CN215678103U - Microcosmic visual hydrate analyzer - Google Patents
Microcosmic visual hydrate analyzer Download PDFInfo
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- CN215678103U CN215678103U CN202121143953.5U CN202121143953U CN215678103U CN 215678103 U CN215678103 U CN 215678103U CN 202121143953 U CN202121143953 U CN 202121143953U CN 215678103 U CN215678103 U CN 215678103U
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Abstract
The utility model discloses a microscopic visual hydrate analyzer, which mainly comprises: the device comprises a sample loading module, a pressurizing module, a temperature control module, a high-pressure visual module, a microscopic observation module and an online measurement module; the sample is added into the high-pressure visual module through the sample loading module, the high-pressure visual module is connected with the pressurizing module, the sample is pressurized through the pressurizing module, the processed sample is loaded into the temperature control module to be subjected to temperature control, and the sample processed in the temperature control module is subjected to microscopic observation and Raman test through the microscopic observation module. The utility model can realize real-time observation and on-line analysis of the sample in the environment of variable temperature and variable pressure by mutually associating all the modules, carrying out pressurization and temperature control treatment in batches and observing and detecting the sample by a Raman microscope.
Description
Technical Field
The utility model relates to the technical field of petroleum and natural gas, in particular to a microscopic visual hydrate analyzer.
Background
In the oil and gas field, the sample usually needs to be tested at high temperature and high pressure, but common test equipment can not realize real-time testing, and the sample is often subjected to pressurization and temperature control treatment, and then data are detected through the equipment, so that the temperature is easily diffused in the process, and the pressure is reduced to cause the result to have deviation.
Therefore, how to provide a device capable of not only performing high temperature and high pressure processing but also analyzing data in real time is a problem that needs to be solved by those skilled in the art.
SUMMERY OF THE UTILITY MODEL
In view of the above, the utility model provides a microscopic visual hydrate analyzer capable of performing high-temperature and high-pressure processing and analyzing data in real time.
In order to achieve the above object, the present invention provides the following technical solutions, which mainly include: the device comprises a sample loading module, a pressurizing module, a temperature control module, a high-pressure visual module, a microscopic observation module and an online measurement module; the sample is added into the high-pressure visual module through the sample loading module, the high-pressure visual module is connected with the pressurizing module, the sample is pressurized through the pressurizing module, the processed sample is loaded into the temperature control module to be subjected to temperature control, and the sample processed in the temperature control module is subjected to microscopic observation and Raman test through the microscopic observation module.
Preferably, in the microscopic visual hydrate analyzer, the high-pressure visual module is a high-pressure visual cavity; the temperature control module is a cold and hot platform and the microscopic observation module is a Raman microscope.
Preferably, in the microscopic visual hydrate analyzer, the pressurizing range of the pressurizing module is mechanical vacuum to 100 mpa; the temperature control module is used for controlling the temperature to be-195-500 ℃.
Preferably, in the microscopic visual hydrate analyzer, the high-pressure visual cavity is a silicon tube.
Preferably, in the microscopic visualization hydrate analyzer, the raman microscope includes: the system comprises a spectrometer, a Raman box, a laser controller and data analysis equipment; the Raman box is arranged on a microscope, an ocular is arranged on the microscope, and an ocular adjusting knob is arranged on the side surface of the microscope; the processed sample is mounted on the microscope, the detection is carried out through the spectrometer and the laser controller, the detected information is transmitted to the data analysis equipment, and microscopic observation is carried out through the ocular lens.
According to the technical scheme, compared with the prior art, the utility model discloses a microscopic visual hydrate analyzer; the utility model can realize real-time observation and on-line analysis of the sample in the environment of variable temperature and variable pressure by mutually associating all the modules, carrying out pressurization and temperature control treatment in batches and observing and detecting the sample by a Raman microscope.
Drawings
In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings used in the description of the embodiments or the prior art will be briefly described below, it is obvious that the drawings in the following description are only embodiments of the present invention, and for those skilled in the art, other drawings can be obtained according to the provided drawings without creative efforts.
FIG. 1 is a schematic diagram of the present invention.
Fig. 2 is a schematic diagram of the working principle of the utility model.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring to fig. 1-2, a microscopic visual hydrate analyzer is disclosed in the present invention.
The utility model mainly comprises the following steps: the device comprises a sample loading module 1, a pressurizing module 2, a temperature control module 3, a high-pressure visual module, a microscopic observation module 4 and an online measurement module; the sample is added into the high-pressure visual module through the sample loading module 1, the high-pressure visual module is connected with the pressurizing module 2, the sample is pressurized through the pressurizing module 2, the processed sample is loaded into the temperature control module 3 for temperature control, and microscopic observation and Raman test are carried out on the sample processed in the temperature control module 3 through the microscopic observation module 4.
