CN215466998U - Safe, unmanned, intelligent and efficient treatment device for Grignard residues - Google Patents

Safe, unmanned, intelligent and efficient treatment device for Grignard residues Download PDF

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Publication number
CN215466998U
CN215466998U CN202122182378.6U CN202122182378U CN215466998U CN 215466998 U CN215466998 U CN 215466998U CN 202122182378 U CN202122182378 U CN 202122182378U CN 215466998 U CN215466998 U CN 215466998U
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grignard
chamber
intelligent
unmanned
safe
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CN202122182378.6U
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蔡斌
徐思虎
张�杰
项玉燕
王世镇
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Nanping Mingzheng Pharmaceutical Chemical Co ltd
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Nanping Mingzheng Pharmaceutical Chemical Co ltd
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Abstract

The utility model relates to the technical field of chemical equipment, in particular to a safe, unmanned, intelligent and efficient Grignard residue treatment device which comprises a treatment box, a drying mechanism arranged on a left panel of the treatment box and a control mechanism arranged on a right panel of the treatment box. According to the utility model, a settling chamber and a filtering chamber are arranged in a processing box, wherein a feeding mechanism and a medicament adding mechanism arranged on the settling chamber are synchronously opened and closed, so that the addition of a treatment medicament is realized while adding Grignard residues, the Grignard residues and the medicament are mixed, the Grignard residues are introduced into the filtering chamber when the precipitation time is up, a filtering screen arranged in the filtering chamber can realize solid-liquid separation of the Grignard residues, and after liquid is discharged, a drying mechanism is used for drying solids intercepted on the filtering screen, so that the pipelined treatment of the Grignard residues is realized.

