CN214863562U

CN214863562U - Environment-friendly sulfonation reaction device

Info

Publication number: CN214863562U
Application number: CN202121634669.8U
Authority: CN
Inventors: 王伟丰; 王海华; 王齐昌
Original assignee: Jiangsu Dinglitong Technology Co ltd
Current assignee: Jiangsu Dinglitong Technology Co ltd
Priority date: 2021-07-19
Filing date: 2021-07-19
Publication date: 2021-11-26
Anticipated expiration: 2031-07-19

Abstract

The utility model discloses an environment-friendly sulfonation reaction device, including the cooler bin, the top fixedly connected with reactor of cooler bin, the bottom of reactor is equipped with the discharging pipe, the outer wall of discharging pipe has the bleeder valve through the clamp joint, the top outer wall fixedly connected with of reactor weighs the meter, the outer wall of weighing the meter is equipped with quality display screen, the top of weighing the meter is equipped with the weighing cup, the outer wall of weighing the cup is equipped with the inlet pipe, the outer wall of inlet pipe is equipped with the feed valve, the top outer wall of cooler bin is opened there is the feed port. The utility model discloses put into the weighing cup respectively with the reactant and weigh, according to weighing the data of counting the quality display screen, adjust quality and proportion between each reactant, treat the adjustment back that finishes, open agitator motor's switch, do not appropriately twist the feed valve that moves two inlet pipes again for each reactant gets into the reactor with fixed speed and reacts, increases reaction efficiency.

Description

Environment-friendly sulfonation reaction device

Technical Field

The utility model relates to a sulfonation reaction technical field especially relates to an environment-friendly sulfonation reaction device.

Background

The reaction of introducing sulfonic acid groups into the molecule of an organic compound is called sulfonation or sulfation. Sulfonation refers to a reaction in which a sulfur atom is bonded to a carbon atom to give a sulfonic acid compound. Sulfonation is an exothermic reaction, cooling is needed in low-temperature sulfonation, and heating and heat preservation are needed in high-temperature sulfonation. The aliphatic compounds are usually sulfonated by an indirect method. Aromatic compounds are predominantly sulfonated directly (electrophilic substitution).

The existing environment-friendly sulfonation reaction device has the following defects: before the sulfonation of the existing sulfonation reaction device, the mass of reactants needs to be weighed and proportioned firstly, and then the reactants are put into a reaction container manually for reaction, so that the process is complicated, the blanking speed of each reactant is not easy to control, and the reaction efficiency is reduced.

SUMMERY OF THE UTILITY MODEL

The utility model aims at solving the defects existing in the prior art and providing an environment-friendly sulfonation reaction device.

In order to achieve the above purpose, the utility model adopts the following technical scheme:

the utility model provides an environment-friendly sulfonation reaction device, includes the cooler bin, the top fixedly connected with reactor of cooler bin, the bottom of reactor is equipped with the discharging pipe, the outer wall of discharging pipe has the bleeder valve through the clamp joint, the top outer wall fixedly connected with of reactor weighs the meter, the outer wall of weighing the meter is equipped with quality display screen, the top of weighing the meter is equipped with the weighing cup, the outer wall of weighing the cup is equipped with the inlet pipe, the outer wall of inlet pipe is equipped with the feed valve, the top outer wall of cooler bin is opened there is the feed port, the one end of inlet pipe is pegged graft in the inner wall of feed port, the top outer wall fixedly connected with agitator motor of cooler bin, agitator motor's output shaft has the stirring roller through the coupling joint.

Furthermore, a water inlet pipe is arranged on the outer wall of one side of the cooling box, and a water outlet pipe is arranged on the outer wall of the other side of the cooling box.

Further, the top outer wall of reactor is equipped with the outlet duct, and the centre of outlet duct is equipped with the purge tube, and the inside of purge tube is equipped with the active carbon.

Furthermore, the outer wall of the top of the reactor is fixedly connected with a temperature display, the outer wall of the temperature display is provided with a temperature probe, and one end of the temperature probe extends into the reactor.

Further, the bottom outer wall fixedly connected with of cooler bin filters the motor, and filters the output shaft of motor and has the pivot through the coupling joint, and the one end fixedly connected with of pivot filters the bowl.

Furthermore, the bottom of filtering the bowl is equipped with filter paper, and filters the bowl and can dismantle the change, filters the bowl and is located under the discharging pipe.

Furthermore, the outer wall of the bottom of the cooling box is fixedly connected with bottom supports which are distributed equidistantly through bolts.

