CN215930180U - A n-butanol recovery unit for neutral dye is synthetic - Google Patents

A n-butanol recovery unit for neutral dye is synthetic Download PDF

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Publication number
CN215930180U
CN215930180U CN202122022904.2U CN202122022904U CN215930180U CN 215930180 U CN215930180 U CN 215930180U CN 202122022904 U CN202122022904 U CN 202122022904U CN 215930180 U CN215930180 U CN 215930180U
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fixedly connected
box
pipe
communicated
inner cavity
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CN202122022904.2U
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于文静
李昂
徐斌
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Abstract

The utility model discloses a n-butanol recovery device for neutral dye synthesis, which comprises a base, wherein the left side of the top of the base is fixedly connected with a box body, the bottom of an inner cavity of the box body is fixedly connected with a heating plate, a heat conducting plate is fixedly connected between two sides of the inner cavity of the box body, the top of the box body is fixedly connected with an equipment shell, and the top of the equipment shell is fixedly connected with a motor. The utility model solves the problems of poor cooling effect and low recovery efficiency of the conventional n-butyl alcohol recovery device for synthesizing neutral dye by arranging the sealing plate, the condensing plate, the partition plate, the conveying pipe, the liquid storage box, the first valve, the second valve, the cooling shell, the first bevel gear, the rotating shaft, the second bevel gear, the filtering plate, the second water pump, the cooling pipe, the air inlet pipe and the semiconductor refrigerator.

