CN215028009U - Equipment of drawing of ceramic porous material based on MOFs - Google Patents
Equipment of drawing of ceramic porous material based on MOFs Download PDFInfo
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- CN215028009U CN215028009U CN202121030652.1U CN202121030652U CN215028009U CN 215028009 U CN215028009 U CN 215028009U CN 202121030652 U CN202121030652 U CN 202121030652U CN 215028009 U CN215028009 U CN 215028009U
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- extraction
- mofs
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- ceramic porous
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Abstract
The utility model discloses a ceramic porous material's extraction equipment based on MOFs, including drawing the jar and drawing the lid, draw the lid and set up in drawing the tank deck portion, draw the fixed intercommunication in lid top portion and have at least two sets of inlet pipes, two sets of all install first valve on the inlet pipe, draw the jar and draw the junction of lid and be provided with seal assembly, the utility model discloses through setting up filter tank, recess, first filter screen board and second filter screen board and cooperating the use, throw into ceramic powder and metal organic framework material in drawing the jar, stir and make its misce bene, add dispersant to the mixture again, add the binder after the misce bene and continue the ball-milling, obtain metal organic framework-ceramic composite thick liquids enter first filter screen board and second filter screen board and filter, carry a large amount of tiny particulate matter in the metal organic framework-ceramic composite thick liquids and filter and hold back, and the effect of fine particles on the formation of the ceramic porous material of the MOFs in the later period is prevented.
Description
Technical Field
The utility model relates to an extract equipment technical field, specifically be a ceramic porous material's equipment of extracting based on MOFs.
Background
The preparation method of the MOFs-based ceramic porous material comprises the following steps: preparing a metal organic framework material by taking a metal precursor and an organic ligand as raw materials; dispersing zirconium salt in a solvent, stirring and mixing to generate transparent gel, sealing and aging for a period of time, and drying to obtain xerogel; calcining the dried gel at high temperature, and performing ball milling to obtain ceramic powder; dispersing ceramic powder and a metal organic framework material in a solvent, and stirring to uniformly mix the ceramic powder and the metal organic framework material, wherein the addition amount of the metal organic framework material is 30-70 wt% of the ceramic powder; adding a dispersing agent into the mixture, adding a binder after ball milling is uniform, and continuing ball milling to obtain metal organic framework-ceramic composite slurry; pouring the metal organic framework-ceramic composite slurry into a forming mold, and drying to obtain a ceramic blank; and calcining the ceramic blank at a high temperature to obtain the MOFs-based ceramic porous material.
However, a large amount of fine particles can be carried in the metal organic framework-ceramic composite slurry obtained in the preparation of the MOFs-based ceramic porous material, so that the effect is influenced; also can cause the blockage of the discharge hole and limit the application of the extraction equipment.
For this reason, we need to provide an extraction device of ceramic porous materials based on MOFs to solve the above problems.
SUMMERY OF THE UTILITY MODEL
An object of the utility model is to provide a ceramic porous material's equipment of drawing based on MOFs, metal organic framework-ceramic composite slurry gets into first filter screen board and the second filters the otter board and filters, smugglies a large amount of tiny particulate matters secretly in the composite slurry with metal organic framework-ceramic and filters and hold back, prevents that tiny particulate matters from influencing the effect that later stage MOFs's ceramic porous material formed to solve the problem that proposes in the above-mentioned background art.
In order to achieve the above object, the utility model provides a following technical scheme: an extraction device of ceramic porous materials based on MOFs comprises an extraction tank and an extraction cover, wherein the extraction cover is arranged on the top of the extraction tank, the top of the extraction cover is fixedly communicated with at least two groups of inlet pipes, a first valve is arranged on each of the two groups of inlet pipes, a sealing assembly is arranged at the joint of the extraction tank and the extraction cover, a stirring mechanism is arranged on the top of the extraction cover, the bottom of the extraction tank is fixedly communicated with a filter tank, grooves are formed in the two sides of the filter tank, springs are fixedly connected in the two groups of grooves, one end of each spring is fixedly connected with a connecting plate, a first filter screen plate and a second filter screen plate are sequentially distributed between the two groups of connecting plates according to the hole diameter, an electric push rod is fixedly connected to one side of one group of connecting plates, a push block is fixedly connected to an output rod of the electric push rod, and a block is fixedly connected to one side of the other group of connecting plates, one side of the push block is mutually abutted against one side of the abutting block, the bottom of the filter tank is fixedly communicated with a discharge pipe, and a second valve is mounted on the discharge pipe.
