CN215139864U - Chlorobenzoic acid processing is with reation kettle of being convenient for inside clearance based on iodine - Google Patents

Chlorobenzoic acid processing is with reation kettle of being convenient for inside clearance based on iodine Download PDF

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Publication number
CN215139864U
CN215139864U CN202121095409.8U CN202121095409U CN215139864U CN 215139864 U CN215139864 U CN 215139864U CN 202121095409 U CN202121095409 U CN 202121095409U CN 215139864 U CN215139864 U CN 215139864U
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reaction kettle
iodine
chlorobenzoic acid
convenient
processing
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CN202121095409.8U
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袁海军
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Jiangsu Hengzhou Chemical Co ltd
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Jiangsu Hengzhou Chemical Co ltd
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Abstract

The utility model discloses a reation kettle convenient for internal cleaning for processing chlorobenzoic acid based on iodine, which comprises a reaction kettle body, wherein a charging hole is welded above the reaction kettle body, a scraper blade is movably arranged outside a stirring rod, two sides above the scraper blade are both connected with telescopic rods, and the upper part of each telescopic rod is in threaded connection with a driving hydraulic cylinder; the liquid storage tank is fixedly arranged at the rear end of the reaction kettle body, and a conveying pipe is arranged inside the liquid storage tank. This reation kettle of chlorobenzoic acid processing with being convenient for inside clearance based on iodine drives the scraper blade through the telescopic link and carries out the removal of direction from top to bottom, can strike off the coagulum of reation kettle internal wall through reciprocating of scraper blade to can be convenient for clear up it, avoid the reation kettle of chlorobenzoic acid processing usefulness of iodine after long-time the use, the cubic coagulum of its inner wall adhesion is difficult to wash away with the water, can influence going on of chemical reaction backward in the existence reation kettle.