Description

A n-butanol recovery unit for neutral dye is synthetic
Technical Field
The utility model relates to the technical field of n-butyl alcohol recovery, in particular to a n-butyl alcohol recovery device for neutral dye synthesis.
Background
Butanol is a colorless liquid, has wine flavor, is mainly used for manufacturing n-butyl ester plasticizers of phthalic acid, aliphatic dibasic acid and phosphoric acid, and is widely used in various plastic and rubber products, and is also a raw material for preparing butyraldehyde, butyric acid, butylamine, butyl lactate and the like in organic synthesis.
SUMMERY OF THE UTILITY MODEL
The utility model aims to provide a n-butanol recovery device for neutral dye synthesis, which has the advantages of good cooling effect and high recovery efficiency and solves the problems of poor cooling effect and low recovery efficiency of the conventional n-butanol recovery device for neutral dye synthesis.
In order to achieve the purpose, the utility model provides the following technical scheme: the n-butanol recovery device comprises a base, a left fixedly connected box body at the top of the base, a heating plate fixedly connected to the bottom of an inner cavity of the box body, a heat conducting plate fixedly connected between two sides of the inner cavity of the box body, an equipment shell fixedly connected to the top of the box body, a motor fixedly connected to the top of the equipment shell, a rotary rod fixedly connected to the bottom of the output end of the motor, a first gear sleeved on the surface of the rotary rod and positioned in the inner cavity of the equipment shell, a second gear arranged on two sides of the first gear, a stirring rod fixedly connected to the bottom of the second gear, an inner cavity of the box body penetrated by the bottom of the stirring rod, one side opposite to the two second gears engaged with the first gear, a solvent tank fixedly connected to the left of the box body, the bottom of the solvent box is fixedly connected with a first water pump, a water inlet at the top of the first water pump is communicated with the solvent box, a water outlet at the right side of the first water pump is communicated with the box body, the right side of the top of the base is fixedly connected with a separation box, the left side of the separation box is communicated with the box body, a sealing plate is fixedly connected at the top between two sides of an inner cavity of the separation box, a condensing plate is arranged at the top of the sealing plate, the bottom of the condensing plate penetrates to the bottom of the sealing plate, a partition plate is fixedly connected at the bottom between two sides of the inner cavity of the separation box, the bottom of the partition plate is communicated with a conveying pipe, a liquid storage box is arranged at the bottom of the inner cavity of the separation box, the top of the liquid storage box is communicated with the conveying pipe, the right end of the conveying pipe penetrates to the outer side of the separation box and is sleeved with a first valve, a second valve is sleeved on the left side of the surface of the conveying pipe, and a cooling shell is fixedly connected with the top of the separation box, the top of the output end of the motor penetrates through the inner cavity of the cooling shell and is fixedly connected with a first bevel gear, the left side of the inner cavity of the cooling shell is movably connected with a rotating shaft, the surface of the rotating shaft is sleeved with a second bevel gear, the bottom of the second bevel gear is meshed with the first bevel gear, the right side of the surface of the rotating shaft is sleeved with a filter plate, the top and the bottom of the filter plate are fixedly connected with the inner wall of the cooling shell, the right side of the rotating shaft is fixedly connected with fan blades, the bottom of the cooling shell is fixedly connected with a second water pump, a water inlet on the right side of the second water pump is communicated with the separation box, the top of the second water pump is communicated with a cooling pipe, one end, away from the second water pump, of the cooling pipe penetrates through the inner cavity of the cooling shell, one end, away from the second water pump, of the cooling pipe penetrates through the cooling shell and is communicated with the separation box, and the left side of the top of the cooling shell is communicated with an air inlet pipe, and a semiconductor refrigerator is arranged at the top of the cooling shell and positioned on the right side of the air inlet pipe, and the bottom of the semiconductor refrigerator penetrates through the inner cavity of the cooling shell.