Preferably, the sealing assembly comprises a sealing block and a rubber sleeve, the sealing block is inserted in the joint of the extracting tank and the extracting cover, a clamping groove is formed in the sealing block, the rubber sleeve is arranged in the clamping groove, and the rubber sleeve is clamped in the joint of the extracting tank and the extracting cover.
Preferably, two groups of inserting blocks are fixedly connected to one side of the sealing block, slots are formed in the side walls of the extracting tank and the extracting cover, the inserting blocks are inserted into the slots, and a handle is fixedly mounted on the other side of the sealing block.
Preferably, rabbling mechanism includes motor, pivot and puddler, motor fixed mounting is in drawing the caping portion, pivot one end is run through and is drawn the output shaft fixed connection of caping portion and motor, the puddler equidistance distributes in the pivot.
Preferably, the output shaft end of pivot one end and motor passes through shaft coupling fixed connection, the equidistance distributes in the pivot has fixed cover, the puddler distributes in fixed cover a week.
Preferably, the connecting plate both ends are the equal fixedly connected with slider, the spout has all been seted up to both sides in the recess, slider sliding connection is in the spout.
Compared with the prior art, the beneficial effects of the utility model are that:
1. the utility model discloses a set up filter tank, recess, first filter screen board and second filter screen board cooperation use, drop into ceramic powder and metal organic framework material and draw in the jar, stir and make its misce bene, add the dispersant to the mixture again, add the binder after the stirring and continue the ball-milling, the compound thick liquids that obtains metal organic framework-pottery enter first filter screen board and second filter screen board and filter, carry a large amount of tiny particulate matters in the compound thick liquids of metal organic framework-pottery and carry out the filtration and hold back, prevent that tiny particulate matters from influencing the effect that the ceramic porous material of later stage MOFs formed;
2. through the arrangement of the springs, the connecting plate, the electric push rod, the push block and the abutting block, after the first filter screen plate and the second filter screen plate filter the metal organic framework-ceramic composite slurry, the electric push rod is started to drive the push block to move towards the abutting block and further abut against the abutting block, so that the springs compress back and forth, the first filter screen plate and the second filter screen plate vibrate, the discharging pipe cannot be blocked, and the application of the extraction equipment is improved.
Drawings
FIG. 1 is a schematic sectional view of the present invention;
FIG. 2 is a schematic structural view of the present invention;
fig. 3 is an enlarged schematic structural view of a portion a in fig. 1 according to the present invention.
Fig. 4 is a schematic structural view of the filter tank of the present invention.
In the figure: 1. an extraction tank; 2. an extraction cover; 3. a seal assembly; 4. a sealing block; 401. a card slot; 5. a rubber sleeve; 6. a handle; 7. inserting a block; 8. a slot; 9. a stirring mechanism; 10. a motor; 11. a rotating shaft; 12. a stirring rod; 13. fixing a sleeve; 14. a feed pipe; 15. a first valve; 16. a filter tank; 1601. a groove; 17. a spring; 18. a connecting plate; 19. a first filter screen plate; 20. a second filter screen plate; 21. an electric push rod; 22. a push block; 23. a resisting block; 24. a second valve; 25. and (4) discharging the pipe.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
