movable clamping part 810, and an end of the fixed column 821 not connected to the fixed clamping part 820 is fixedly connected to the fixed part 830.
Here, it should also be noted that, in one possible implementation, the fixing portion 830 has a "Z" shaped plate shape. Wherein, fixed part 830 includes first plate, second face and the third plate that is "Z" font and connects, has seted up the mounting hole more than two on the face of first plate, has seted up the screw thread mounting hole that corresponds with the mounting hole case on the install bin 200, from this, can make one side that first plate is not connected with the second plate pass through bolted connection with install bin 200. The fixed clamping part 820 is fixedly connected with one side of the third plate, which is far away from the second plate.
In a possible implementation manner, a groove for placing the first container 300 is formed in the top of the heating member 500, the groove is hemispherical, and the structure of the nano heating layer matches with the top structure of the heating member 500. Therefore, the heating area of the first container 300 can be increased through the grooves, so that the heating effect of the substances to be distilled in the first container is better, and the distillation efficiency is higher. Here, it should be noted that, furthermore, the heating element 500 may be implemented by using a hemispherical microcrystalline ceramic heating jacket, which is not described herein.
Here, it should be noted that in one possible implementation, the heating member 500 is in the shape of a rectangular block, and the nano-heating layer is disposed on top of the heating member 500, and the nano-heating layer is in a rectangular structure matching the heating member 500. The bottom of heating member 500 is equipped with the support column, and the support column is equipped with four, and four support columns set up respectively in the bottom four corners department of heating member 500, and the support column is all fixed at the top of install bin 200.
In a possible implementation manner, the condensation pipe 600 is located right above the water inlet of the second container 400, the water outlet of the condensation pipe 600 is arranged downward, the water outlet of the condensation pipe 600 is provided with a water drainage pipe 900, and the water drainage pipe 900 penetrates through the water inlet of the second container 400 and extends into the interior of the second container 400. Therefore, the structure of the embodiment of the application is further optimized.
In one possible implementation, the console 100 and the installation box 200 are connected in an "L" shape, and the height of the console 100 is smaller than that of the installation box 200. Thereby, the structure of the embodiment of the present application is further optimized.
Here, it should be noted that in one possible implementation, the console 100 is in the shape of a rectangular table, and the side of the console 100 facing away from the installation box 200 is provided with a cut edge, thereby providing a slope on the side of the console 100 facing away from the installation box 200. And the control panel is provided on the inclined plane to thereby facilitate control of heating of the first container 300 by the nano-heating layer on the heating member 500.
Having described embodiments of the present application, the foregoing description is intended to be exemplary, not exhaustive, and not limited to the disclosed embodiments. Many modifications and variations will be apparent to those of ordinary skill in the art without departing from the scope and spirit of the described embodiments. The terminology used herein is chosen in order to best explain the principles of the embodiments, the practical application, or improvements made to the technology in the marketplace, or to enable others of ordinary skill in the art to understand the embodiments disclosed herein.

Claims (9)

