CN216093658U

CN216093658U - Integrated preparation facilities of wave-absorbing multifunctional material of light heat conduction

Info

Publication number: CN216093658U
Application number: CN202122338071.0U
Authority: CN
Inventors: 何建忠; 李颖; 曹亚萍; 杨旭林; 徐伟; 余建华
Original assignee: Wuxi Jiade Composite Material Co ltd
Current assignee: Wuxi Jiade Composite Material Co ltd
Priority date: 2021-09-26
Filing date: 2021-09-26
Publication date: 2022-03-22
Anticipated expiration: 2031-09-26

Abstract

The utility model discloses an integrated preparation device of a light heat-conducting wave-absorbing multifunctional material, which comprises a reaction cylinder, wherein a fixing frame is arranged on the outer side of the reaction cylinder, a reaction chamber is arranged in the reaction cylinder, a drying chamber is arranged below the reaction chamber, the lower end of the reaction chamber is connected with an electromagnetic valve, a heating coil is arranged in the inner wall of the reaction chamber, and a sealing cover is arranged on the upper side of the reaction chamber; the inner wall of the drying chamber is provided with an atomizing nozzle, and the drying chamber is internally provided with a filter screen. The bayonet mounting bracket is installed to filter screen week side, the thread groove has been seted up on the outer wall of drying chamber bottom, and the drying cylinder is installed to the drying chamber bottom. The method is simple to operate and low in cost, and the iron-nickel alloy graphene composite material prepared by one step through the thermal decomposition method is good in wave absorbing performance. Can accelerate the reaction efficiency in the reaction chamber of liquid medicine through the design (mixing) shaft to the filter screen that filters impurity can be changed, has improved reaction purity, and the drying cylinder can demolish, conveniently collects the material that forms.

Description

Integrated preparation facilities of wave-absorbing multifunctional material of light heat conduction

Technical Field

The utility model relates to the technical field of nano material production equipment, in particular to an integrated preparation device of a light heat-conducting wave-absorbing multifunctional material.

Background

Graphene is a single-layer sheet-like structure material composed of carbon atoms, is called as 'black gold', and is the king of new materials, as a novel nano material which is the thinnest, the largest in strength, excellent in wave absorbing performance and the strongest in electric conduction and heat conduction performance and is discovered at present.

With the development of electronic communication technology, the harm of electromagnetic waves in daily life of people is increasingly prominent, so that an electromagnetic wave absorbing material with excellent wave absorbing performance is required. The existing graphene production equipment has the defects of complex process, high cost and harsh reaction conditions for preparing aerogel from the existing graphene, so the utility model provides an integrated preparation device of a light heat-conducting wave-absorbing multifunctional material, and aims to solve the problems in the background art.

SUMMERY OF THE UTILITY MODEL

The utility model aims to provide an integrated preparation device of a light heat-conducting wave-absorbing multifunctional material, which aims to solve the problems in the background art.

In order to achieve the purpose, the utility model provides the following technical scheme:

an integrated preparation device of a light heat-conducting wave-absorbing multifunctional material comprises a reaction cylinder, wherein a fixing frame is arranged on the outer side of the reaction cylinder, a reaction chamber is arranged in the reaction cylinder, a drying chamber is arranged below the reaction chamber, the lower end of the reaction chamber is connected with an electromagnetic valve, a heating coil is arranged in the inner wall of the reaction chamber, and a sealing cover is arranged on the upper side of the reaction chamber;

the inner wall of the drying chamber is provided with an atomizing nozzle, and the drying chamber is internally provided with a filter screen. The bayonet mounting bracket is installed to filter screen week side, the thread groove has been seted up on the outer wall of drying chamber bottom, and the drying cylinder is installed to the drying chamber bottom, the drying cylinder bottom is provided with the heating base.

Preferably: a first motor is arranged in the sealing cover, a stirring shaft is connected to the lower end of the first motor, lifting handles are installed on two sides of the first motor, a first liquid inlet pipe is connected to the left side of the reaction chamber, and an air inlet pipe is arranged on one side of the first liquid inlet pipe.

Preferably: and a second motor is installed in the fixing frame, the lower end of the second motor is connected with a driving toothed shaft, the driving toothed shaft is meshed with the outer wall of the drying cylinder, and the drying cylinder is in threaded connection with the outer wall of the drying chamber through a threaded groove.

Preferably: and a liquid inlet pipe II is installed on one side of the outer wall of the drying chamber and is connected with the atomizing spray head.

Preferably: the drying cylinder is characterized in that a limiting groove is formed in the bottom side of the drying cylinder, a sliding groove is formed in the bottom of the fixing frame, a push-pull plate is arranged in the sliding groove, a limiting block is mounted on the push-pull plate, and the push-pull plate is meshed and clamped with the limiting groove through the limiting block.