Description

Safe, unmanned, intelligent and efficient treatment device for Grignard residues
Technical Field
The utility model relates to the technical field of chemical equipment, in particular to a safe, unmanned, intelligent and efficient treatment device for Grignard residues.
Background
Most of Grignard residue treatment equipment in the existing market needs manual online operation, so that the production cost is improved, and the treatment efficiency is low.
SUMMERY OF THE UTILITY MODEL
The utility model aims to provide a safe, unmanned, intelligent and efficient treatment device for Grignard residues, which comprises a sedimentation chamber and a filter chamber arranged in a treatment box, wherein, the feeding mechanism and the medicament adding mechanism arranged on the settling chamber are synchronously opened and closed, so that the addition of the treatment medicament is realized while the addition of the Grignard residue is realized, the Grignard residue and the medicament are mixed, the Grignard residue is introduced into the filtering chamber when the settling time is up, the solid-liquid separation of the Grignard residue can be realized by the filtering net arranged in the filtering chamber, after the liquid is discharged, the drying mechanism is utilized to dry the solid trapped on the filter screen, thereby realizing the production line type treatment of the Grignard residue, the control mechanism of the device adopts time relays for all relays of a relay group, and the intelligent control of the processing device is realized under the control of a PLC (programmable logic controller) so as to solve the problems in the background technology.
In order to achieve the purpose, the utility model provides the following technical scheme:
the utility model provides a safe unmanned intelligent efficient processing apparatus of grignard's residue, including handling the case, the stoving mechanism of setting on handling case left side panel with set up the control mechanism on handling case right side panel, handle incasement portion from last deposit room and the filter chamber of down having set gradually, be provided with the unloading pipe of intercommunication filter chamber on the bottom plate of deposit room, be provided with the unloading valve on the unloading pipe, turn right from a left side on the roof of deposit room and set gradually medicament interpolation mechanism and feed mechanism, the filter chamber is inside to be provided with filtering mechanism, filtering mechanism specifically is the filter screen of setting on inner wall in the middle part of the filter chamber.
As a preferred scheme, the inner wall of the right side of the filtering chamber is provided with a impurity removing port on the right side of the filtering screen, and an end cover is arranged on the impurity removing port.
As a preferred scheme, the right side of the bottom of the filtering chamber is provided with a water outlet pipe extending out of the treatment tank, and the water outlet pipe is provided with a switch valve.
As a preferred scheme, stoving mechanism is including setting up air heating box and the draught fan on handling the case left side panel, and the exhaust tube of draught fan connects the gas outlet of air heating box, and the air supply pipe of draught fan connects the dry trachea that sets up on the filter chamber bottom plate.
As a preferred scheme, a filtering chamber and a heating chamber are sequentially arranged in the air heating box from top to bottom, a filtering layer is arranged in the filtering chamber, an electric heating net is arranged in the heating chamber, the filtering chamber and the heating chamber are communicated with each other, an air inlet is formed in the top of the air heating box, an air outlet is formed in the bottom of the air heating box, and the filtering layer specifically comprises a stainless steel filtering net and an active carbon filtering net.
As a preferred scheme, the drying air pipe is provided with an air jet hole aligned with the filter screen, and the left end of the drying air pipe is provided with a reflux valve.
As a preferred scheme, the medicament adding mechanism comprises a solvent tank which is arranged on a top panel of the treatment tank and a dropper of which extends into the settling chamber, and a feeding valve is arranged on the dropper of the solvent tank.
Preferably, the feeding mechanism comprises a feeding pump which is arranged on the top panel of the treatment box and the feeding pipe extends into the settling chamber.
As a preferred scheme, control mechanism is including setting up the control box on handling case right side panel, be provided with relay group on the inside bottom plate of control box, each group relay is respectively through the unloading valve of line connection unloading pipe, the charge valve of medicament interpolation mechanism, feed mechanism's charge pump, the draught fan and the electrical heating net of stoving mechanism and the ooff valve of outlet pipe in the relay group, be provided with the PLC controller on the right side inner wall of control box, the control scheme of each group relay is connected the PLC controller respectively in the relay group.
Compared with the prior art, the utility model has the beneficial effects that: the treatment box is internally provided with the settling chamber and the filtering chamber, wherein the feeding mechanism and the medicament adding mechanism arranged on the settling chamber are synchronously opened and closed, so that the addition of treatment medicaments is realized while adding the Grignard residues, the Grignard residues and the medicaments are mixed, the Grignard residues are introduced into the filtering chamber when the precipitation time reaches, the solid-liquid separation of the Grignard residues can be realized by the filtering screen arranged in the filtering chamber, after liquid is discharged, the solid intercepted on the filtering screen is dried by the drying mechanism, the pipelined treatment of the Grignard residues is realized, time relays are adopted by all relays of a relay group in a control mechanism of the device, the intelligent control of the treatment device is realized under the control of a PLC (programmable logic controller), and the device is suitable for popularization and use.
Drawings
Fig. 1 is a schematic diagram of the overall structure of a safe, unmanned, intelligent and efficient grignard residue treatment device.
In the figure: 1. a treatment tank; 101. a settling chamber; 102. a filtering chamber; 103. a water outlet pipe; 104. an on-off valve; 105. a discharging pipe; 106. removing impurities; 2. an air heating box; 201. a filtering chamber; 202. a heating chamber; 203. a filter layer; 204. an electrical heating grid; 205. an induced draft fan; 206. drying the air pipe; 207. a reflux valve; 208. a gas injection hole; 3. a filter screen; 4. a feed pump; 5. a solvent tank; 501. a dropper; 6. a control box; 601. a relay group; 602. a PLC controller.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention is described in further detail below with reference to the accompanying drawings and embodiments. It should be understood that the specific embodiments described herein are merely illustrative of the utility model and are not intended to limit the utility model.