Preferably, the left side intercommunication of heat-conducting plate bottom has the blow off pipe, and the surface cover of blow off pipe is equipped with the third valve, and the one end that the heat-conducting plate was kept away from to the blow off pipe runs through to the outside of box, the top intercommunication of solvent case has notes material pipe, the left bottom fixedly connected with controller of box.
Preferably, the bottom and the heat-conducting plate swing joint of rotary rod, the junction of the surface of puddler and box is through first bearing swing joint, the both sides of rotary rod and the equal fixedly connected with hybrid pole of inner chamber that is located the box.
Preferably, the left side of baffle top fixedly connected with guide plate, the surface of rotation axis passes through second bearing swing joint with the junction of filter.
Preferably, the top on the right side of the separation box is communicated with a gas storage tank, the bottom of the gas storage tank is communicated with a gas supply pipe, one end, far away from the gas storage tank, of the gas supply pipe is communicated with the separation box, and the right side of the separation box is communicated with an exhaust pipe.
Preferably, the right side of the air storage tank is fixedly connected with a fan, an air inlet at the top of the fan is communicated with the air storage tank, and an air outlet at the bottom of the fan is communicated with the separation box through a guide pipe.
Compared with the prior art, the utility model has the following beneficial effects:
1. the utility model solves the problems of poor cooling effect and low recovery efficiency of the conventional n-butyl alcohol recovery device for synthesizing neutral dye by arranging the sealing plate, the condensing plate, the partition plate, the conveying pipe, the liquid storage box, the first valve, the second valve, the cooling shell, the first bevel gear, the rotating shaft, the second bevel gear, the filtering plate, the second water pump, the cooling pipe, the air inlet pipe and the semiconductor refrigerator.
2. According to the utility model, the heating plate is arranged and can be matched with the heat conduction plate to heat the recovered liquid, the rotating rod is arranged and can be matched with the motor and the first gear to drive the second gear and the stirring rod to rotate, the first water pump is arranged and can be used for conveying the separated solution in the solvent box to the inner cavity of the box body, the condensing plate is arranged and can be used for facilitating rapid condensation of steam, the rotating shaft is arranged and can be matched with the first bevel gear and the second bevel gear to drive the fan blades to rotate, the semiconductor refrigerator is arranged and can be used for reducing the temperature of air entering the cooling shell, and the gas storage tank and the gas supply pipe are arranged and can be matched with the fan to circulate steam for secondary condensation.
Drawings
FIG. 1 is a schematic structural view of the present invention;
FIG. 2 is a front view of the structure of the present invention;
FIG. 3 is an enlarged view of a portion of FIG. 1.
In the figure: 1. a base; 2. a box body; 3. heating plates; 4. a heat conducting plate; 5. an equipment housing; 6. a motor; 7. rotating the rod; 8. a first gear; 9. a second gear; 10. a stirring rod; 11. a solvent tank; 12. a first water pump; 13. a separation tank; 14. a sealing plate; 15. a condensing plate; 16. a partition plate; 17. a delivery pipe; 18. a liquid storage tank; 19. a first valve; 20. a second valve; 21. cooling the shell; 22. a first bevel gear; 23. a rotating shaft; 24. a second bevel gear; 25. a filter plate; 26. a fan blade; 27. a second water pump; 28. a cooling tube; 29. an air inlet pipe; 30. a semiconductor refrigerator; 31. a gas storage tank; 32. an air supply pipe; 33. a fan.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
In the description of the present invention, it should be noted that the terms "upper", "lower", "inner", "outer", "front", "rear", "both ends", "one end", "the other end", and the like indicate orientations or positional relationships based on the orientations or positional relationships shown in the drawings, and are only for convenience of describing the present invention and simplifying the description, but do not indicate or imply that the referred device or element must have a specific orientation, be constructed in a specific orientation, and be operated, and thus, should not be construed as limiting the present invention. Furthermore, the terms "first" and "second" are used for descriptive purposes only and are not to be construed as indicating or implying relative importance.
