CN215917347U

CN215917347U - High-efficient acidolysis protein reaction unit

Info

Publication number: CN215917347U
Application number: CN202122269081.3U
Authority: CN
Inventors: 韩士群; 陈丙法; 巫佳杰
Original assignee: Jiangsu Academy of Agricultural Sciences
Current assignee: Jiangsu Academy of Agricultural Sciences
Priority date: 2021-09-18
Filing date: 2021-09-18
Publication date: 2022-03-01
Anticipated expiration: 2031-09-18

Abstract

The utility model relates to the technical field of chemical equipment and discloses a high-efficiency acidolysis protein reaction device.A ceramic reaction kettle is placed on a support frame and comprises a top cover and a kettle body, and a liquid collecting part is fixed at the bottom of the kettle body; the top cover is provided with a microwave generator which is communicated with the kettle body through a waveguide tube; the top cover is provided with a feeding hole; a control mechanism, a stirring part and an inductor are arranged in the kettle body, and a steam heating part is arranged at the bottom of the kettle body; the control mechanism comprises a fixed plate fixedly connected to the top cover, a compression rod is connected to the fixed plate, a compression plate is fixedly connected to one end of the compression rod, a control rod is fixedly connected to the compression plate, the bottom of the control rod sequentially penetrates through the fixed plate and the top cover, and a sealing block is connected to one end of the control rod; the utility model controls the liquid to flow out through the control rod, reduces the liquid taking difficulty after the reaction is finished, reduces the reaction cost by adopting ceramic as the material of the ceramic reaction kettle, and reduces the time required by the reaction through the auxiliary device.

Description

High-efficient acidolysis protein reaction unit

Technical Field

The utility model relates to the technical field of chemical equipment, in particular to a high-efficiency acidolysis protein reaction device.

Background

The ceramic reaction kettle is a reaction device, and raw materials complete various reactions in the ceramic reaction kettle to generate new substances or change partial characteristics of the raw materials.

The conventional metal ceramic reaction kettle is not resistant to hydrochloric acid, and the cost is greatly increased if a polytetrafluoroethylene coating is used; in addition, generally, a metal shields microwaves, and a non-metal material is not heat-resistant and pressure-resistant although it can transmit microwaves. And the liquid taking is complex after the reaction of the conventional ceramic reaction kettle is finished, the liquid after the reaction is easy to be polluted, the waste is caused, and the time required by the acidolysis protein reaction of the conventional reaction kettle is too long.

SUMMERY OF THE UTILITY MODEL

The utility model aims to provide a high-efficiency acidolysis protein reaction device to solve the problems in the prior art.

In order to achieve the purpose, the utility model provides the following scheme: the utility model provides a high-efficiency acidolysis protein reaction device, which comprises a support frame, wherein a ceramic reaction kettle is placed on the support frame, the ceramic reaction kettle comprises a top cover and a kettle body, a feeding hole is formed in the top cover, and the bottom of the kettle body is fixedly connected with a liquid collecting part; the top cover is fixedly provided with a microwave generator, the microwave generator is connected with a waveguide tube, and the waveguide tube is communicated with the kettle body; a control mechanism, a stirring part and an inductor are arranged in the kettle body, and a steam heating part is fixedly connected to the bottom of the kettle body;

control mechanism includes buffering portion, buffering portion includes fixed connection and is in fixed plate on the top cap, the fixed plate is located the charge cavity with between the microwave generator, fixedly connected with compression pole on the fixed plate, the compression pole is kept away from the one end fixedly connected with compression board of fixed plate, compression board central point puts the fixedly connected with control lever, the control lever bottom runs through in proper order the fixed plate with the top cap, the control lever is kept away from the sealed piece of one end fixedly connected with of compression board, sealed piece with collection liquid portion corresponds the setting.

Preferably, the support frame is a cross structure, a clamping block is arranged on the outer side of the ceramic reaction kettle, and the support frame is connected with the ceramic reaction kettle in a clamping mode through the clamping block.

Preferably, the liquid collecting part comprises a liquid collecting groove fixedly installed at the bottom of the kettle body, the liquid collecting groove is communicated with the kettle body, a liquid leakage hole is formed in the bottom of the liquid collecting groove, a collecting bottle is fixedly sleeved on the outer side of the liquid collecting groove, the liquid leakage hole is located inside the collecting bottle, and a liquid outlet hole is formed in the bottom of the collecting bottle.