It will be understood that when an element is referred to as being "secured to" or "disposed on" another element, it can be directly on the other element or be indirectly on the other element. When an element is referred to as being "connected to" another element, it can be directly connected to the other element or be indirectly connected to the other element.
In the description of the present invention, it is to be understood that the terms "length", "width", "upper", "lower", "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outer", and the like, indicate orientations or positional relationships based on the orientations or positional relationships illustrated in the drawings, and are used merely for convenience in describing the present invention and for simplicity in description, and do not indicate or imply that the devices or elements referred to must have a particular orientation, be constructed in a particular orientation, and be operated, and thus, are not to be construed as limiting the present invention.
Furthermore, the terms "first", "second" and "first" are used for descriptive purposes only and are not to be construed as indicating or implying relative importance or implicitly indicating the number of technical features indicated. Thus, a feature defined as "first" or "second" may explicitly or implicitly include one or more of that feature. In the description of the present invention, "a plurality" means two or more unless specifically defined otherwise.
For better understanding of the above technical solutions, the following detailed descriptions will be provided in conjunction with the drawings and the detailed description of the present invention.
Example (b):
referring to fig. 1, the present embodiment provides a technical solution:
a safe, unmanned, intelligent and efficient Grignard residue treatment device comprises a treatment box 1, a drying mechanism arranged on a left panel of the treatment box 1 and a control mechanism arranged on a right panel of the treatment box 1, wherein a sedimentation chamber 101 and a filtering chamber 102 are sequentially arranged in the treatment box 1 from top to bottom, a bottom plate of the sedimentation chamber 101 is provided with a blanking pipe 105 communicated with the filtering chamber 102, the blanking pipe 105 is provided with a blanking valve, a top plate of the sedimentation chamber 101 is sequentially provided with a medicament adding mechanism and a feeding mechanism from left to right, the filtering chamber 102 is internally provided with a filtering mechanism, the right inner wall of the right side of the filtering chamber 102 is provided with a impurity removing port 106 on the right side of a filtering screen 3, the impurity removing port 106 is provided with an end cover, the right side of the bottom of the filtering chamber 102 is provided with a water outlet pipe 103 extending out of the treatment box 1, and the water outlet pipe 103 is provided with a switch valve 104;
wherein, the filtering mechanism is a filter screen 3 arranged on the inner wall of the middle part of the filtering chamber 102;
the drying mechanism comprises an air heating box 2 and an induced draft fan 205 which are arranged on a left side panel of the processing box 1, an air exhaust pipe of the induced draft fan 205 is connected with an air outlet of the air heating box 2, an air supply pipe of the induced draft fan 205 is connected with a drying air pipe 206 which is arranged on a bottom plate of a filtering chamber 102, a filtering chamber 201 and a heating chamber 202 are sequentially arranged in the air heating box 2 from top to bottom, a filtering layer 203 is arranged in the filtering chamber 201, an electric heating net 204 is arranged in the heating chamber 202, the filtering chamber 201 and the heating chamber 202 are mutually communicated, an air inlet is arranged at the top of the air heating box 2, an air outlet is arranged at the bottom of the air heating box 2, the filtering layer 203 specifically comprises a stainless steel filtering net and an active carbon filtering net, an air injection hole 208 which is aligned with the filtering net 3 is arranged on the drying air pipe 206, and a reverse flow valve 207 is arranged at the left end of the drying air pipe 206;
the medicament adding mechanism comprises a solvent box 5 which is arranged on the top panel of the treatment box 1, a dropper 501 extends into the settling chamber 101, and a charging valve is arranged on the dropper 501 of the solvent box 5;
wherein the feeding mechanism comprises a feeding pump 4 which is arranged on the top panel of the treatment box 1 and the feeding pipe extends into the settling chamber 101;
wherein, control mechanism is including setting up the control box 6 on handling case 1 right side panel, be provided with relay group 601 on the inside bottom plate of control box 6, each group relay is respectively through the unloading valve of line connection unloading pipe 105 in relay group 601, the charge valve of medicament interpolation mechanism, feed mechanism's charge pump 4, drying mechanism's draught fan 205 and electric heating net 204 and outlet pipe 103's ooff valve 104, be provided with PLC controller 602 on the right side inner wall of control box 6, each group relay's in relay group 601 control circuit is connected PLC controller 602 respectively.
The working principle is as follows: the treatment box is internally provided with the settling chamber and the filtering chamber, wherein the feeding mechanism and the medicament adding mechanism arranged on the settling chamber are synchronously opened and closed, so that the addition of treatment medicaments is realized while adding the Grignard residues, the Grignard residues and the medicaments are mixed, the Grignard residues are introduced into the filtering chamber when the precipitation time reaches, the solid-liquid separation of the Grignard residues can be realized by the filtering screen arranged in the filtering chamber, after liquid is discharged, the solid intercepted on the filtering screen is dried by the drying mechanism, the pipelined treatment of the Grignard residues is realized, time relays are adopted by all relays of a relay group in a control mechanism of the device, the intelligent control of the treatment device is realized under the control of a PLC (programmable logic controller), and the device is suitable for popularization and use.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the utility model, the scope of which is defined in the appended claims and their equivalents.