In the description of the present invention, it is to be noted that, unless otherwise explicitly specified or limited, the terms "mounted", "provided", "connected", and the like are to be construed broadly, such as "connected", which may be fixedly connected, detachably connected, or integrally connected; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meanings of the above terms in the present invention can be understood in specific cases to those skilled in the art.
Referring to fig. 1-3, a n-butanol recovery device for neutral dye synthesis comprises a base 1, a box 2 is fixedly connected to the left side of the top of the base 1, a heating plate 3 is fixedly connected to the bottom of the inner cavity of the box 2, a heat conducting plate 4 is fixedly connected between the two sides of the inner cavity of the box 2, an equipment housing 5 is fixedly connected to the top of the box 2, a motor 6 is fixedly connected to the top of the equipment housing 5, a rotary rod 7 is fixedly connected to the bottom of the output end of the motor 6, the bottom of the rotary rod 7 penetrates through the inner cavity of the box 2, a first gear 8 is sleeved on the surface of the rotary rod 7 and positioned in the inner cavity of the equipment housing 5, second gears 9 are respectively arranged on the two sides of the first gear 8, a stirring rod 10 is fixedly connected to the bottom of the second gear 9, the bottom of the stirring rod 10 penetrates through the inner cavity of the box 2, and one sides opposite to the two second gears 9 are respectively engaged with the first gear 8, a solvent box 11 is fixedly connected to the left side of the box body 2, a first water pump 12 is fixedly connected to the bottom of the solvent box 11, a water inlet at the top of the first water pump 12 is communicated with the solvent box 11, a water outlet at the right side of the first water pump 12 is communicated with the box body 2, a separation box 13 is fixedly connected to the right side of the top of the base 1, the left side of the separation box 13 is communicated with the box body 2, a sealing plate 14 is fixedly connected to the top between two sides of an inner cavity of the separation box 13, a condensation plate 15 is arranged at the top of the sealing plate 14, the bottom of the condensation plate 15 penetrates to the bottom of the sealing plate 14, a partition plate 16 is fixedly connected to the bottom between two sides of the inner cavity of the separation box 13, the bottom of the partition plate 16 is communicated with a conveying pipe 17, a liquid storage box 18 is arranged at the bottom of the inner cavity of the separation box 13, the top of the liquid storage box 18 is communicated with the conveying pipe 17, the right end of the conveying pipe 17 penetrates to the outer side of the separation box 13 and is sleeved with a first valve 19, a second valve 20 is sleeved on the left side of the surface of the conveying pipe 17, the top of the separation box 13 is fixedly connected with a cooling shell 21, the top of the output end of the motor 6 penetrates through the inner cavity of the cooling shell 21 and is fixedly connected with a first bevel gear 22, the left side of the inner cavity of the cooling shell 21 is movably connected with a rotating shaft 23, the surface of the rotating shaft 23 is sleeved with a second bevel gear 24, the bottom of the second bevel gear 24 is meshed with the first bevel gear 22, the right side of the surface of the rotating shaft 23 is sleeved with a filter plate 25, the top and the bottom of the filter plate 25 are fixedly connected with the inner wall of the cooling shell 21, the right side of the rotating shaft 23 is fixedly connected with fan blades 26, the bottom of the cooling shell 21 is fixedly connected with a second water pump 27, a water inlet on the right side of the second water pump 27 is communicated with the separation box 13, the top of the second water pump 27 is communicated with a cooling pipe 28, one end, far away from the second water pump 27, of the cooling pipe 28 penetrates through the inner cavity of the cooling shell 21 and is communicated with the separation box 13, the left side of the top of the cooling shell 21 is communicated with an air inlet pipe 29, the top of the cooling shell 21 and the right side of the air inlet pipe 29 are provided with a semiconductor refrigerator 30, the bottom of the semiconductor refrigerator 30 penetrates into the inner cavity of the cooling shell 21, the left side of the bottom of the heat conducting plate 4 is communicated with a sewage discharge pipe, the surface of the sewage discharge pipe is sleeved with a third valve, one end of the sewage discharge pipe, far away from the heat conducting plate 4, penetrates into the outer side of the box body 2, the top of the solvent box 11 is communicated with a material injection pipe, the left