CN215693962U

CN215693962U - Iron-based metal organic framework-boron-based covalent organic framework composite reaction kettle

Info

Publication number: CN215693962U
Application number: CN202121934552.1U
Authority: CN
Inventors: 栾奕; 周子浩
Original assignee: Jiaxing Zhefuete Environmental Protection Technology Co ltd
Current assignee: Jiaxing Zhefuete Environmental Protection Technology Co ltd
Priority date: 2021-08-18
Filing date: 2021-08-18
Publication date: 2022-02-01
Anticipated expiration: 2031-08-18

Abstract

The utility model discloses an iron-based metal organic framework-boron-based covalent organic framework composite reaction kettle, which belongs to the technical field of chemical equipment, and adopts the technical scheme that the reaction kettle comprises a kettle body and a kettle cover, wherein the kettle body and the kettle cover are detachably connected through bolts, a motor is arranged on the upper end surface of the kettle cover, the output end of the motor is fixedly connected with a rotating shaft, the other end of the rotating shaft penetrates through the kettle cover and extends to the lower part of the kettle cover, the outer side wall of the rotating shaft is fixedly connected with a rotating pipe, the outer side wall of the rotating pipe is fixedly connected with a plurality of first stirring blades which are uniformly distributed, a solution poured into the reaction kettle is conveniently isolated from the inner bottom end of the kettle body through a sealing box and an electromagnetic block, the problem that the solution in the reaction kettle enters a discharging pipe is avoided, and the stirring effect of the solution in the kettle body is poor, resulting in a problem of insufficient reaction.

Description

Iron-based metal organic framework-boron-based covalent organic framework composite reaction kettle

Technical Field

The utility model relates to the technical field of chemical equipment, in particular to an iron-based metal organic framework-boron-based covalent organic framework composite reaction kettle.

Background

Among the prior art, reation kettle is the essential equipment of chemical production, mainly includes a jar body that can be inclosed, and jar internal stirring subassembly that can be provided with, stirring subassembly include the (mixing) shaft with install at the epaxial stirring rake of stirring, and the top of jar body is provided with motor and the feed inlet that drives stirring subassembly, and is hopper-shaped in the bottom of the jar body, is provided with the discharge gate in the minimum, and the discharge gate can be provided with the control valve.

The existing iron-based metal organic framework-boron-based covalent organic framework composite reaction kettle is generally communicated with a discharge pipe at the bottom end for convenient discharge, and a valve is arranged outside the discharge pipe, but the stirring effect of the iron-based metal organic framework-boron-based covalent organic framework in the discharge pipe is poor due to the mode, and further insufficient reaction is caused.

SUMMERY OF THE UTILITY MODEL

In order to solve the problems in the background art, the utility model provides an iron-based metal organic framework-boron-based covalent organic framework composite reaction kettle which has the characteristics that a solution poured into the reaction kettle is conveniently isolated from the inner bottom end of a kettle body by arranging a sealing box and an electromagnetic block, so that the problem that the solution in the reaction kettle enters a discharge pipe is avoided, and further the problem that the solution in the kettle body is not well stirred and the reaction is not sufficient is caused.

In order to achieve the purpose, the utility model provides the following technical scheme: an iron-based metal organic framework-boron-based covalent organic framework composite reaction kettle comprises a kettle body and a kettle cover, wherein the kettle body and the kettle cover are detachably connected through bolts, a motor is installed on the upper end face of the kettle cover, a rotating shaft is fixedly connected with the output end of the motor, the other end of the rotating shaft penetrates through the kettle cover and extends to the lower part of the kettle cover, a rotating pipe is fixedly connected with the outer side wall of the rotating shaft, a plurality of first stirring blades which are uniformly distributed are fixedly connected with the outer side wall of the rotating pipe, second stirring blades are fixedly connected with the lower end faces of the first stirring blades positioned below the lower part of the rotating pipe, a sliding groove is fixedly connected with the inner bottom end of the rotating pipe, two sliding balls are slidably connected with the inner part of the sliding groove, a sliding rod is fixedly connected with one side of each sliding ball opposite to the other side of each sliding ball, an air cylinder is fixedly connected between the two sliding rods, and a piston rod is fixedly connected with the output end of the air cylinder, the other end of the piston rod runs through the lower end of the rotating pipe and extends to the lower part of the rotating pipe, the piston rod extends to one end fixedly connected with sealing box below the rotating pipe, and the lower end fixedly connected with of the sealing box is connected with the electromagnetic block matched with the bottom end inside the kettle body.