Preferably: connecting blocks are installed at two ends of the plug-in mounting rack, and the plug-in mounting rack is connected with the outer wall of the drying chamber through the connecting blocks.

Compared with the prior art, the utility model has the beneficial effects that:

1. the method is simple to operate and low in cost, and the iron-nickel alloy graphene composite material prepared by one step through the thermal decomposition method is good in wave absorbing performance.

2. Can accelerate the reaction efficiency in the reaction chamber of liquid medicine through the design (mixing) shaft to the filter screen that filters impurity can be changed, has improved reaction purity, and the drying cylinder can demolish, conveniently collects the material that forms.

Drawings

Fig. 1 is a three-dimensional structure diagram of an integrated preparation apparatus for a light heat-conducting wave-absorbing multifunctional material provided in an embodiment of the present application.

Fig. 2 is a schematic structural diagram of a reaction cylinder in an integrated preparation apparatus for a light heat-conducting wave-absorbing multifunctional material provided in an embodiment of the present application.

Fig. 3 is a sectional structure view of an integrated preparation apparatus for a light heat-conducting wave-absorbing multifunctional material provided in an embodiment of the present application.

Fig. 4 is an explosion structure diagram of an integrated preparation apparatus for a light heat-conducting wave-absorbing multifunctional material provided in an embodiment of the present application.

Fig. 5 is a schematic structural diagram of a drying cylinder in an integrated preparation apparatus for a light heat-conducting wave-absorbing multifunctional material provided in an embodiment of the present application.

In the figure: 1. a reaction cylinder; 2. a fixed mount; 3. a reaction chamber; 4. a drying chamber; 5. an electromagnetic valve; 6. a liquid inlet pipe I; 7. an air inlet pipe; 8. a liquid inlet pipe II; 9. an atomizing spray head; 10. a sealing cover;

11. a first motor; 12. a stirring shaft; 13. lifting the handle; 14. a plug-in mounting bracket; 15. filtering with a screen; 16. connecting blocks; 17. a drying cylinder; 18. heating the base; 19. a heating coil; 20. a drive gear shaft;

21. a second motor; 22. a thread groove; 23. a chute; 24. a push-pull plate; 25. a limiting block; 26. a limiting groove.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

Example 1:

referring to fig. 1 to 5, in the embodiment of the utility model, an integrated preparation apparatus for a light heat-conducting wave-absorbing multifunctional material comprises a reaction cylinder 1, wherein a fixed frame 2 is installed on the outer side of the reaction cylinder 1, a second motor 21 is installed in the fixed frame 2, the lower end of the second motor 21 is connected with a driving gear shaft 20, the driving gear shaft 20 is meshed with the outer wall of a drying cylinder 17, the drying cylinder 17 is in threaded connection with the outer wall of a drying chamber 4 through a thread groove 22, a reaction chamber 3 is arranged in the reaction cylinder 1, the drying chamber 4 is arranged below the reaction chamber 3, the lower end of the reaction chamber 3 is connected with an electromagnetic valve 5, a heating coil 19 is installed in the inner wall of the reaction chamber 3, and a sealing cover 10 is arranged on the upper side of the reaction chamber 3;

a first motor 11 is arranged in the sealing cover 10, the lower end of the first motor 11 is connected with a stirring shaft 12, lifting handles 13 are arranged on two sides of the first motor 11, a first liquid inlet pipe 6 is connected to the left side of the reaction chamber 3, an air inlet pipe 7 is arranged on one side of the first liquid inlet pipe 6, a second liquid inlet pipe 8 is arranged on one side of the outer wall of the drying chamber 4, and the second liquid inlet pipe 8 is connected with an atomizing nozzle 9;

and an atomizing nozzle 9 is arranged on the inner wall of the drying chamber 4, and a filter screen 15 is arranged in the drying chamber 4. An insertion type mounting frame 14 is mounted on the periphery of the filter screen 15, a thread groove 22 is formed in the outer wall of the bottom of the drying chamber 4, a drying cylinder 17 is mounted at the bottom of the drying chamber 4, a heating base 18 is arranged at the bottom of the drying cylinder 17, a limiting groove 26 is formed in the bottom side of the drying cylinder 17, a sliding groove 23 is formed in the bottom of the fixing frame 2, a push-pull plate 24 is arranged in the sliding groove, a limiting block 25 is mounted on the push-pull plate 24, and the push-pull plate 24 is meshed and clamped with the limiting groove 26 through the limiting block 25;