side of the box body 2 is fixedly connected with a controller, the bottom of the rotating rod 7 is movably connected with the heat conducting plate 4, the joint of the surface of the stirring rod 10 and the box body 2 is movably connected through a first bearing, the inner cavities on the two sides of the rotating rod 7 and positioned in the box body 2 are fixedly connected with a mixing rod, the left side of the top of the partition plate 16 is fixedly connected with a guide plate, the joint of the surface of the rotating shaft 23 and the filter plate 25 is movably connected through a second bearing, the top of the right side of the separation box 13 is communicated with an air storage tank 31, the bottom of the air storage tank 31 is communicated with an air delivery pipe 32, one end of the air delivery pipe 32, which is far away from the air storage tank 31, is communicated with the separation box 13, the right side of the separation box 13 is communicated with an exhaust pipe, the right side of the air storage tank 31 is fixedly connected with a fan 33, an air inlet at the top of the fan 33 is communicated with the air storage tank 31, an air outlet at the bottom of the fan 33 is communicated with the separation box 13 through a guide pipe, a recovered liquid can be heated by being matched with a heat conduction plate 4 through arranging a heating plate 3, a second gear 9 and a stirring rod 10 can be driven to rotate by being matched with a motor 6 and a first gear 8 through arranging a rotating rod 7, a separated solution in a solvent box 11 can be conveyed to an inner cavity of a box body 2 through arranging a first water pump 12, rapid condensation of steam can be facilitated by arranging a condensation plate 15, and a rotating shaft 23 can be matched with a first bevel gear 22 and a second bevel gear 24 to drive a fan blade 26 to rotate, through setting up semiconductor cooler 30, can reduce the temperature that gets into the air in the cooling shell 21, through setting up gas holder 31 and air feed pipe 32, can cooperate the circulation steam recondensation with fan 33, through setting up sealing plate 14, condensation plate 15, baffle 16, conveyer pipe 17, deposit liquid case 18, first valve 19, second valve 20, cooling shell 21, first bevel gear 22, rotation axis 23, second bevel gear 24, filter 25, second water pump 27, cooling tube 28, air-supply line 29 and semiconductor cooler 30, the problem that the current n-butanol recovery unit for the synthesis of neutral dye is poor in cooling effect, recovery efficiency is low has been solved, this n-butanol recovery unit for the synthesis of neutral dye possesses the advantage that the cooling effect is good, recovery efficiency is high, is worth promoting.
When the device is used, a solution to be recovered is conveyed to the box body 2, the heating plate 3, the motor 6 and the first water pump 12 are started, the first water pump 12 conveys a separation solution in the solvent box 11 to the inside of the box body 2, the motor 6 is matched with the rotating rod 7 to drive the first gear 8 to rotate, the first gear 8 is matched with the second gear 9 to drive the stirring rod 10 to rotate, the stirring rod 10 stirs the solution, meanwhile, the heating plate 3 is matched with the heat conducting plate 4 to heat the solution, the inside of the box body 2 is heated to the boiling point of water through the controller, water vapor enters the separation box 13, the steam is matched with the condensing plate 15 to generate condensed water, the first valve 19 is started, the condensed water is discharged through the conveying pipe 17, the second water pump 27 is started, the second water pump 27 is matched with the cooling pipe 28 to circulate the cooling liquid in the separation box 13, and simultaneously, the motor 6 is matched with the first bevel gear 22 to drive the second bevel gear 24 and the rotating shaft 23 to rotate, rotation shaft 23 rotates and drives flabellum 26 and rotates, the cooperation through semiconductor cooler 30 will inhale the air temperature in the cooling shell 21 and reduce fast, flabellum 26 blows off the cooling air to cooling tube 28 and accelerates its heat dissipation and increase the result of use of condensation plate 15, make the inside boiling point of box 2 heat to the n-butyl alcohol through controller control hot plate 3 afterwards, make its evaporation form steam, after n-butyl alcohol steam gets into separator box 13, open second valve 20 and close first valve 19, condensation plate 15 condenses the n-butyl alcohol steam, and carry through conveyer pipe 17 and collect to depositing in the liquid case 18.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the utility model, the scope of which is defined in the appended claims and their equivalents.