In order to conveniently control the pressure inside the reaction kettle, the iron-based metal organic framework-boron-based covalent organic framework composite reaction kettle is preferably used, a pressure gauge is installed at the front end of the outer side wall of the kettle body, a pressure relief pipe is communicated with the left side of the kettle body, and a pressure relief valve is installed on the outer side wall of the pressure relief pipe.

In order to facilitate feeding and discharging, the iron-based metal organic framework-boron-based covalent organic framework composite reaction kettle is preferably used as the iron-based metal organic framework-boron-based covalent organic framework composite reaction kettle provided by the utility model, the upper end surface of the kettle cover is communicated with a feeding pipe, the upper end of the outer side wall of the feeding pipe is in threaded connection with a sealing cover, the lower end surface of the kettle body is communicated with a discharging pipe, and the outer side wall of the discharging pipe is provided with a valve.

In order to support the reaction kettle conveniently, the preferable iron-based metal organic framework-boron-based covalent organic framework composite reaction kettle is characterized in that the outer side wall of the kettle body is fixedly connected with a plurality of uniformly distributed supporting blocks, the lower end surfaces of the supporting blocks are fixedly connected with supporting columns, and the lower end surfaces of the supporting columns are fixedly connected with supporting plates.

In order to facilitate control of the reaction kettle, the iron-based metal organic framework-boron-based covalent organic framework composite reaction kettle is preferably used, wherein a control panel is installed at the front end of the outer side wall of the kettle body, and the control panel is located below a pressure gauge.

In order to conveniently dissipate heat of the motor, the iron-based metal organic framework-boron-based covalent organic framework composite reaction kettle is preferably used, a heat dissipation box is arranged outside the motor, a heat dissipation fan is arranged on the upper end face of the heat dissipation box, and a plurality of heat dissipation holes are uniformly distributed in the outer side wall of the heat dissipation box in a penetrating mode.

Compared with the prior art, the utility model has the beneficial effects that:

1. before the iron-based metal organic framework-boron-based covalent organic framework composite reaction kettle is poured into a reaction kettle, firstly, a cylinder is started, the cylinder drives a sealing box to move downwards through a piston rod connected with the cylinder until an annular electromagnetic block is tightly attached to the inside of a kettle body, then, the electromagnetic block is electrified to be adsorbed and fixed with the inside of the kettle body, the sealing box and the electromagnetic block are convenient to isolate the solution poured into the reaction kettle from the bottom end inside the kettle body, the problem that the solution inside the kettle body enters a discharge pipe is avoided, after the solution is poured into the reaction kettle, a motor is started, the motor drives a rotating pipe to rotate through a rotating shaft, and then drives a first stirring blade to stir the solution in the reaction kettle, and a second stirring blade is arranged to avoid the problem that the solution stirring effect of the bottom end inside the kettle body is poor, the runner pipe drives the spout rotatory in the stirring process, and then the sliding rod connection sliding ball slides in the spout, when avoiding the runner pipe rotatory, drives the rotatory problem of cylinder.

2. This kind of compound reation kettle of iron-based metal organic framework-boron base covalence organic framework observes when the inside pressure of cauldron body is too high through the manometer, starts the relief valve, and the inside air current of cauldron body is slowly discharged from the relief pipe, and then has reduced the inside pressure of cauldron body, and then has reached the effect of the inside pressure of convenient control cauldron body.

3. This kind of compound reation kettle of iron-based metal organic framework-boron base covalence organic framework, when pouring solution into reation kettle, at first unscrew sealed lid, fall into solution from the inlet pipe of kettle cover installation after that, when taking out solution, at first cut off the power supply for the electromagnetic block, start the cylinder after that, the cylinder passes through the piston rod and drives the seal box and shift up, open the valve after that, solution among the reation kettle flows from the discharging pipe, and then has reached the effect of making things convenient for feeding and ejection of compact.

To sum up, this kind of reation kettle is through setting up seal box and electromagnetism piece, and the solution that conveniently will pour into in reation kettle is isolated with the inside bottom of the internal body of cauldron, has avoided the problem in the inside solution entering discharging pipe of reation kettle, and then leads to the internal portion of cauldron solution stirring effect not good, leads to reacting insufficient problem.

Drawings

The accompanying drawings, which are included to provide a further understanding of the utility model and are incorporated in and constitute a part of this specification, illustrate embodiments of the utility model and together with the description serve to explain the principles of the utility model and not to limit the utility model.

