CN215783379U - Titanium liquid hydrolysis experimental device - Google Patents
Titanium liquid hydrolysis experimental device Download PDFInfo
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- CN215783379U CN215783379U CN202122460604.2U CN202122460604U CN215783379U CN 215783379 U CN215783379 U CN 215783379U CN 202122460604 U CN202122460604 U CN 202122460604U CN 215783379 U CN215783379 U CN 215783379U
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Abstract
The utility model provides a titanium liquid hydrolysis experimental device which comprises a constant-temperature water bath kettle, a three-neck flask, a first motor, a first shaft lever, a first stirring paddle, a thermometer and a reflux condenser pipe, wherein the lower part of the three-neck flask is positioned in the constant-temperature water bath kettle, three bottle openings of the three-neck flask are respectively provided with a first bottle plug, a second bottle plug and a third bottle plug, a glass bulb of the thermometer penetrates through the first bottle plug and then enters the three-neck flask, the second bottle plug is provided with a condenser pipe port, the lower end of an inner pipe of the reflux condenser pipe is connected with the condenser pipe port, the upper end of the inner pipe of the reflux condenser pipe is sealed, the upper end of the first shaft lever is fixed on a rotating shaft of the first motor, the lower end of the first shaft lever penetrates through the third bottle plug and then enters the three-neck flask, the upper end of the first shaft lever is provided with the first stirring paddle, the first shaft lever is sleeved with a sleeve pipe, and the upper end of the sleeve pipe is fixed on the third bottle. Due to the adoption of the technical scheme, the experimental result can be more accurate.
Description
Technical Field
The utility model belongs to the technical field of experimental equipment, and particularly relates to a titanium liquid hydrolysis experimental device.
Background
The existing titanium liquid hydrolysis experiment device comprises a constant-temperature water bath kettle, a three-neck flask, a motor, a shaft lever and a stirring paddle, wherein the upper end of the shaft lever is connected with a rotating shaft of the motor, the lower end of the shaft lever penetrates through a bottle plug on the three-neck flask to enter the three-neck flask, and the stirring paddle is fixed at the lower end of the shaft lever. When carrying out the experiment of titanium liquid hydrolysis, earlier with the bottom water of constant temperature water bath heating, the bottom water in the constant temperature water bath heats the titanium liquid in the three-necked flask, then the starter motor drives the axostylus axostyle and rotates, and the axostylus axostyle drives the stirring rake and stirs the titanium liquid. In the experimentation, titanium liquid is heated and can steam, and at axostylus axostyle internal rotation in-process in the bottle plug, steam spills over from the position that the axostylus axostyle penetrated the bottle plug easily, leads to the acidity and the concentration of titanium liquid can change, finally can lead to the experimental result inaccurate.
SUMMERY OF THE UTILITY MODEL
Aiming at the technical problems in the prior art, the utility model provides a titanium liquid hydrolysis experimental device.
The utility model aims to realize the technical scheme, which comprises a constant temperature water bath kettle, a three-neck flask, a first motor, a first shaft lever, a first stirring paddle, a thermometer and a reflux condensation pipe, wherein the lower part of the three-neck flask is positioned in the constant temperature water bath kettle, three bottle mouths of the three-neck flask are respectively provided with a first bottle stopper, a second bottle stopper and a third bottle stopper, a glass bulb of the thermometer penetrates through the first bottle stopper and then enters the three-neck flask, the second bottle stopper is provided with a condensation pipe interface, the lower end of an inner pipe of the reflux condensation pipe is connected with the condensation pipe interface, the upper end of the inner pipe of the reflux condensation pipe is sealed, the upper end of the first shaft lever is fixed on a rotating shaft of the first motor, the lower end of the first shaft lever penetrates through the third bottle stopper and then enters the three-neck flask, the lower end of the first shaft lever is provided with the first stirring paddle, and a sleeve is sleeved on the first shaft lever, the upper end of the sleeve is fixed on the third bottle stopper.
Further, first bottle plug, second bottle plug and third bottle plug are rubber buffer or silica gel stopper.
Furthermore, a sealing plug is arranged at the upper end of the reflux condensation pipe.
Further, the sealing plug is a rubber plug or a silica gel plug.
Furthermore, the titanium liquid hydrolysis experimental device further comprises a second motor, a second shaft rod and a second stirring paddle, wherein the upper end of the second shaft rod is fixedly connected to a rotating shaft of the second motor, the stirring paddle is fixed at the lower end of the second shaft rod, and the stirring paddle is located in the constant-temperature water bath.