Preferably, the sealing block is slidably connected in the liquid collecting tank, a spring is fixedly connected to the bottom of the sealing block, one end, far away from the sealing block, of the spring is fixedly connected to the bottom of the liquid collecting tank, and the sealing block is in interference fit with the liquid collecting tank.

Preferably, the inside installation cavity that is provided with of control lever, inductor fixed mounting be in the installation cavity, the top fixedly connected with digital display of compression board, digital display with inductor electric connection.

Preferably, the control rod is fixedly sleeved with two gear bearings, the control rod is sleeved with an installation sleeve, the installation sleeve is positioned between the two gear bearings and is fixedly connected with the two gear bearings, and the installation sleeve is fixedly connected with the blades; the top cap bottom fixedly connected with rotates the motor, the output fixedly connected with drive gear of rotating the motor, drive gear with gear bearing meshes mutually.

Preferably, the top cover is provided with a mounting hole, the waveguide tube is communicated with the ceramic reaction kettle through the mounting hole, and a sealing ring is arranged between the waveguide tube and the mounting hole.

Preferably, the ceramic reaction kettle is a ceramic reaction kettle.

Preferably, the kettle body is divided into an inner layer and an outer layer, a heating cavity is formed between the inner layer and the outer layer, a pressure release valve is arranged on the outer layer, and the pressure release valve is communicated with the heating cavity; steam heating portion includes the catch basin, catch basin fixed mounting in heating chamber bottom, the gas pocket is seted up at the catch basin top, the catch basin passes through the gas pocket with heating chamber intercommunication, catch basin bottom fixedly connected with heater.

Preferably, the fixed plate and the compression plate are both rectangular structures, and the compression rods are positioned at four corners of the fixed plate.

The utility model discloses the following technical effects:

according to the utility model, the control rod is used for controlling the liquid after the reaction to directly flow out of the ceramic reaction kettle from the bottom of the ceramic reaction kettle, the liquid taking difficulty after the reaction is reduced, the inductor is arranged in the middle of the control rod, and the temperature and the pressure inside the ceramic reaction kettle are directly and clearly observed through the display electrically connected with the inductor at the top end of the ceramic reaction kettle, so that the influence of the temperature and the pressure on the reaction is avoided.

The time required by the acidolysis reaction is greatly reduced by the auxiliary action of the microwave generator, the steam heating part and the stirring device, so that the reaction time of protein acidolysis is controlled to be about 2 hours.

The ceramic material of the ceramic reaction kettle is adopted, so that the shielding of the metal ceramic reaction kettle on the microwave is avoided, and the cost caused by large-area coating of polytetrafluoroethylene in the ceramic reaction kettle is avoided from being too high.

Drawings

In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings needed to be used in the embodiments will be briefly described below, and it is obvious that the drawings in the following description are only some embodiments of the present invention, and it is obvious for those skilled in the art to obtain other drawings without inventive exercise.

FIG. 1 is a sectional view of a front view of a high efficiency acidolysis protein reaction apparatus according to the present invention;

FIG. 2 is a cross-sectional view taken along line B-B of FIG. 1;

FIG. 3 is an enlarged view at C of FIG. 1;

fig. 4 is an enlarged view of a point a in fig. 1.

The device comprises a support frame-1, a kettle body-2, an inner layer-201, an outer layer-202, a top cover-3, a control rod-4, a heater-5, a water storage tank-6, an inductor-7, an installation sleeve-8, blades-9, a gear bearing-10, a microwave generator-11, a waveguide tube-12, a feed hole-13, a rotating motor-14, a liquid collecting tank-15, a sealing block-16, a collecting bottle-17, a digital display-18, a compression rod-19, a fixing plate-20, a compression plate-21, a clamping block-22 and a pressure release valve-23.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

In order to make the aforementioned objects, features and advantages of the present invention comprehensible, embodiments accompanied with figures are described in further detail below.

The utility model provides a high-efficiency acidolysis protein reaction device, which comprises a support frame 1, wherein a ceramic reaction kettle is placed on the support frame 1, the ceramic reaction kettle comprises a top cover 3 and a kettle body 2, a feeding hole 13 is formed in the top cover 3, and a liquid collecting part is fixedly connected to the bottom of the kettle body 2; a microwave generator 11 is fixedly installed on the top cover 3, a waveguide tube 12 is connected to the microwave generator 11, and the waveguide tube 12 is communicated with the kettle body 2; a control mechanism, a stirring part and an inductor 7 are arranged in the kettle body 2, and a steam heating part is fixedly connected to the bottom of the kettle body 2;

control mechanism includes the buffering portion, the buffering portion includes fixed connection fixed plate 20 on the top cap 3, fixed plate 20 is located charge door 13 with between the microwave generator 11, fixedly connected with compression pole 19 on the fixed plate 20, compression pole 19 is kept away from the one end fixedly connected with compression board 21 of fixed plate 20, compression board 21 central point puts fixedly connected with control lever 4, run through in proper order in control lever 4 bottom fixed plate 20 with top cap 3, control lever 4 is kept away from the one end fixedly connected with seal block 16 of compression board 21, seal block 16 with the corresponding setting of collection liquid portion.