Referring to fig. 1-4, the present invention provides a technical solution: a ceramic porous material extraction device based on MOFs comprises an extraction tank 1 and an extraction cover 2, wherein the extraction cover 2 is arranged at the top of the extraction tank 1, the top of the extraction cover 2 is fixedly communicated with at least two groups of inlet pipes 14, each group of inlet pipes 14 is provided with a first valve 15, a sealing assembly 3 is arranged at the joint of the extraction tank 1 and the extraction cover 2, each sealing assembly 3 comprises a sealing block 4 and a rubber sleeve 5, each sealing block 4 is inserted outside the joint of the extraction tank 1 and the extraction cover 2, each sealing block 4 is internally provided with a clamping groove 401, each rubber sleeve 5 is arranged in each clamping groove 401, each rubber sleeve 5 is clamped outside the joint of the extraction tank 1 and the extraction cover 2, one side of each sealing block 4 is fixedly connected with two groups of insertion blocks 7, the side walls of the extraction tank 1 and the extraction cover 2 are respectively provided with a slot 8, each insertion block 7 is inserted in each slot 8, the other side of each sealing block 4 is fixedly provided with a handle 6, each rubber sleeve 5 can be clamped outside the joint of the extraction tank 1 and the extraction cover 2, the sealing block 4 is inserted outside the joint of the extraction tank 1 and the extraction cover 2, so that the sealing performance between the joint of the extraction tank 1 and the extraction cover 2 is improved;
the top of the extraction cover 2 is provided with a stirring mechanism 9, the stirring mechanism 9 comprises a motor 10, a rotating shaft 11 and a stirring rod 12, the motor 10 is fixedly installed at the top of the extraction cover 2, one end of the rotating shaft 11 penetrates through the top of the extraction cover 2 and is fixedly connected with the output shaft of the motor 10, the stirring rods 12 are equidistantly distributed on the rotating shaft 11, one end of the rotating shaft 11 is fixedly connected with the output shaft end of the motor 10 through a coupler, fixing sleeves 13 are equidistantly distributed on the rotating shaft 11, the stirring rods 12 are distributed on the periphery of the fixing sleeves 13, the coupler is arranged so that one end of the rotating shaft 11 and the output shaft end of the motor 10 can be connected more stably, and the fixing sleeves 13 are arranged so that the stirring rods 12 can be installed and replaced;
putting ceramic powder and metal organic framework material into an extraction tank 1 from a feeding pipe 14, starting a motor 10 of a stirring mechanism 9, driving a rotating shaft 11 and a stirring rod 12 to rotate by the motor 10, stirring the ceramic powder and the metal organic framework material uniformly, turning off the motor 10, adding a dispersing agent into the mixture, then starting the motor 10 of the stirring mechanism 9 again, driving the rotating shaft 11 and the stirring rod 12 to rotate by the motor 10, adding a binder to continue rotating after uniform stirring, and obtaining metal organic framework-ceramic composite slurry;
the bottom of the extraction tank 1 is fixedly communicated with a filter tank 16, grooves 1601 are formed in two sides of the filter tank 16, springs 17 are fixedly connected into the two groups of grooves 1601, one end of each spring 17 is fixedly connected with a connecting plate 18, a first filter screen plate 19 and a second filter screen plate 20 are sequentially distributed between the two groups of connecting plates 18 according to the pore size, the metal organic framework-ceramic composite slurry enters the first filter screen plate 19 and the second filter screen plate 20 for filtration, a large number of fine particles are carried in the metal organic framework-ceramic composite slurry for filtration and interception, and the fine particles are prevented from influencing the effect of formation of ceramic porous materials of MOFs in the later period;
18 one side fixedly connected with electric putter 21 of a set of connecting plate, electric putter 21's output lever end fixedly connected with ejector pad 22, another 18 one side fixedly connected with of connecting plate support piece 23, ejector pad 22 one side with support 23 one side and contradict each other, 16 fixed intercommunications in filter-tank bottom have discharging pipe 25, install second valve 24 on the discharging pipe 25, the equal fixedly connected with slider in connecting plate 18 both ends, the spout has all been seted up to both sides in the recess 1601, slider sliding connection is in the spout, set up the structure that slider and spout cooperation were matchd, it is more smooth and easy to be convenient for connecting plate 18 to slide in recess 1601.