In the drawings:

FIG. 1 is a structural diagram of an iron-based metal organic framework-boron-based covalent organic framework composite reaction kettle of the utility model;

FIG. 2 is a sectional view of an iron-based metal organic framework-boron-based covalent organic framework composite reaction kettle of the utility model;

FIG. 3 is an enlarged view of the utility model at A in FIG. 2.

In the figure, 1, a kettle body; 2. a kettle cover; 3. a motor; 4. a rotating shaft; 5. pipe rotation; 6. a first stirring blade; 7. a chute; 8. a sliding ball; 9. a slide bar; 10. a cylinder; 11. a piston rod; 12. a sealing box; 13. an electromagnetic block; 14. a second stirring blade; 15. a pressure gauge; 16. a pressure relief pipe; 17. a pressure relief valve; 18. a feed pipe; 19. a sealing cover; 20. a discharge pipe; 21. a valve; 22. a support block; 23. a support pillar; 24. a support plate; 25. a control panel; 26. a heat dissipation box; 27. a heat dissipation fan.

Detailed Description

In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention is described in further detail below with reference to the accompanying drawings and embodiments. It should be understood that the specific embodiments described herein are merely illustrative of the utility model and are not intended to limit the utility model.

In the description of the present invention, it is to be understood that the terms "length", "width", "upper", "lower", "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outer", and the like, indicate orientations or positional relationships based on the orientations or positional relationships illustrated in the drawings, and are used merely for convenience in describing the present invention and for simplicity in description, and do not indicate or imply that the devices or elements referred to must have a particular orientation, be constructed in a particular orientation, and be operated, and thus, are not to be construed as limiting the present invention. Further, in the description of the present invention, "a plurality" means two or more unless specifically defined otherwise.

Referring to fig. 1-3, the present invention provides the following technical solutions: an iron-based metal organic framework-boron-based covalent organic framework composite reaction kettle comprises a kettle body 1 and a kettle cover 2, wherein the kettle body 1 and the kettle cover 2 are detachably connected through bolts, a motor 3 is installed on the upper end face of the kettle cover 2, a rotating shaft 4 is fixedly connected with the output end of the motor 3, the other end of the rotating shaft 4 penetrates through the kettle cover 2 and extends to the lower part of the kettle cover 2, a rotating pipe 5 is fixedly connected with the outer side wall of the rotating shaft 4, a plurality of uniformly distributed first stirring blades 6 are fixedly connected with the outer side wall of the rotating pipe 5, second stirring blades 14 are fixedly connected with the lower end faces of the first stirring blades 6 positioned below, a sliding groove 7 is fixedly connected with the inner bottom end of the rotating pipe 5, two sliding balls 8 are slidably connected with the inner part of the sliding groove 7, sliding rods 9 are fixedly connected with one side opposite to the two sliding balls 8, an air cylinder 10 is fixedly connected between the two sliding rods 9, and a piston rod 11 is fixedly connected with the output end of the air cylinder 10, the other end of piston rod 11 runs through the lower extreme of runner pipe 5 and extends to the below of runner pipe 5, and piston rod 11 extends to the one end fixedly connected with seal box 12 of runner pipe 5 below, and the lower extreme fixedly connected with of seal box 12 and the inside bottom assorted electromagnetism piece 13 of cauldron body 1.

In this embodiment: before pouring the iron-based metal organic framework-boron-based covalent organic framework solution into the reaction kettle, firstly starting the air cylinder 10, driving the sealing box 12 to move downwards by the air cylinder 10 through the piston rod 11 connected with the air cylinder until the annular electromagnetic block 13 is tightly attached to the inner part of the kettle body 1, then electrifying the electromagnetic block 13 to ensure that the electromagnetic block 13 is adsorbed and fixed with the inner part of the kettle body 1, conveniently isolating the solution poured into the reaction kettle from the inner bottom end of the kettle body 1 by the sealing box 12 and the electromagnetic block 13, avoiding the problem that the solution in the kettle body 1 enters the discharge pipe 20, starting the motor 3 after pouring the solution into the reaction kettle, driving the rotating pipe 5 to rotate by the motor 3 through the rotating shaft 4, further driving the first stirring blade 6 to stir the solution in the reaction kettle, and avoiding the problem that the solution stirring effect of the inner bottom end of the kettle body 1 is poor by the arrangement of the second stirring blade 14, in the stirring process, the rotating pipe 5 drives the sliding groove 7 to rotate, and then the sliding rod 9 is connected with the sliding ball 8 to slide in the sliding groove 7, so that the problem that the rotating pipe 5 drives the air cylinder 10 to rotate when rotating is avoided.