1. A distillation device is characterized by comprising a control console, an installation box, a first container and a second container;
the top of the mounting box is fixedly provided with a heating element, the top of the heating element is provided with a nano heating layer, the first container is placed on the nano heating layer, and the nano heating layer is used for heating materials in the first container;
a condensation pipe is arranged on the first container and is communicated with the first container;
a circulating device is arranged in the installation box and communicated with the condensing pipe so as to enable condensed water to circulate in the condensing pipe;
the control console is fixed on the side of the installation box, a controller is arranged in the control console, and the controller is electrically connected with the heating element and used for controlling the heating element to heat;
the second container is placed on the top table surface of the console, and a water inlet of the second container is communicated with a water outlet of the condensation pipe;
the top of the heating element is provided with a groove for placing the first container, and the groove is hemispherical;
the structure of nanometer zone of heating with the top structure phase-match of heating member.
2. A distilling apparatus according to claim 1, wherein the heating member is provided in two or more, and the two or more heating members are arranged in sequence on the top of the installation case;
the number of the first containers is matched with that of the heating elements, and the first containers are placed on the nano heating layers of the heating elements in a one-to-one correspondence manner;
the number of the condensing pipes is matched with that of the first containers, and the condensing pipes are communicated with the first containers in a one-to-one correspondence manner;
the number of the second containers is matched with that of the condensation pipes, and the second containers are arranged in one-to-one correspondence with the condensation pipes.
3. A distilling apparatus according to claim 2, wherein the two heating members are arranged in a line, and the circulating apparatus is provided with a first water outlet and a first water inlet;
a first water outlet pipeline is arranged at the first water outlet, a first water inlet pipeline is arranged at the first water inlet, and the first water outlet pipeline and the first water inlet pipeline both extend out of the installation box;
the bottom of each condensing pipe is provided with a circulating water inlet, and the top of each condensing pipe is provided with a circulating water outlet;
the first water outlet pipe is communicated with a circulating water inlet of the condenser pipe at one end, and the first water inlet pipe is communicated with a circulating water outlet of the condenser pipe at the other end;
and the circulating water inlet and the circulating water outlet of the adjacent condensation pipe are communicated.
4. The distillation apparatus as claimed in claim 1, wherein the mounting box further comprises a first holding frame disposed beside the heating member for holding the first container.
5. Distillation apparatus according to claim 4, wherein the first holder comprises a support bar, a clamp and an adjustment knob;
the supporting rod is vertically fixed at the top of the installation box and is positioned beside the heating element;
the clamp comprises a clamping jaw and a connecting column, a through hole is formed in the side wall of the connecting column and matched with the supporting rod, the clamping jaw is fixedly installed at one end of the connecting column, and the clamping jaw is used for clamping the first container;
the other end of the connecting column is provided with a threaded hole which is communicated with the through hole;
and a screw rod is arranged at one end of the adjusting knob and is matched with the threaded hole.
6. The distillation apparatus of claim 1, further comprising a second holder;
the second clamping frame is fixedly installed on one side, facing the console, of the installation box and used for clamping the bottom of the condensation pipe.
7. The distillation apparatus according to claim 6, wherein the second holder comprises a fixed portion, a movable engaging portion and a fixed engaging portion;
the fixing part is plate-shaped, and one end of the fixing part is fixedly connected with the installation box;
the fixed clamping part and the movable clamping part are both in omega-shaped structures matched with the tube body of the condensation tube, the movable clamping part and the fixed clamping part are detachably connected, and the opening of the movable clamping part and the opening of the fixed clamping part are oppositely arranged;
and one side of the fixed clamping part, which is not connected with the movable clamping part, is fixedly connected with the fixed part.
8. Distillation apparatus according to any one of claims 1 to 7, wherein the condenser tube is located directly above the water inlet of the second vessel;
the water outlet of the condensation pipe is arranged downwards, a water outlet pipe is arranged at the water outlet of the condensation pipe, and the water inlet of the second container is penetrated through by the water outlet pipe and extends into the second container.
9. Distillation apparatus according to any one of claims 1 to 7, wherein the console and the mounting box are connected in an "L" shape;
the height of the control console is smaller than that of the installation box.
CN202121644369.8U 2021-07-19 2021-07-19 Distillation apparatus Active CN216137259U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202121644369.8U CN216137259U (en) 2021-07-19 2021-07-19 Distillation apparatus

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202121644369.8U CN216137259U (en) 2021-07-19 2021-07-19 Distillation apparatus

Publications (1)

Publication Number Publication Date
CN216137259U true CN216137259U (en) 2022-03-29

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN202121644369.8U Active CN216137259U (en) 2021-07-19 2021-07-19 Distillation apparatus

Country Status (1)

Country Link
CN (1) CN216137259U (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115770408A (en) * 2023-01-05 2023-03-10 广东海洋大学 Novel multi-functional compound distillation device

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115770408A (en) * 2023-01-05 2023-03-10 广东海洋大学 Novel multi-functional compound distillation device
CN115770408B (en) * 2023-01-05 2023-05-23 广东海洋大学 Novel multi-functional compound distillation device

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Effective date of registration: 20240220

Address after: 516000, 4th floor, No.3 Tan Gong South Road (Building 3), Dayawan West District, Huizhou City, Guangdong Province

Patentee after: Huizhou Huaboke Micro Semiconductor Equipment Co.,Ltd.

Country or region after: China

Address before: 518000 Room 518, floor 5, okwei building, No. 23, yantian'ao, Yantian street, Yantian District, Shenzhen, Guangdong (No. 447, Donghai Road West)

Patentee before: SHENZHEN BODAJING TECHNOLOGY INDUSTRY CO.,LTD.

Country or region before: China