The working principle is as follows: when in use, the first valve 15 is opened, ceramic powder and metal organic framework materials are put into the extraction tank 1 from the feeding pipe 14, then the first valve 15 is closed, the motor 10 of the stirring mechanism 9 is started, the motor 10 works to drive the rotating shaft 11 and the stirring rod 12 to rotate, stirring the ceramic powder and the metal organic framework material to uniformly mix, turning off the motor 10, adding the dispersing agent into the mixture, starting the motor 10 of the stirring mechanism 9 again, driving the rotating shaft 11 and the stirring rod 12 to rotate by the operation of the motor 10, adding the binder to continue rotating after uniform stirring to obtain the metal organic framework-ceramic composite slurry, wherein the composite slurry can enter the first filter screen plate 19 and the second filter screen plate 20 for filtering, and filtering and intercepting a large amount of fine particles carried in the metal organic framework-ceramic composite slurry, so as to prevent the fine particles from influencing the effect of the formation of the ceramic porous materials of the MOFs at the later stage; after the first filter screen plate 19 and the second filter screen plate 20 filter the metal organic framework-ceramic composite slurry, the electric push rod 21 is started to drive the push block 22 to move towards the abutting block 23, and further abut against the abutting block 23, so that the spring 17 is compressed back and forth to drive the first filter screen plate 19 and the second filter screen plate 20 to vibrate, the discharge pipe 25 cannot be blocked, and the application of the extraction equipment is improved.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (6)
1. An equipment for extracting ceramic porous materials based on MOFs, comprising an extraction tank (1) and an extraction cover (2), characterized in that: the extraction cover (2) is arranged at the top of the extraction tank (1), the top of the extraction cover (2) is fixedly communicated with at least two sets of inlet pipes (14), the inlet pipes (14) are provided with first valves (15), the junction of the extraction tank (1) and the extraction cover (2) is provided with a sealing component (3), the top of the extraction cover (2) is provided with a stirring mechanism (9), the bottom of the extraction tank (1) is fixedly communicated with a filter tank (16), two sides of the filter tank (16) are provided with grooves (1601), two sets of grooves (1601) are formed in the grooves (1601) and are fixedly connected with springs (17), one end of each spring (17) is fixedly connected with a connecting plate (18), a first filter screen plate (19) and a second filter screen plate (20) are sequentially distributed between the two sets of connecting plates (18) according to the aperture size, one set of connecting plates (18) is fixedly connected with an electric push rod (21), the automatic feeding device is characterized in that a pushing block (22) is fixedly connected to an output rod end of the electric push rod (21), a supporting block (23) is fixedly connected to one side of the other group of connecting plates (18), one side of the pushing block (22) is abutted against one side of the supporting block (23), a discharging pipe (25) is fixedly communicated with the bottom of the filter tank (16), and a second valve (24) is installed on the discharging pipe (25).
2. An extraction plant of ceramic porous materials based on MOFs according to claim 1, characterized in that: seal assembly (3) are including sealed piece (4) and rubber sleeve (5), it is outside in the junction of drawing jar (1) and drawing lid (2) to peg graft in sealed piece (4), draw-in groove (401) have been seted up in sealed piece (4), rubber sleeve (5) set up in draw-in groove (401), rubber sleeve (5) joint is outside in the junction of drawing jar (1) and drawing lid (2).
3. An extraction plant of ceramic porous materials based on MOFs according to claim 2, characterized in that: two sets of inserted blocks (7) of sealed piece (4) one side fixedly connected with, draw jar (1) and draw lid (2) lateral wall and all seted up slot (8), inserted block (7) are pegged graft in slot (8), sealed piece (4) opposite side fixed mounting has handle (6).
4. An extraction plant of ceramic porous materials based on MOFs according to claim 1, characterized in that: rabbling mechanism (9) include motor (10), pivot (11) and puddler (12), motor (10) fixed mounting is in drawing lid (2) top, pivot (11) one end is run through and is drawn the output shaft fixed connection who covers (2) top and motor (10), puddler (12) equidistance distributes on pivot (11).
5. An extraction plant of ceramic porous materials based on MOFs according to claim 4, characterized in that: the utility model discloses a motor, including pivot (11), fixed cover (13), puddler (12), fixed cover (13) a week, pivot (11) one end and the output shaft end of motor (10) pass through shaft coupling fixed connection, equidistant distribution has fixed cover (13) in pivot (11), puddler (12) distribute in fixed cover (13).
6. An extraction plant of ceramic porous materials based on MOFs according to claim 1, characterized in that: the equal fixedly connected with slider in connecting plate (18) both ends, the spout has all been seted up to both sides in recess (1601), slider sliding connection is in the spout.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202121030652.1U CN215028009U (en) | 2021-05-14 | 2021-05-14 | Equipment of drawing of ceramic porous material based on MOFs |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202121030652.1U CN215028009U (en) | 2021-05-14 | 2021-05-14 | Equipment of drawing of ceramic porous material based on MOFs |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN215028009U true CN215028009U (en) | 2021-12-07 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202121030652.1U Active CN215028009U (en) | 2021-05-14 | 2021-05-14 | Equipment of drawing of ceramic porous material based on MOFs |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN215028009U (en) |
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2021
- 2021-05-14 CN CN202121030652.1U patent/CN215028009U/en active Active
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