Due to the adoption of the technical scheme, the utility model has the beneficial effects that:
before the titanium liquid hydrolysis experiment device disclosed by the utility model is used for carrying out a titanium liquid hydrolysis experiment, titanium liquid is added into a three-neck flask, so that the lower end of a sleeve and glass bubbles of a thermometer are submerged by the titanium liquid. When a hydrolysis experiment is carried out, bottom water in a constant-temperature water bath kettle is heated to a required temperature, titanium liquid in a three-neck flask is heated by the bottom water in the constant-temperature water bath kettle, the temperature of the titanium liquid is determined by an observation thermometer, and a time point when the titanium liquid reaches the required hydrolysis temperature is conveniently determined. Start first motor, first motor drives the rotation of primary shaft pole, the stirring rake stirs the titanium liquid along with the rotation of primary shaft pole, because sheathed tube one end is fixed on the third bottle plug, the sheathed tube other end submerges in the titanium liquid, primary shaft pole rotates the in-process, the vapor that the position that can significantly reduce penetrated the third bottle plug from primary shaft pole spills over, vapor can get into the backward flow condenser pipe through the condenser pipe interface and carry out the condensation backward flow, the reduction volume of the water that makes in the titanium liquid is less, the acidity and the concentration variation volume that make the titanium liquid are less, it is more accurate to make the experimental result.
Drawings
FIG. 1 is a schematic structural diagram of a titanium liquid hydrolysis experimental apparatus of the present invention.
In the figure, 1, a constant temperature water bath kettle; 2. a three-neck flask; 3. a first motor; 4. a first shaft lever; 5. first stirring slurry; 6. a thermometer; 7. a reflux condenser tube; 8. a first stopper; 9. a second stopper; 10. a third bottle stopper; 11. a condenser tube interface; 12. a sealing plug; 13. a sleeve; 14. a second motor; 15. a second shaft lever; 16. a second stirring paddle.
Detailed Description
In order to make the technical means, the creation characteristics, the achievement purposes and the effects of the utility model easy to understand, the utility model is further explained below by combining the specific drawings.
As shown in fig. 1, the present invention includes a constant temperature water bath 1, a three-neck flask 2, a first motor 3, a first shaft rod 4, a first stirring paddle 5, a thermometer 6 and a reflux condenser tube 7, wherein the lower portion of the three-neck flask 2 is located in the constant temperature water bath 1, three necks of the three-neck flask 2 are respectively provided with a first bottle stopper 8, a second bottle stopper 9 and a third bottle stopper 10, a glass bulb of the thermometer 6 passes through the first bottle stopper 8 and then enters the three-neck flask 2, the second bottle stopper 9 is provided with a condenser tube interface 11, and the condenser tube interface 11 penetrates through two ends of the second bottle stopper 9, such that water vapor generated in the three-neck flask 2 can enter the reflux condenser tube 7 connected to the condenser tube interface 11 through the condenser tube interface 11. The lower end of the inner pipe of the reflux condenser pipe 7 is connected with a condenser pipe interface 11, and the upper end of the reflux condenser pipe 7 is provided with a sealing plug 12, so that the upper end of the inner pipe of the reflux condenser pipe 7 is sealed. The sealing plug 12 is a rubber plug, and in other embodiments, the sealing plug 12 may also be a silicone plug. The upper end of the first shaft rod 4 is fixed on the rotating shaft of the first motor 3, the lower end of the first shaft rod 4 passes through the third bottle stopper 10 and then enters the three-mouth flask 2, the lower end of the first shaft rod 4 is provided with a first stirring paddle, the first shaft rod 4 is sleeved with a sleeve 13, and the upper end of the sleeve 13 is fixed on the third bottle stopper 10. In order to seal the opening of the three-mouth flask 2 well, the first bottle plug 8, the second bottle plug 9 and the third bottle plug 10 are rubber plugs, and the first bottle plug 8, the second bottle plug 9 and the third bottle plug 10 can also be silica gel plugs in other embodiments.
The titanium liquid hydrolysis experiment device further comprises a second motor 14, a second shaft rod 15 and a second stirring paddle 16, wherein the upper end of the second shaft rod 15 is fixedly connected to a rotating shaft of the second motor 14, the stirring paddle is fixed at the lower end of the second shaft rod 15, and the stirring paddle is located in the constant-temperature water bath 1. Can drive second axostylus axostyle 15 through second motor 14 and rotate, second stirring rake 16 rotates along with second axostylus axostyle 15 to stir the end water in the constant temperature water bath 1, when constant temperature water bath 1 heats end water, can drive the water that is close to the heating element of constant temperature water bath 1 and keeps away from the water of the heating element of constant temperature water bath 1 and constantly mix, can make the hydroenergy of each position in the constant temperature water tank can more even intensification.