Further, for improving the stability of support frame 1, reduce support frame area, cross structure is chooseed for use to support frame 1, and for reducing the dismouting degree of difficulty, through the 22 joints of fixture block between support frame 1 and the ceramic reaction cauldron simultaneously.

Furthermore, in order to avoid liquid being insufficiently taken after the reaction and leading to liquid still existing in the ceramic reaction kettle, the bottom of the kettle body 2 of the ceramic reaction kettle is convex.

Further, in order to improve the sealing performance of the liquid collecting tank 15, a spring is mounted at the bottom of the sealing block 16, two ends of the spring are fixedly connected with the bottom end of the sealing block and the bottom end of the liquid collecting tank 15 respectively, the liquid collecting tank 15 is sealed through the support of the spring, and liquid leakage caused by downward sliding of the sealing block 16 is avoided; meanwhile, in order to increase the sealing effect of the sealing block 16, the sealing block 16 is in interference fit with the liquid collecting groove 15.

Further, in order to monitor the temperature and pressure inside the ceramic reaction kettle in real time, the ceramic reaction kettle is internally provided with an inductor 7, and the top end of the compression plate is provided with a digital display 18 electrically connected with the inductor 7.

Furthermore, in order to accelerate the reaction speed of protein acidolysis, a stirring device is arranged in the ceramic reaction kettle.

Furthermore, in order to avoid pressure leakage in the ceramic reaction kettle, a sealing ring is arranged between the waveguide tube 12 and the mounting hole, and a sealing plug is arranged on the feed hole of the top cover 3.

Furthermore, in order to improve the heat-resistant and pressure-resistant capability of the reactor on the basis of reducing the material consumption, a ceramic reaction kettle is adopted, and the surfaces of other devices in the ceramic reaction kettle are coated with polytetrafluoroethylene coatings.

Further, in order to further increase the reaction speed, the ceramic reaction kettle is provided with an inner layer 201 and an outer layer 202, and a water storage tank 6 and a heater 5 are arranged at the bottom of a heating cavity formed by the inner layer 201 and the outer layer 202 to provide steam heating.

Further, in order to ensure the smooth operation of the control rod 4, the compression rods 19 are symmetrically and fixedly installed at four corners of the rectangular fixing plate 20.

Example (b): the ceramic reaction kettle provided by the utility model feeds materials into the ceramic reaction kettle through the feeding hole 13, and simultaneously, the compression rod 19 is used for driving the control rod 4 to move up and down, so that the outflow of reaction liquid is controlled, the difficulty of taking the liquid after the reaction of the ceramic reaction kettle is reduced, the reaction speed of the ceramic reaction kettle is improved by arranging the rotating motor 14 to drive the blades 9 to form the stirring device, the steam heating device formed by the heater 5 and the water storage tank 6 and the microwave generating device, the reaction time of acidolysis protein is controlled to be about 2 hours, and the time required by acidolysis reaction is reduced. The real-time monitoring of the pressure and the temperature in the ceramic reaction kettle is ensured by arranging the sensing device in the control rod 4 and installing the digital display 18 which is electrically connected with the control rod 4 on the compression plate 21.

In the description of the present invention, it is to be understood that the terms "longitudinal", "lateral", "upper", "lower", "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outer", and the like, indicate orientations or positional relationships based on those shown in the drawings, are merely for convenience of description of the present invention, and do not indicate or imply that the referenced devices or elements must have a particular orientation, be constructed and operated in a particular orientation, and thus, are not to be construed as limiting the present invention.

The above-described embodiments are merely illustrative of the preferred embodiments of the present invention, and do not limit the scope of the present invention, and various modifications and improvements of the technical solutions of the present invention can be made by those skilled in the art without departing from the spirit of the present invention, and the technical solutions of the present invention are within the scope of the present invention defined by the claims.