As a technical optimization scheme of the utility model, a pressure gauge 15 is arranged at the front end of the outer side wall of the kettle body 1, the left side of the kettle body 1 is communicated with a pressure relief pipe 16, and a pressure relief valve 17 is arranged on the outer side wall of the pressure relief pipe 16.

In this embodiment: observe the inside pressure of the cauldron body 1 when too high through manometer 15, start relief valve 17, slow discharge in 16 from the pressure release pipe is followed to the inside air current of the cauldron body 1, and then has reduced the inside pressure of the cauldron body 1, and then has reached the effect of conveniently controlling the inside pressure of the cauldron body 1.

As a technical optimization scheme of the utility model, the upper end surface of the kettle cover 2 is communicated with a feeding pipe 18, the upper end of the outer side wall of the feeding pipe 18 is in threaded connection with a sealing cover 19, the lower end surface of the kettle body 1 is communicated with a discharging pipe 20, and the outer side wall of the discharging pipe 20 is provided with a valve 21.

In this embodiment: when pouring solution into reation kettle, at first unscrew sealed lid 19, pour into solution from the inlet pipe 18 of installation on the kettle cover 2 after that, when taking out solution, at first cut off the power supply for electromagnetic block 13, start cylinder 10 after that, cylinder 10 shifts up through piston rod 11 drive seal box 12, opens valve 21 after that, and solution in the reation kettle flows out from discharging pipe 20, and then has reached the effect that makes things convenient for feeding and ejection of compact.

As a technical optimization scheme of the utility model, the outer side wall of the kettle body 1 is fixedly connected with a plurality of uniformly distributed supporting blocks 22, the lower end surfaces of the supporting blocks 22 are fixedly connected with supporting columns 23, and the lower end surfaces of the supporting columns 23 are fixedly connected with supporting plates 24.

In this embodiment: supporting shoe 22 plays the effect of connecting still body 1 and support column 23, and support column 23 has the effect that conveniently supports still body 1, and backup pad 24 has increased the area of contact with ground, the pressure of the dispersion support column 23 of being convenient for, installs the whole reation kettle of control panel 25 of being convenient for control at the 1 front end of the still body to set up control panel 25 in the below of manometer 15, the operation of being convenient for.

As a technical optimization scheme of the utility model, the front end of the outer side wall of the kettle body 1 is provided with a control panel 25, and the control panel 25 is positioned below the pressure gauge 15.

In this embodiment: through installing control panel 25 at the lateral wall front end of cauldron body 1, and then have the effect of conveniently controlling reation kettle.

As a technical optimization scheme of the utility model, a heat dissipation box 26 is arranged outside the motor 3, a heat dissipation fan 27 is installed on the upper end face of the heat dissipation box 26, and a plurality of heat dissipation holes are uniformly distributed and penetrate through the outer side wall of the heat dissipation box 26.

In this embodiment: when the motor 3 generates heat in the long-time working process, the heat dissipation fan 27 is started, the heat dissipation of the motor 3 is facilitated, and the heat dissipation effect is further improved due to the plurality of heat dissipation holes formed in the outer side wall of the heat dissipation box 26.

The working principle and the using process of the utility model are as follows: before pouring the iron-based metal organic framework-boron-based covalent organic framework solution into the reaction kettle, firstly starting the air cylinder 10, driving the sealing box 12 to move downwards by the air cylinder 10 through the piston rod 11 connected with the air cylinder until the annular electromagnetic block 13 is tightly attached to the inner part of the kettle body 1, then electrifying the electromagnetic block 13 to ensure that the electromagnetic block 13 is adsorbed and fixed with the inner part of the kettle body 1, conveniently isolating the solution poured into the reaction kettle from the inner bottom end of the kettle body 1 by the sealing box 12 and the electromagnetic block 13, avoiding the problem that the solution in the kettle body 1 enters the discharge pipe 20, starting the motor 3 after pouring the solution into the reaction kettle, driving the rotating pipe 5 to rotate by the motor 3 through the rotating shaft 4, further driving the first stirring blade 6 to stir the solution in the reaction kettle, and avoiding the problem that the solution stirring effect of the inner bottom end of the kettle body 1 is poor by the arrangement of the second stirring blade 14, in the stirring process, the runner 5 drives the chute 7 to rotate, and then the slide bar 9 is connected the smooth ball 8 and is slided in the chute 7, when avoiding runner 5 to rotate, drive the rotatory problem of cylinder 10, in the solution reaction process, observe the pressure change of the internal portion of cauldron body 1 through manometer 15, when pressure is too high, start relief valve 17, the slow discharge in the pressure release pipe 16 is followed to the air current of the internal portion of cauldron body 1, and then reached the effect of the internal portion's of convenient control cauldron body 1 pressure, when the solution after will taking out the reaction, at first cut off the power supply for electromagnetic block 13, start cylinder 10 after that, cylinder 10 drives seal box 12 through piston rod 11 and shifts up, open valve 21 after that, the solution in the reation kettle flows out from discharging pipe 20.