The high-voltage visual module is a high-voltage visual cavity; the temperature control module 3 is a cold and hot stage, and the microscopic observation module 4 is a Raman microscope.
In order to further optimize the technical scheme, the high-pressure visual cavity is a silicon tube.
In order to further optimize the technical scheme, the pressurizing range of the pressurizing module 2 is mechanical vacuum to 100 MPa; the temperature control module is used for controlling the temperature to be-195-500 ℃.
In order to further optimize the technical scheme, the change of the sample in the temperature and pressure changing process is observed in real time during microscopic observation in a Raman microscope; and the change of the substance in the temperature and pressure changing process is detected in real time during the Raman test.
In order to further optimize the above technical solution, the raman microscope comprises: the system comprises a spectrometer, a Raman box, a laser controller and data analysis equipment; the Raman box is arranged on a microscope, an ocular is arranged on the microscope, and an ocular adjusting knob is arranged on the side surface of the microscope; the processed sample is mounted on the microscope, the detection is carried out through the spectrometer and the laser controller, the detected information is transmitted to the data analysis equipment, and microscopic observation is carried out through the ocular lens.
In order to further optimize the technical scheme, the silicon tube is used as a sample cavity of the visual hydrate, the real-time pressurizing module 2 is configured, the sample cavity can be pressurized, the cold and hot platform is connected, the sample cavity can be subjected to real-time temperature change, the Raman microscope is configured, and real-time observation and test are performed in the temperature and pressure changing process of the sample.
The embodiments in the present description are described in a progressive manner, each embodiment focuses on differences from other embodiments, and the same and similar parts among the embodiments are referred to each other. For the modules disclosed in the embodiments, the description is relatively simple because the modules correspond to the methods disclosed in the embodiments, and the relevant points can be referred to the method part for description.
The previous description of the disclosed embodiments is provided to enable any person skilled in the art to make or use the present invention. Various modifications to these embodiments will be readily apparent to those skilled in the art, and the generic principles defined herein may be applied to other embodiments without departing from the spirit or scope of the utility model. Thus, the present invention is not intended to be limited to the embodiments shown herein but is to be accorded the widest scope consistent with the principles and novel features disclosed herein.
Claims (5)
1. The microscopic visualization hydrate analyzer is characterized by mainly comprising: the device comprises a sample loading module, a pressurizing module, a temperature control module, a high-pressure visual module, a microscopic observation module and an online measurement module; the sample loading module is used for loading a sample into the high-pressure visual module, the high-pressure visual module is connected with the pressurizing module, the sample is pressurized through the pressurizing module, the processed sample is loaded into the temperature control module for temperature control, and microscopic observation and Raman test are carried out on the sample processed in the temperature control module through the microscopic observation module.
2. The microscopic visual hydrate analyzer according to claim 1, wherein the high pressure visual module is a high pressure visual chamber; the temperature control module is a cold and hot platform and the microscopic observation module is a Raman microscope.
3. The microscopic visual hydrate analyzer according to claim 2, wherein the high pressure visual cavity is a silicon tube.
4. The microscopic visualization hydrate analyzer of claim 2, wherein the raman microscope comprises: the system comprises a spectrometer, a Raman box, a laser controller and data analysis equipment; the Raman box is arranged on a microscope, an ocular is arranged on the microscope, and an ocular adjusting knob is arranged on the side surface of the microscope; the processed sample is mounted on the microscope, the detection is carried out through the spectrometer and the laser controller, the detected information is transmitted to the data analysis equipment, and microscopic observation is carried out through the ocular lens.
5. The microscopic visual hydrate analyzer according to claim 1, wherein the pressurizing module is pressurized in a range of mechanical vacuum to 100 mpa; the temperature range of the temperature control module is-195-500 ℃.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202121143953.5U CN215678103U (en) | 2021-05-26 | 2021-05-26 | Microcosmic visual hydrate analyzer |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202121143953.5U CN215678103U (en) | 2021-05-26 | 2021-05-26 | Microcosmic visual hydrate analyzer |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN215678103U true CN215678103U (en) | 2022-01-28 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
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| CN202121143953.5U Active CN215678103U (en) | 2021-05-26 | 2021-05-26 | Microcosmic visual hydrate analyzer |
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| CN (1) | CN215678103U (en) |
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2021
- 2021-05-26 CN CN202121143953.5U patent/CN215678103U/en active Active
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