Claims

1. The high-efficiency acidolysis protein reaction device is characterized by comprising a support frame (1), wherein a ceramic reaction kettle is placed on the support frame (1), the ceramic reaction kettle comprises a top cover (3) and a kettle body (2), a feeding hole (13) is formed in the top cover (3), and a liquid collecting part is fixedly connected to the bottom of the kettle body (2); the top cover (3) is fixedly provided with a microwave generator (11), the microwave generator (11) is connected with a waveguide tube (12), and the waveguide tube (12) is communicated with the kettle body (2); a control mechanism, a stirring part and an inductor (7) are arranged in the kettle body (2), and a steam heating part is fixedly connected to the bottom of the kettle body (2);

control mechanism includes buffering portion, buffering portion includes fixed plate (20) of fixed connection on top cap (3), fixed plate (20) are located charge door (13) with between microwave generator (11), fixedly connected with compression pole (19) are gone up in fixed plate (20), keep away from compression pole (19) the one end fixedly connected with compression board (21) of fixed plate (20), fixedly connected with control lever (4) are put to compression board (21) center, control lever (4) bottom is run through in proper order fixed plate (20) with top cap (3), control lever (4) are kept away from the one end fixedly connected with seal block (16) of compression board (21), seal block (16) with the corresponding setting of liquid collecting portion.

2. The high efficiency acid hydrolysis protein reaction device as claimed in claim 1, wherein: support frame (1) is the cross structure, the ceramic reaction cauldron outside is provided with fixture block (22), support frame (1) with ceramic reaction cauldron passes through fixture block (22) joint.

3. The high efficiency acid hydrolysis protein reaction device as claimed in claim 1, wherein: liquid collecting part is including fixed mounting in collecting tank (15) of cauldron body (2) bottom, collecting tank (15) with cauldron body (2) intercommunication, the weeping hole has been seted up to collecting tank (15) bottom, the fixed cover in collecting tank (15) outside has connect receiving flask (17), the weeping hole is located inside receiving flask (17), the liquid outlet has been seted up to receiving flask (17) bottom.

4. The high efficiency acid hydrolysis protein reaction device as claimed in claim 3, wherein: sealed piece (16) sliding connection be in collecting tank (15), sealed piece (16) bottom fixedly connected with spring, the spring is kept away from the one end fixed connection of sealed piece (16) is in collecting tank (15) bottom, sealed piece (16) with collecting tank (15) interference fit.

5. The high efficiency acid hydrolysis protein reaction device as claimed in claim 1, wherein: the utility model discloses a compressor, including control lever (4), inductor (7), top fixedly connected with digital display (18) of compression board (21), digital display (18) with inductor (7) electric connection, the inside installation cavity that is provided with of control lever (4), inductor (7) fixed mounting be in the installation cavity, the top fixedly connected with digital display (18) of compression board (21).

6. The high efficiency acid hydrolysis protein reaction device as claimed in claim 1, wherein: the control rod (4) is sleeved with two gear bearings (10), the inner sides of the two gear bearings (10) are fixedly connected with the control rod (4), the control rod (4) is sleeved with an installation sleeve (8), the installation sleeve (8) is positioned between the two gear bearings (10) and is fixedly connected with the two gear bearings (10), and the installation sleeve (8) is fixedly connected with blades (9); top cap (3) bottom fixedly connected with rotates motor (14), the output fixedly connected with drive gear of rotating motor (14), drive gear with gear bearing (10) mesh mutually.

7. The high efficiency acid hydrolysis protein reaction device as claimed in claim 1, wherein: the top cover (3) is provided with a mounting hole, the waveguide tube (12) is communicated with the ceramic reaction kettle through the mounting hole, and a sealing ring is arranged between the waveguide tube (12) and the mounting hole.

8. The high efficiency acid hydrolysis protein reaction device as claimed in claim 1, wherein: the kettle body (2) is divided into an inner layer (201) and an outer layer (202), a heating cavity is formed between the inner layer (201) and the outer layer (202), a pressure release valve (23) is arranged on the outer layer (202), and the pressure release valve (23) is communicated with the heating cavity; steam heating portion includes catch basin (6), catch basin (6) fixed mounting be in heating chamber bottom, the gas pocket has been seted up at catch basin (6) top, catch basin (6) pass through the gas pocket with the heating chamber intercommunication, catch basin (6) bottom fixedly connected with heater (5).

9. The high efficiency acid hydrolysis protein reaction device as claimed in claim 1, wherein: the fixed plate (20) and the compression plate (21) are both rectangular structures, and the compression rods (19) are positioned at four corners of the fixed plate (20).