Description

Chlorobenzoic acid processing is with reation kettle of being convenient for inside clearance based on iodine
Technical Field
The utility model relates to a reation kettle technical field specifically is a reation kettle of being convenient for inside clearance is used in chlorobenzoic acid processing based on iodine.
Background
Iodine is a non-metallic element, and the elementary iodine is a purple black crystal, is easy to sublimate, is easy to desublimate after sublimation, and has toxicity and corrosivity. The method is mainly used for preparing medicines, dyes, iodine, test paper, iodine compounds and the like, the chlorobenzoic acid is a white powdery chemical, and a reaction kettle for processing the chlorobenzoic acid based on iodine is needed during the processing of the chlorobenzoic acid of the iodine.
After the existing reaction kettle for processing the chlorobenzoic acid based on iodine is used for a long time, the inner wall of the reaction kettle is usually adhered with blocky coagulants, the coagulants are difficult to flush with water directly, and the subsequent chemical reaction is influenced in the reaction kettle.
SUMMERY OF THE UTILITY MODEL
An object of the utility model is to provide a reation kettle of chlorobenzoic acid processing usefulness convenient to inside clearance based on iodine to the suggestion is in solving above-mentioned background art because the reation kettle of current chlorobenzoic acid processing usefulness based on iodine uses the back for a long time, and its inner wall can the cubic coagulum of adhesion usually, and direct water is difficult to wash it off, can influence the problem of going on of chemical reaction backward in the reation kettle.
In order to achieve the above object, the utility model provides a following technical scheme: the utility model provides an iodine-based reation kettle of chlorobenzoic acid processing with being convenient for inside clearance, includes:
the reaction kettle comprises a reaction kettle body, wherein a charging hole is welded above the reaction kettle body, a driving motor is installed in the middle of the charging hole, a rotating shaft is connected below the driving motor in a threaded manner, and a stirring rod is welded on the outer wall of the rotating shaft;
the scraper is movably arranged on the outer side of the stirring rod, telescopic rods are connected to two sides above the scraper, and a driving hydraulic cylinder is connected to the upper portion of each telescopic rod in a threaded mode;
the liquid storage tank is fixedly arranged at the rear end of the reaction kettle body, and a conveying pipe is arranged in the liquid storage tank;
the discharge port is formed below the reaction kettle body, and the right side of the discharge port is connected with a discharging pipe;
the sample connection, it is seted up the left side of discharge gate, the control flange is installed in the outside of sample connection.
Preferably, the driving motor forms a rotating structure through the rotating shaft and the stirring rods, and the stirring rods are uniformly distributed along the outer wall of the rotating shaft.
Preferably, the driving hydraulic cylinder forms a telescopic structure through the telescopic rod and the scraper, and the scraper is of a circular ring structure.
Preferably, the diameter of the scraper is consistent with the diameter of the inner wall of the reaction kettle body, and the liquid storage tank forms a communicating structure with the reaction kettle body through the conveying pipe.
Preferably, the sampling port is further provided with:
and the fixed plates are fixedly arranged on two sides below the sampling port, and the inner sides of the fixed plates are movably provided with limiting frames.
Preferably, a sliding structure is formed between the limiting frame and the fixing plate, and the fixing plate is symmetrically distributed about the vertical center line of the limiting frame.
Preferably, the limit frame is further provided with:
the sampling beaker is arranged inside the limiting frame, and a semi-surrounding structure is formed between the limiting frame and the sampling beaker.
Compared with the prior art, the utility model provides a processing of chlorobenzoic acid is with reation kettle of being convenient for inside clearance based on iodine possesses following beneficial effect: this reation kettle of chlorobenzoic acid processing with inside clearance of being convenient for based on iodine can drive the removal of scraper blade direction from top to bottom through the telescopic link, can strike off the coagulum of reation kettle internal wall through reciprocating of scraper blade to can be convenient for clear up it.
1. The driving motor arranged in the utility model can drive the stirring rod to rotate through the rotating shaft, the rotating stirring rod can mix and stir chemicals in the reaction kettle body, thereby promoting the reaction, the liquid storage tank can store the cleaning liquid, the cleaning liquid can be conveyed into the reaction kettle body through the conveying pipe, thereby cleaning and soaking the reaction kettle, the driving hydraulic cylinder can drive the scraper blade to move up and down through the telescopic rod, the coagulated substances on the inner wall of the reaction kettle body can be scraped through the up-and-down movement of the scraper blade, thereby being convenient to clean, avoiding the problems that after the existing reaction kettle for processing the chlorobenzoic acid based on iodine is used for a long time, usually, the inner wall of the reaction kettle is adhered with blocky coagulants which are difficult to flush by water directly, so that the problem that the chemical reaction in the reaction kettle is influenced later is solved;
2. the utility model can facilitate the outflow of the sample through the sampling port, can hold the outflowing sample through the sampling beaker, and can play a limiting effect on the sampling beaker through the limiting frame, thereby ensuring the stability of the sampling beaker in the sampling process;
3. the utility model discloses there is the groove with the mutual block of spacing frame in the fixed plate inboard that sets up to can be convenient for spacing frame slide from top to bottom, and then can be convenient for adjust the position of sample beaker, can be convenient for simultaneously take and put of sample beaker.
Drawings
FIG. 1 is a schematic view of the overall structure of the present invention;
FIG. 2 is a schematic view of the internal structure of the present invention;
FIG. 3 is a schematic diagram of the structure of the reaction kettle body of the present invention as seen from the right;
FIG. 4 is a schematic structural view of the scraper of the present invention;
fig. 5 is an enlarged schematic view of a portion a in fig. 2 according to the present invention.
In the figure: 1. a reaction kettle body; 2. a rotating shaft; 3. a stirring rod; 4. driving the hydraulic cylinder; 5. a telescopic rod; 6. a squeegee; 7. a drive motor; 8. a feed inlet; 9. a discharge port; 10. a discharging pipe; 11. a liquid storage tank; 12. a delivery pipe; 13. a sampling port; 14. sampling a beaker; 15. a control flange; 16. a fixing plate; 17. and a limiting frame.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