Claims (6)

1. The utility model provides a n-butanol recovery unit for neutral dye is synthetic, includes base (1), its characterized in that: the heating device is characterized in that a box body (2) is fixedly connected to the left side of the top of a base (1), a heating plate (3) is fixedly connected to the bottom of an inner cavity of the box body (2), a heat conducting plate (4) is fixedly connected between two sides of the inner cavity of the box body (2), an equipment shell (5) is fixedly connected to the top of the box body (2), a motor (6) is fixedly connected to the top of the equipment shell (5), a rotary rod (7) is fixedly connected to the bottom of the output end of the motor (6), the bottom of the rotary rod (7) penetrates through the inner cavity of the box body (2), a first gear (8) is sleeved on the surface of the rotary rod (7) and positioned in the inner cavity of the equipment shell (5), second gears (9) are arranged on two sides of the first gear (8), stirring rods (10) are fixedly connected to the bottom of the second gears (9), and the bottom of the stirring rods (10) penetrates through the inner cavity of the box body (2), one side, opposite to the two second gears (9), of each of the two second gears is meshed with the corresponding first gear (8), the left side of the box body (2) is fixedly connected with a solvent box (11), the bottom of the solvent box (11) is fixedly connected with a first water pump (12), a water inlet in the top of the first water pump (12) is communicated with the solvent box (11), a water outlet in the right side of the first water pump (12) is communicated with the box body (2), the right side of the top of the base (1) is fixedly connected with a separation box (13), the left side of the separation box (13) is communicated with the box body (2), a sealing plate (14) is fixedly connected to the top between the two sides of an inner cavity of the separation box (13), a condensation plate (15) is arranged on the top of the sealing plate (14), the bottom of the condensation plate (15) penetrates through to the bottom of the sealing plate (14), and a partition plate (16) is fixedly connected to the bottom between the two sides of the inner cavity of the separation box (13), the bottom of the partition plate (16) is communicated with a conveying pipe (17), a liquid storage box (18) is arranged at the bottom of an inner cavity of the separation box (13), the top of the liquid storage box (18) is communicated with the conveying pipe (17), the right end of the conveying pipe (17) penetrates through the outer side of the separation box (13) and is sleeved with a first valve (19), a second valve (20) is sleeved on the left side of the surface of the conveying pipe (17), a cooling shell (21) is fixedly connected to the top of the separation box (13), the top of an output end of the motor (6) penetrates through the inner cavity of the cooling shell (21) and is fixedly connected with a first bevel gear (22), a rotating shaft (23) is movably connected to the left side of the inner cavity of the cooling shell (21), a second bevel gear (24) is sleeved on the surface of the rotating shaft (23), and the bottom of the second bevel gear (24) is meshed with the first bevel gear (22), the right side of the surface of the rotating shaft (23) is sleeved with a filter plate (25), the top and the bottom of the filter plate (25) are fixedly connected with the inner wall of the cooling shell (21), the right side of the rotating shaft (23) is fixedly connected with fan blades (26), the bottom of the cooling shell (21) is fixedly connected with a second water pump (27), a water inlet on the right side of the second water pump (27) is communicated with the separation box (13), the top of the second water pump (27) is communicated with a cooling pipe (28), one end, far away from the second water pump (27), of the cooling pipe (28) penetrates through the inner cavity of the cooling shell (21), one end, far away from the second water pump (27), of the cooling pipe (28) penetrates through the cooling shell (21) and is communicated with the separation box (13), the left side of the top of the cooling shell (21) is communicated with an air inlet pipe (29), the right side, positioned on the air inlet pipe (29), of the top of the cooling shell (21) is provided with a semiconductor refrigerator (30), the bottom of the semiconductor refrigerator (30) penetrates into the inner cavity of the cooling shell (21).
2. The device for recovering n-butanol used for the synthesis of neutral dyes according to claim 1, characterized in that: the left side intercommunication of heat-conducting plate (4) bottom has the blow off pipe, and the surface cover of blow off pipe is equipped with the third valve, and the one end that heat-conducting plate (4) were kept away from to the blow off pipe runs through to the outside of box (2), the top intercommunication of solvent case (11) has notes material pipe, the left bottom fixedly connected with controller of box (2).
3. The device for recovering n-butanol used for the synthesis of neutral dyes according to claim 1, characterized in that: the bottom and heat-conducting plate (4) swing joint of rotary rod (7), the junction of the surface of puddler (10) and box (2) is through first bearing swing joint, the both sides of rotary rod (7) and the equal fixedly connected with hybrid rod in inner chamber that is located box (2).
4. The device for recovering n-butanol used for the synthesis of neutral dyes according to claim 1, characterized in that: the left side fixedly connected with guide plate at baffle (16) top, the junction through second bearing swing joint of the surface of rotation axis (23) and filter (25).
5. The device for recovering n-butanol used for the synthesis of neutral dyes according to claim 1, characterized in that: the top on the right side of the separation box (13) is communicated with a gas storage tank (31), the bottom of the gas storage tank (31) is communicated with a gas supply pipe (32), one end, away from the gas storage tank (31), of the gas supply pipe (32) is communicated with the separation box (13), and the right side of the separation box (13) is communicated with an exhaust pipe.
6. The device for recovering n-butanol used for the synthesis of neutral dyes according to claim 5, characterized in that: the right side fixedly connected with fan (33) of air holder (31), the air intake and air holder (31) intercommunication at fan (33) top, the air outlet and separator box (13) of fan (33) bottom pass through the pipe intercommunication.
CN202122022904.2U 2021-08-26 2021-08-26 A n-butanol recovery unit for neutral dye is synthetic Expired - Fee Related CN215930180U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202122022904.2U CN215930180U (en) 2021-08-26 2021-08-26 A n-butanol recovery unit for neutral dye is synthetic

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202122022904.2U CN215930180U (en) 2021-08-26 2021-08-26 A n-butanol recovery unit for neutral dye is synthetic

Publications (1)

Publication Number Publication Date
CN215930180U true CN215930180U (en) 2022-03-01

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Application Number Title Priority Date Filing Date
CN202122022904.2U Expired - Fee Related CN215930180U (en) 2021-08-26 2021-08-26 A n-butanol recovery unit for neutral dye is synthetic

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Granted publication date: 20220301