Before the titanium liquid hydrolysis experiment device is used for carrying out a titanium liquid hydrolysis experiment, titanium liquid is added into the three-neck flask 2, so that the lower end of the sleeve 13 and glass bubbles of the thermometer 6 are submerged by the titanium liquid. When a hydrolysis experiment is carried out, the bottom water in the constant-temperature water bath pot 1 is heated to a required temperature, the titanium liquid in the three-neck flask 2 is heated by the bottom water in the constant-temperature water bath pot 1, the temperature of the titanium liquid is determined by the observation thermometer 6, and the time point when the titanium liquid reaches the required hydrolysis temperature is conveniently determined. Start first motor 3, first motor 3 drives first axostylus axostyle 4 and rotates, the stirring rake stirs the titanium liquid along with first axostylus axostyle 4 rotation, because the one end of sleeve pipe 13 is fixed on third bottle plug 10, the other end of sleeve pipe 13 submerges in the titanium liquid, first axostylus axostyle 4 rotates the in-process, the vapor that the position that can significantly reduce to penetrate third bottle plug 10 from first axostylus axostyle 4 spills over, vapor can get into backward flow condenser pipe 7 through condenser pipe interface 11 and carry out the condensation backward flow, make the reduction volume of the water in the titanium liquid less, make the acidity and the concentration variation of titanium liquid less, it is more accurate to make the experimental result.
The above description is only an embodiment of the present invention, and not intended to limit the scope of the present invention, and all equivalent structures made by using the contents of the present specification and the drawings can be directly or indirectly applied to other related technical fields, and are within the scope of the present invention.
Claims (5)
1. The utility model provides a titanium liquid experimental apparatus that hydrolysises which characterized in that: the temperature-controlled three-mouth water bath kettle comprises a constant-temperature water bath kettle, a three-mouth flask, a first motor, a first shaft lever, a first stirring paddle, a thermometer and a reflux condensation pipe, wherein the lower part of the three-mouth flask is positioned in the constant-temperature water bath kettle, three bottle mouths of the three-mouth flask are respectively provided with a first bottle plug, a second bottle plug and a third bottle plug, a glass bulb of the thermometer penetrates through the first bottle plug and then enters the three-mouth flask, a condensation pipe port is arranged on the second bottle plug, the lower end of an inner pipe of the reflux condensation pipe is connected with the condensation pipe port, the upper end of the inner pipe of the reflux condensation pipe is sealed, the upper end of the first shaft lever is fixed on a rotating shaft of the first motor, the lower end of the first shaft lever penetrates through the third bottle plug and then enters the three-mouth flask, the lower end of the first shaft lever is provided with the first stirring paddle, a sleeve is sleeved on the first shaft lever, and the upper end of the sleeve is fixed on the third bottle.
2. The titanium liquid hydrolysis experimental device as set forth in claim 1, characterized in that: the first bottle stopper, the second bottle stopper and the third bottle stopper are rubber stoppers or silica gel stoppers.
3. The titanium liquid hydrolysis experimental device as set forth in claim 1, characterized in that: and a sealing plug is arranged at the upper end of the reflux condensation pipe.
4. The titanium liquid hydrolysis experimental device as set forth in claim 3, wherein: the sealing plug is a rubber plug or a silica gel plug.
5. The titanium liquid hydrolysis experimental device as set forth in claim 1, characterized in that: the titanium liquid hydrolysis experimental device further comprises a second motor, a second shaft lever and a second stirring paddle, wherein the upper end of the second shaft lever is fixedly connected to a rotating shaft of the second motor, the stirring paddle is fixed at the lower end of the second shaft lever, and the stirring paddle is located in the constant-temperature water bath.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202122460604.2U CN215783379U (en) | 2021-10-12 | 2021-10-12 | Titanium liquid hydrolysis experimental device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202122460604.2U CN215783379U (en) | 2021-10-12 | 2021-10-12 | Titanium liquid hydrolysis experimental device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN215783379U true CN215783379U (en) | 2022-02-11 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202122460604.2U Active CN215783379U (en) | 2021-10-12 | 2021-10-12 | Titanium liquid hydrolysis experimental device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN215783379U (en) |
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2021
- 2021-10-12 CN CN202122460604.2U patent/CN215783379U/en active Active
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