The utility model has the advantages that:

1. according to the environment-friendly sulfonation reaction device, the weighing meter, the weighing cup and the feeding pipes are arranged, before reactants are added, the reactants are respectively placed in the weighing cup to be weighed, the mass and the proportion of the reactants are adjusted according to the data of the mass display screen on the weighing meter, after the adjustment is finished, the switch of the stirring motor is opened, and then the feeding valves of the two feeding pipes are respectively and properly screwed, so that the reactants enter the reactor at a fixed speed to react, and the reaction efficiency is increased.

2. This environment-friendly sulfonation reaction device, through being provided with the filter motor, filter bowl and temperature monitor, the filter bowl can be when the discharging pipe ejection of compact, filter the solution of resultant, filter out dust particle or coking granule, make solution impurity reduce, the filter motor will filter the bowl and slowly rotate, increase filter area, improve filtration efficiency, the inside temperature of temperature monitor real-time detection reactor, and according to the intake speed of temperature regulation inlet tube, thereby keep the inside temperature of reactor.

The part not related in the device all is the same with prior art or can adopt prior art to realize, and the device design structure is reasonable, and convenient to use satisfies people's user demand.

Drawings

FIG. 1 is a schematic diagram of an overall three-dimensional structure of an environmentally friendly sulfonation reaction apparatus according to the present invention;

FIG. 2 is a three-dimensional structure diagram of a reactor of the environmental-friendly sulfonation reaction device provided by the utility model;

FIG. 3 is a three-dimensional structure diagram of a weighing meter of the environmental-friendly sulfonation reaction device provided by the utility model;

fig. 4 is a three-dimensional structure diagram of a filtering bowl of the environment-friendly sulfonation reaction device provided by the utility model.

In the figure: 1-purifying tube, 2-reactor, 3-cooling box, 4-water inlet tube, 5-bottom bracket, 6-filtering bowl, 7-water outlet tube, 8-weighing cup, 9-discharge valve, 10-discharge tube, 11-feeding tube, 12-stirring motor, 13-feeding hole, 14-temperature display, 15-quality display screen, 16-weighing meter, 17-air outlet tube, 18-filter paper, 19-rotating shaft and 20-filtering motor.

Detailed Description

The technical solution of the present patent will be described in further detail with reference to the following embodiments.

Reference will now be made in detail to embodiments of the present patent, examples of which are illustrated in the accompanying drawings, wherein like or similar reference numerals refer to the same or similar elements or elements having the same or similar function throughout. The embodiments described below with reference to the drawings are exemplary only for the purpose of explaining the present patent and are not to be construed as limiting the present patent.

In the description of this patent, it is to be understood that the terms "center," "upper," "lower," "front," "rear," "left," "right," "vertical," "horizontal," "top," "bottom," "inner," "outer," and the like are used in the orientations and positional relationships indicated in the drawings for the convenience of describing the patent and for the simplicity of description, and are not intended to indicate or imply that the referenced devices or elements must have a particular orientation, be constructed and operated in a particular orientation, and are not to be considered limiting of the patent.

In the description of this patent, it is noted that unless otherwise specifically stated or limited, the terms "mounted," "connected," and "disposed" are to be construed broadly and can include, for example, fixedly connected, disposed, detachably connected, disposed, or integrally connected and disposed. The specific meaning of the above terms in this patent may be understood by those of ordinary skill in the art as appropriate.

Referring to fig. 1-4, an environment-friendly sulfonation reaction device, including cooling box 3, the top fixedly connected with reactor 2 of cooling box 3, the bottom of reactor 2 is equipped with discharging pipe 10, discharging pipe 10's outer wall has bleeder valve 9 through the clamp joint, reactor 2's top outer wall fixedly connected with weighs the meter 16, the outer wall of weighing meter 16 is equipped with quality display screen 15, the top of weighing meter 16 is equipped with weighing cup 8, weighing cup 8's outer wall is equipped with inlet pipe 11, inlet pipe 11's outer wall is equipped with the feed valve, cooling box 3's top outer wall is opened has feed port 13, the one end of inlet pipe 11 is pegged graft in the inner wall of feed port 13, cooling box 3's top outer wall fixedly connected with agitator motor 12, agitator motor 12's output shaft has the stirring roller through the coupling joint.

The utility model discloses in, one side outer wall of cooler bin 3 is equipped with inlet tube 4, and the opposite side outer wall of cooler bin 3 is equipped with outlet pipe 7, and outlet pipe 7 highly is higher than inlet tube 4's height.

The utility model discloses in, the top outer wall of reactor 2 is equipped with outlet duct 17, and the centre of outlet duct 17 is equipped with purifying tube 1, and purifying tube 1's inside is equipped with the active carbon, and purifying tube 1 is used for purifying the gas that the reaction generated.