as shown in the figure, a reaction solution is injected into a reaction chamber 3 through a first liquid inlet pipe 6, the reaction solution is heated through a heating coil 19 in the inner wall, reaction gas is injected into the reaction chamber 3 through an air inlet pipe 7, the solution is stirred through a stirring shaft 12 to accelerate the reaction efficiency, the solution which is subjected to primary reaction enters a drying chamber 4 through an opened electromagnetic valve 5, meanwhile, a second liquid inlet pipe 8 is matched with an atomizing nozzle 9 to spray a second round of reaction liquid medicine and is filtered through a filter screen 15, the solution which is subjected to primary reaction is subjected to secondary reaction, the solution after the secondary reaction falls into a drying cylinder 17, and the solution in the drying cylinder 17 leaves a finally formed graphene material along with the baking of a heating base 18;

and the drying cylinder 17 is in threaded connection with the reaction cylinder 1, the two motors 21 and the two driving gear shafts 20 drive the drying cylinder to rotate and move up and down, the automatic disassembly effect is achieved, the molded material is convenient to take, a limiting groove 26 is formed in the lower side of the drying cylinder 17, the limiting groove 26 is clamped with a limiting block 25 on a push-pull plate 24 after the drying cylinder 17 is separated from the reaction cylinder 1, and the drying cylinder 17 can be pulled out through the push-pull plate 24.

Example 2:

in the embodiment of the present invention, this embodiment is further improved as the previous embodiment, and specifically, the difference is that connecting blocks 16 are installed at two ends of the plug-in mounting bracket 14, and the plug-in mounting bracket 14 is connected with the outer wall of the drying chamber 4 through the connecting blocks 16;

connecting blocks 16 are arranged at two ends of the plug-in mounting rack 14, and the connecting blocks 16 can be in threaded connection with the connecting blocks 16 on the outer wall of the reaction cylinder 1 and the threaded rods, so that the purposes of good sealing performance and detachability are achieved.

The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and equivalent alternatives or modifications according to the technical solution of the present invention and the inventive concept thereof should be covered by the scope of the present invention.

Claims

1. An integrated preparation device of a light heat-conducting wave-absorbing multifunctional material comprises a reaction cylinder (1), wherein a fixing frame (2) is installed on the outer side of the reaction cylinder (1), and is characterized in that a reaction chamber (3) is arranged in the reaction cylinder (1), a drying chamber (4) is arranged below the reaction chamber (3), the lower end of the reaction chamber (3) is connected with an electromagnetic valve (5), a heating coil (19) is installed in the inner wall of the reaction chamber (3), and a sealing cover (10) is arranged on the upper side of the reaction chamber (3);

be provided with atomizer (9) on drying chamber (4) inner wall, be provided with filter screen (15) in drying chamber (4), bayonet mounting bracket (14) are installed to filter screen (15) week side, thread groove (22) have been seted up on drying chamber (4) bottom outer wall, and drying cylinder (17) are installed to drying chamber (4) bottom, drying cylinder (17) bottom is provided with heating base (18).

2. The integrated preparation device of the light heat-conducting wave-absorbing multifunctional material as claimed in claim 1, wherein a first motor (11) is arranged in the sealing cover (10), a stirring shaft (12) is connected to the lower end of the first motor (11), lifting handles (13) are installed on two sides of the first motor (11), a first liquid inlet pipe (6) is connected to the left side of the reaction chamber (3), and an air inlet pipe (7) is arranged on one side of the first liquid inlet pipe (6).

3. The integrated preparation device of the light heat-conducting wave-absorbing multifunctional material according to claim 1, characterized in that a second motor (21) is installed in the fixing frame (2), a driving gear shaft (20) is connected to the lower end of the second motor (21), the driving gear shaft (20) is meshed with the outer wall of the drying cylinder (17), and the drying cylinder (17) is in threaded connection with the outer wall of the drying chamber (4) through a threaded groove (22).

4. The integrated preparation device of the light heat-conducting wave-absorbing multifunctional material according to claim 1, wherein a second liquid inlet pipe (8) is installed on one side of the outer wall of the drying chamber (4), and the second liquid inlet pipe (8) is connected with an atomizing nozzle (9).

5. The integrated preparation device of the light heat-conducting wave-absorbing multifunctional material according to claim 1, wherein a limiting groove (26) is formed in the bottom side of the drying cylinder (17), a sliding groove (23) is formed in the bottom of the fixing frame (2), a push-pull plate (24) is arranged in the sliding groove, a limiting block (25) is mounted on the push-pull plate (24), and the push-pull plate (24) is engaged and clamped with the limiting groove (26) through the limiting block (25).

6. The integrated preparation device of a light heat-conducting wave-absorbing multifunctional material according to claim 1, wherein two ends of the plug-in mounting rack (14) are provided with connecting blocks (16), and the plug-in mounting rack (14) is connected with the outer wall of the drying chamber (4) through the connecting blocks (16).