Referring to fig. 1-3, an iodine-based chlorobenzoic acid processing reactor for internal cleaning comprises: the reaction kettle comprises a reaction kettle body 1, wherein a feed inlet 8 is welded above the reaction kettle body 1, a driving motor 7 is installed in the middle of the feed inlet 8, a rotating shaft 2 is connected to the lower portion of the driving motor 7 in a threaded mode, and a stirring rod 3 is welded to the outer wall of the rotating shaft 2; the driving motor 7 forms a rotating structure with the stirring rod 3 through the rotating shaft 2, and the stirring rod 3 is uniformly distributed along the outer wall of the rotating shaft 2; the driving motor 7 that sets up can drive the stirring rod 3 through axis of rotation 2 and rotate, and pivoted stirring rod 3 can mix the stirring to the chemicals in the reation kettle cauldron body 1 to can promote going on of its reaction.
Referring to fig. 2 and 4-5, an iodine-based chlorobenzoic acid processing reactor for easy internal cleaning comprises: the scraping plate 6 is movably arranged on the outer side of the stirring rod 3, telescopic rods 5 are connected to two sides above the scraping plate 6, and a driving hydraulic cylinder 4 is connected to the upper portion of each telescopic rod 5 in a threaded mode; the driving hydraulic cylinder 4 forms a telescopic structure through the telescopic rod 5 and the scraper 6, and the scraper 6 is in a circular structure; the driving hydraulic cylinder 4 can drive the scraper 6 to move up and down through the telescopic rod 5, and coagulants on the inner wall of the reaction kettle body 1 can be scraped through the up-and-down movement of the scraper 6, so that the cleaning of the reaction kettle can be facilitated, and the problems that after the existing reaction kettle for processing chlorobenzoic acid based on iodine is used for a long time, the inner wall of the reaction kettle is usually adhered with blocky coagulants, the coagulants are difficult to wash away by direct water, and the proceeding of the backward chemical reaction in the reaction kettle is influenced are solved; the discharge port 9 is arranged below the reaction kettle body 1, and the right side of the discharge port 9 is connected with a discharging pipe 10; a sampling port 13 arranged on the left side of the discharge port 9, and a control flange 15 is arranged on the outer side of the sampling port 13; the outflow of the sample can be facilitated through the sampling port 13; the fixed plate 16 is fixedly arranged at two sides below the sampling port 13, and the inner side of the fixed plate 16 is movably provided with a limit frame 17; a sliding structure is formed between the limiting frame 17 and the fixing plate 16, and the fixing plate 16 is symmetrically distributed about the vertical center line of the limiting frame 17; the sampling beaker 14 is arranged inside the limit frame 17, and a semi-surrounding structure is formed between the limit frame 17 and the sampling beaker 14; the flowing sample can be contained through the sampling beaker 14, and the limiting frame 17 can play a limiting effect on the sampling beaker 14, so that the stability of the sampling beaker 14 in the sampling process can be ensured; the fixed plate 16 inboard that sets up has the groove with the mutual block of spacing frame 17 to can be convenient for spacing frame 17 slide from top to bottom, and then can be convenient for adjust the position of sample beaker 14, can be convenient for simultaneously take and put of sample beaker 14.
Referring to fig. 3, a reaction vessel for processing chlorobenzoic acid based on iodine, which is convenient for internal cleaning, comprises: the liquid storage tank 11 is fixedly arranged at the rear end of the reaction kettle body 1, and a conveying pipe 12 is arranged in the liquid storage tank 11; the diameter of the scraper 6 is consistent with that of the inner wall of the reaction kettle body 1, and the liquid storage tank 11 and the reaction kettle body 1 form a communicating structure through the conveying pipe 12; the liquid reserve tank 11 can save the cleaning liquid, can carry the cleaning liquid to the reation kettle cauldron body 1 in through conveyer pipe 12 to can wash it and soak.
The working principle is as follows: when the reaction kettle convenient for cleaning the interior of the iodine-based chlorobenzoic acid is used for processing chlorobenzoic acid, firstly, chemicals and water which are needed to be used are injected into the reaction kettle body 1 through the feed inlet 8, then the driving motor 7 is started, the driving motor 7 drives the stirring rod 3 to rotate through the rotating shaft 2, and the rotating stirring rod 3 can mix and stir the chemicals in the reaction kettle body 1 to promote the reaction; secondly, in the reaction process, the reactant is required to be sampled to judge the reaction degree of the reactant, the sampling beaker 14 is firstly placed on the inner side of the limit frame 17, then the limit frame 17 and the sampling beaker 14 move upwards through the fixing plate 16 until the sampling beaker 14 moves upwards to the sampling port 13, and the limit frame 17 is fixed by using a bolt; then, the control flange 15 is opened, chemicals in the reaction kettle body 1 can flow into the sampling beaker 14 through the sampling port 13, then the control flange 15 is closed to prevent excessive outflow of materials, the limiting frame 17 and the sampling beaker 14 move downwards through the fixing plate 16, the sampling beaker 14 is taken out of the limiting frame 17, and then the substances in the sampling beaker 14 can be detected to judge whether the reaction is finished; finally, after the reaction is finished, discharging the materials through a discharge port 9 and a blanking pipe 10, cleaning the reaction kettle body 1, conveying the cleaning liquid in the liquid storage tank 11 into the reaction kettle body 1 through a conveying pipe 12, cleaning and soaking the waste water, starting the driving hydraulic cylinder 4, driving the driving hydraulic cylinder 4 to drive the scraper 6 to move up and down through the telescopic rod 5, the coagulated material on the inner wall of the reaction kettle body 1 can be scraped by the up-and-down movement of the scraper 6, the cleaning effect can be achieved, the scraped residue can be communicated with the cleaning liquid to flow out from the discharge hole 9, the reaction kettle for processing the chlorobenzoic acid containing iodine is prevented from being used for a long time, the lumpy coagula adhered on the inner wall of the reaction kettle is difficult to wash away by water, the chemical reaction in the reaction kettle can be influenced, the working principle of the reaction kettle convenient for cleaning the interior of the reaction kettle for processing the chlorobenzoic acid based on the iodine is shown.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims (7)