The utility model discloses in, the top outer wall fixedly connected with temperature monitor 14 of reactor 2, and temperature monitor 14's outer wall is equipped with temperature probe, and inside 2 deep reactors of reactor of temperature probe's one end, temperature monitor 14 was used for the 2 inside temperatures of real-time detection reactor.

The utility model discloses in, the bottom outer wall fixedly connected with of cooler bin 3 filters motor 20, and the output shaft that filters motor 20 has pivot 19 through the coupling joint, and the one end fixedly connected with of pivot 19 filters bowl 6, filters bowl 6 and can rotate under the effect of filtering motor 20.

The utility model discloses in, the bottom of filtering bowl 6 is equipped with filter paper 18, and filters bowl 6 and can dismantle the change, filters bowl 6 and is located discharging pipe 10 under, filters bowl 6 and is used for filtering the resultant solution that generates.

The utility model discloses in, the bottom outer wall of cooler bin 3 passes through the end support 5 that bolt fixedly connected with equidistance distributes.

The working principle is as follows: before adding the reactants, the reactants are respectively put into a weighing cup 8 for weighing, the mass and the proportion of the reactants are adjusted according to the data of a mass display screen 15 on a weighing meter 16, after the adjustment is finished, the switch of the stirring motor 12 is turned on, then the feeding valves of the two feeding pipes 11 are respectively and properly screwed, so that each reactant enters the reactor 2 at a fixed speed for reaction, the reaction efficiency is increased, the solution of the resultant can be filtered by the filtering bowl 6 when the discharging pipe 10 discharges the reactant, dust particles or coking particles are filtered out, so that the impurities in the solution are reduced, the filtering bowl 6 is slowly rotated by the filtering motor 20, the filtering area is increased, the filtering efficiency is improved, the temperature display 14 detects the temperature in the reactor 2 in real time, and adjusts the water inlet speed of the water inlet pipe 4 according to the temperature, thereby maintaining the temperature inside the reactor 2 to be stable.

The above, only be the concrete implementation of the preferred embodiment of the present invention, but the protection scope of the present invention is not limited thereto, and any person skilled in the art is in the technical scope of the present invention, according to the technical solution of the present invention and the utility model, the concept of which is equivalent to replace or change, should be covered within the protection scope of the present invention.

Claims

1. The environment-friendly sulfonation reaction device comprises a cooling box (3) and is characterized in that a reactor (2) is fixedly connected to the top of the cooling box (3), a discharge pipe (10) is arranged at the bottom of the reactor (2), a discharge valve (9) is clamped on the outer wall of the discharge pipe (10) through a clamp, a weighing meter (16) is fixedly connected to the outer wall of the top of the reactor (2), a quality display screen (15) is arranged on the outer wall of the weighing meter (16), a weighing cup (8) is arranged at the top of the weighing meter (16), a feed pipe (11) is arranged on the outer wall of the weighing cup (8), a feed valve is arranged on the outer wall of the feed pipe (11), a feed hole (13) is formed in the outer wall of the top of the cooling box (3), one end of the feed pipe (11) is inserted into the inner wall of the feed hole (13), and a stirring motor (12) is fixedly connected to the outer wall of the top of the cooling box (3), and an output shaft of the stirring motor (12) is connected with a stirring roller through a coupling.

2. The environment-friendly sulfonation reaction device of claim 1, wherein the cooling tank (3) is provided with a water inlet pipe (4) on the outer wall of one side and a water outlet pipe (7) on the outer wall of the other side.

3. The environment-friendly sulfonation reaction device of claim 1, wherein an air outlet pipe (17) is arranged on the outer wall of the top of the reactor (2), a purification pipe (1) is arranged in the middle of the air outlet pipe (17), and activated carbon is arranged inside the purification pipe (1).

4. The environment-friendly sulfonation reaction device of claim 1, wherein a temperature display (14) is fixedly connected to the outer wall of the top of the reactor (2), and a temperature probe is arranged on the outer wall of the temperature display (14), and one end of the temperature probe extends into the reactor (2).

5. The environment-friendly sulfonation reaction device of claim 1, wherein the outer wall of the bottom of the cooling tank (3) is fixedly connected with a filter motor (20), an output shaft of the filter motor (20) is connected with a rotating shaft (19) through a coupler, and one end of the rotating shaft (19) is fixedly connected with a filter bowl (6).

6. The environment-friendly sulfonation reaction device of claim 5, wherein the bottom of the filter bowl (6) is provided with filter paper (18), and the filter bowl (6) can be disassembled and replaced, and the filter bowl (6) is positioned right below the discharge pipe (10).

7. The environment-friendly sulfonation reaction device of claim 6, wherein the bottom outer wall of the cooling tank (3) is fixedly connected with equidistantly distributed bottom brackets (5) through bolts.