Claims (9)

1. The utility model provides a safe unmanned intelligent efficient processing apparatus of grignard's residue, is including handling case (1), setting drying mechanism and the control mechanism of setting on handling case (1) right side panel on handling case (1) left side panel, its characterized in that: handle case (1) inside from last deposit room (101) and filter chamber (102) down having set gradually, be provided with unloading pipe (105) of intercommunication filter chamber (102) on the bottom plate of deposit room (101), be provided with the unloading valve on unloading pipe (105), turn right from a left side and set gradually medicament interpolation mechanism and feed mechanism on the roof of deposit room (101), filter chamber (102) inside is provided with filtering mechanism, filtering mechanism specifically is filter screen (3) of setting on filter chamber (102) middle part inner wall.
2. The safe, unmanned, intelligent and efficient Grignard residue treatment device according to claim 1, wherein: and a impurity removing port (106) is formed in the right side inner wall of the filtering chamber (102) and on the right side of the filtering net (3), and an end cover is arranged on the impurity removing port (106).
3. The safe, unmanned, intelligent and efficient Grignard residue treatment device according to claim 1, wherein: a water outlet pipe (103) extending out of the treatment box (1) is arranged on the right side of the bottom of the filtering chamber (102), and a switch valve (104) is arranged on the water outlet pipe (103).
4. The safe, unmanned, intelligent and efficient Grignard residue treatment device according to claim 1, wherein: drying mechanism is including setting up air heating case (2) and draught fan (205) on handling case (1) left side panel, the gas outlet of air heating case (2) is connected to the exhaust tube of draught fan (205), dry trachea (206) that set up on filter chamber (102) bottom plate are connected to the air supply pipe of draught fan (205).
5. The safe, unmanned, intelligent and efficient Grignard residue treatment device according to claim 4, wherein: air heating case (2) is inside from last down set gradually filter chamber (201) and heating chamber (202), filter chamber (201) is inside to be provided with filter layer (203), heating chamber (202) is inside to be provided with electric heating net (204), communicate each other between filter chamber (201) and heating chamber (202), air heating case (2) top is provided with the air inlet, air heating case (2) bottom is provided with the gas outlet, filter layer (203) specifically includes stainless steel filter screen and active carbon filter screen.
6. The safe, unmanned, intelligent and efficient Grignard residue treatment device according to claim 4, wherein: the drying air pipe (206) is provided with an air injection hole (208) aligned with the filter screen (3), and the left end of the drying air pipe (206) is provided with a reflux valve (207).
7. The safe, unmanned, intelligent and efficient Grignard residue treatment device according to claim 1, wherein: the medicament adding mechanism comprises a solvent box (5) which is arranged on a top panel of the treatment box (1) and a dropper (501) extends into the settling chamber (101), and a charging valve is arranged on the dropper (501) of the solvent box (5).
8. The safe, unmanned, intelligent and efficient Grignard residue treatment device according to claim 1, wherein: the feeding mechanism comprises a feeding pump (4) which is arranged on the top panel of the treatment box (1) and the feeding pipe extends into the settling chamber (101).
9. The safe, unmanned, intelligent and efficient Grignard residue treatment device according to claim 1, wherein: control mechanism is including setting up control box (6) on handling case (1) right side panel, be provided with relay group (601) on the inside bottom plate of control box (6), each group relay adds charge valve, feed mechanism's charge pump (4), drying mechanism's draught fan (205) and electric heating net (204) and outlet pipe (103) through the unloading valve of line connection unloading pipe (105), medicament respectively in relay group (601), be provided with PLC controller (602) on the right side inner wall of control box (6), PLC controller (602) are connected respectively to the control scheme of each group relay in relay group (601).
CN202122182378.6U 2021-09-09 2021-09-09 Safe, unmanned, intelligent and efficient treatment device for Grignard residues Active CN215466998U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202122182378.6U CN215466998U (en) 2021-09-09 2021-09-09 Safe, unmanned, intelligent and efficient treatment device for Grignard residues

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202122182378.6U CN215466998U (en) 2021-09-09 2021-09-09 Safe, unmanned, intelligent and efficient treatment device for Grignard residues

Publications (1)

Publication Number Publication Date
CN215466998U true CN215466998U (en) 2022-01-11

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ID=79768746

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202122182378.6U Active CN215466998U (en) 2021-09-09 2021-09-09 Safe, unmanned, intelligent and efficient treatment device for Grignard residues

Country Status (1)

Country Link
CN (1) CN215466998U (en)

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