The present invention is not limited to the above preferred embodiments, and any modifications, equivalent substitutions and improvements made within the spirit and principle of the present invention should be included in the protection scope of the present invention.

Claims

1. The utility model provides a compound reation kettle of covalent organic skeleton of iron-based metal organic skeleton-boron base, includes cauldron body (1) and kettle cover (2), can dismantle the connection through the bolt between cauldron body (1) and kettle cover (2), its characterized in that: the kettle cover is characterized in that a motor (3) is installed on the upper end face of the kettle cover (2), a rotating shaft (4) is fixedly connected to the output end of the motor (3), the other end of the rotating shaft (4) penetrates through the kettle cover (2) and extends to the lower portion of the kettle cover (2), a rotating pipe (5) is fixedly connected to the outer side wall of the rotating shaft (4), a plurality of uniformly distributed first stirring blades (6) are fixedly connected to the outer side wall of the rotating pipe (5), second stirring blades (14) are fixedly connected to the lower end faces of the first stirring blades (6) located below, a sliding chute (7) is fixedly connected to the inner bottom end of the rotating pipe (5), two sliding balls (8) are slidably connected to the inner portion of the sliding chute (7), a sliding rod (9) is fixedly connected to one side, opposite to the two sliding balls (8), an air cylinder (10) is fixedly connected to the two sliding rods (9), and a piston rod (11) is fixedly connected to the output end of the air cylinder (10), the other end of piston rod (11) runs through the lower extreme of rotating pipe (5) and extends to the below of rotating pipe (5), piston rod (11) extend to one end fixedly connected with seal box (12) of rotating pipe (5) below, the lower extreme fixedly connected with of seal box (12) and the inside bottom assorted electromagnetism piece (13) of cauldron body (1).

2. The iron-based metal organic framework-boron-based covalent organic framework composite reaction kettle of claim 1, which is characterized in that: manometer (15) are installed to the lateral wall front end of cauldron body (1), the left side intercommunication of cauldron body (1) has pressure release pipe (16), pressure release valve (17) are installed to the lateral wall of pressure release pipe (16).

3. The iron-based metal organic framework-boron-based covalent organic framework composite reaction kettle of claim 1, which is characterized in that: the upper end face intercommunication of cauldron lid (2) has inlet pipe (18), the lateral wall upper end threaded connection of inlet pipe (18) has sealed lid (19), the lower terminal surface intercommunication of cauldron body (1) has discharging pipe (20), valve (21) are installed to the lateral wall of discharging pipe (20).

4. The iron-based metal organic framework-boron-based covalent organic framework composite reaction kettle of claim 1, which is characterized in that: the outer side wall of the kettle body (1) is fixedly connected with a plurality of uniformly distributed supporting blocks (22) in a plurality of modes, and the lower end face of each supporting block (22) is fixedly connected with a supporting column (23) in a plurality of modes, and the lower end face of each supporting column (23) is fixedly connected with a supporting plate (24) in a plurality of modes.

5. The iron-based metal organic framework-boron-based covalent organic framework composite reaction kettle of claim 1, which is characterized in that: control panel (25) are installed to the lateral wall front end of cauldron body (1), control panel (25) are located the below of manometer (15).

6. The iron-based metal organic framework-boron-based covalent organic framework composite reaction kettle of claim 1, which is characterized in that: the outside of motor (3) is provided with heat dissipation case (26), heat dissipation fan (27) are installed to the up end of heat dissipation case (26), the lateral wall of heat dissipation case (26) runs through the louvre that has seted up a plurality of evenly distributed.