1. The utility model provides a reation kettle of interior clearance of being convenient for is used in chlorobenzoic acid processing based on iodine which characterized in that includes:
the reaction kettle comprises a reaction kettle body (1), wherein a feed inlet (8) is welded above the reaction kettle body (1), a driving motor (7) is installed in the middle of the feed inlet (8), a rotating shaft (2) is connected to the lower portion of the driving motor (7) in a threaded mode, and a stirring rod (3) is welded to the outer wall of the rotating shaft (2);
the scraping plate (6) is movably arranged on the outer side of the stirring rod (3), telescopic rods (5) are connected to two sides above the scraping plate (6), and a driving hydraulic cylinder (4) is connected to the upper portion of each telescopic rod (5) in a threaded mode;
the liquid storage tank (11) is fixedly arranged at the rear end of the reaction kettle body (1), and a conveying pipe (12) is arranged in the liquid storage tank (11);
the discharge port (9) is arranged below the reaction kettle body (1), and the right side of the discharge port (9) is connected with a discharge pipe (10);
the sampling opening (13) is arranged on the left side of the discharge opening (9), and a control flange (15) is installed on the outer side of the sampling opening (13).
2. The reaction kettle for processing chlorobenzoic acid based on iodine as claimed in claim 1, wherein the driving motor (7) forms a rotating structure with the stirring rod (3) through the rotating shaft (2), and the stirring rod (3) is evenly distributed along the outer wall of the rotating shaft (2).
3. The reaction kettle convenient for internal cleaning for processing chlorobenzoic acid based on iodine as claimed in claim 1, wherein the driving hydraulic cylinder (4) forms a telescopic structure with the scraper (6) through a telescopic rod (5), and the scraper (6) is in a circular ring structure.
4. The reaction kettle for processing chlorobenzoic acid based on iodine, which is convenient for internal cleaning, as claimed in claim 1, wherein the diameter of the scraper (6) is consistent with the diameter of the inner wall of the reaction kettle body (1), and the liquid storage tank (11) is communicated with the reaction kettle body (1) through the delivery pipe (12).
5. The reaction kettle for processing chlorobenzoic acid based on iodine as claimed in claim 1, wherein the sampling port (13) is further provided with:
and the fixing plates (16) are fixedly arranged on two sides below the sampling port (13), and the inner sides of the fixing plates (16) are movably provided with limiting frames (17).
6. The reaction kettle for processing chlorobenzoic acid based on iodine as claimed in claim 5, wherein a sliding structure is formed between the limiting frame (17) and the fixing plate (16), and the fixing plate (16) is symmetrically distributed about the vertical center line of the limiting frame (17).
7. The reaction kettle for processing chlorobenzoic acid based on iodine as claimed in claim 5, wherein the limiting frame (17) is further provided with:
a sampling beaker (14) which is arranged inside the limit frame (17), and a semi-surrounding structure is formed between the limit frame (17) and the sampling beaker (14).
CN202121095409.8U 2021-05-21 2021-05-21 Chlorobenzoic acid processing is with reation kettle of being convenient for inside clearance based on iodine Active CN215139864U (en)

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CN202121095409.8U CN215139864U (en) 2021-05-21 2021-05-21 Chlorobenzoic acid processing is with reation kettle of being convenient for inside clearance based on iodine

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CN202121095409.8U CN215139864U (en) 2021-05-21 2021-05-21 Chlorobenzoic acid processing is with reation kettle of being convenient for inside clearance based on iodine

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114849616A (en) * 2022-06-02 2022-08-05 江苏瑞佳食品添加剂有限公司 Reaction unit of plasticizer

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114849616A (en) * 2022-06-02 2022-08-05 江苏瑞佳食品添加剂有限公司 Reaction unit of plasticizer

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