CN214863367U - High-pressure reaction kettle for controlling hydrothermal and solvothermal reaction processes - Google Patents
High-pressure reaction kettle for controlling hydrothermal and solvothermal reaction processes Download PDFInfo
- Publication number
- CN214863367U CN214863367U CN202023112675.5U CN202023112675U CN214863367U CN 214863367 U CN214863367 U CN 214863367U CN 202023112675 U CN202023112675 U CN 202023112675U CN 214863367 U CN214863367 U CN 214863367U
- Authority
- CN
- China
- Prior art keywords
- fixedly connected
- pipe
- kettle
- liquid
- reaction processes
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Images
Abstract
The utility model discloses a high-pressure reactor for controlling hydrothermal and solvothermal reaction processes, which belongs to the field of reaction kettles and comprises a kettle body, wherein the upper end of the kettle body is connected with a kettle cover through a bolt fixing clamp, the upper end of the kettle cover is fixedly connected with a support frame, the upper end of the support frame is fixedly connected with a motor, a motor shaft of the motor is fixedly connected with a cutting sleeve, the cutting sleeve is connected with a rotating shaft through the bolt fixing clamp, through the arrangement of a pressure gauge and a thermometer, the automatic test function of the kettle body is increased, and the rotating shaft and a stirrer are driven to be automatic through the motor shaft, the objects in the kettle body are convenient to stir, the objects in the kettle body are uniformly stirred and mixed, meanwhile, through a gap, an ear plate and a limiting rod are arranged and connected, the upper end of a liquid through pipe is convenient to be limited and fixed, a positioning block is in sliding insertion with a positioning groove, the lower end of the liquid through pipe is convenient to be limited and fixed, and the liquid through pipe is convenient to be installed and disassembled, convenient to use, dispersion pipe makes liquid homodisperse in the cauldron is internal convenient.
Description
Technical Field
The utility model relates to a reation kettle field, more specifically say, relate to a high-pressure batch autoclave for controlling hydrothermal and solvothermal reaction process.
Background
The broad understanding of the reaction kettle is that the reaction kettle is a container for physical or chemical reaction, and the heating, evaporation, cooling and low-speed mixing functions required by the process are realized through the structural design and parameter configuration of the container. The reaction kettle is widely applied to pressure vessels for petroleum, chemical engineering, rubber, pesticides, dyes, medicines and foods, and is used for completing technological processes such as vulcanization, nitration, hydrogenation, alkylation, polymerization, condensation and the like, such as a reactor, a reaction kettle, a decomposition kettle, a polymerization kettle and the like; the material is generally carbon manganese steel, stainless steel, zirconium, nickel-based (Hastelloy, Monel, Inconel) alloy and other composite materials.
At present current high-pressure batch autoclave's that is used for controlling hydrothermal and solvent thermal reaction process structural function is not good, leads to the result of use not good, and the majority also does not have the function that the stirring mixes in current reation kettle moreover, and the direct perpendicular unsettled inside of installing in reation kettle of transport cold liquid pipe majority that has now simultaneously not only installs the steadiness not good, but also inconvenient installation dismantlement.
SUMMERY OF THE UTILITY MODEL
Problem to exist among the prior art, an object of the utility model is to provide a high-pressure batch autoclave for controlling hydrothermal and solvent thermal reaction process, setting through manometer and thermometer, the automatic test function of the cauldron body has been increased, and it is automatic with the agitator to drive the pivot through the motor shaft, conveniently stir the internal object of cauldron, make the internal object stirring misce bene of cauldron, simultaneously through the breach, otic placode and gag lever post set up and be connected, conveniently carry out spacing fixed to the upper end of leading to the liquid pipe, locating piece and constant head tank slip grafting, conveniently carry out spacing fixed to the lower extreme of leading to the liquid pipe, and conveniently lead to the installation and the dismantlement of liquid pipe, facilitate the use, the dispersion pipe conveniently makes liquid homodisperse in the cauldron is internal.
In order to solve the above problems, the utility model adopts the following technical proposal.
A high-pressure reaction kettle for controlling hydrothermal and solvothermal reaction processes comprises a kettle body, wherein the upper end of the kettle body is connected with a kettle cover through a bolt fixing clamp, the upper end of the kettle cover is fixedly connected with a support frame, the upper end of the support frame is fixedly connected with a motor, a motor shaft of the motor is fixedly connected with a clamping sleeve, the clamping sleeve is connected with a rotating shaft through the bolt fixing clamp, the rotating shaft is fixedly connected with an agitator, the right side of the kettle cover is fixedly connected with a pressure gauge, the right side of the kettle cover is fixedly connected with a thermometer, the lower end of the thermometer is fixedly connected with a temperature measuring pipe, the upper left side of the clamping sleeve is fixedly connected with a liquid inlet pipe, the left side of the upper end of the kettle body is provided with a notch, the inner part of the notch is connected with an ear plate in a sliding and clamping manner, the right side of the ear plate is fixedly connected with a liquid passing pipe, the right side of the liquid passing pipe is fixedly connected with a plurality of dispersion pipes, and the lower end of the liquid passing pipe is fixedly connected with a positioning block, through the setting of manometer and thermometer, the automatic test function of the cauldron body has been increased, and it is automatic with the agitator to drive the pivot through the motor shaft, the convenient object to the internal portion of cauldron stirs, make the internal portion of cauldron stir the misce bene, simultaneously through the breach, the otic placode is connected with the setting of gag lever post, conveniently carry out spacing fixed to the upper end of leading to the liquid pipe, the locating piece is pegged graft with the constant head tank slip, conveniently carry out spacing fixed to the lower extreme that leads to the liquid pipe, and make things convenient for the installation and the dismantlement of leading to the liquid pipe, and convenient to use, the dispersion pipe conveniently makes liquid homodisperse in the cauldron is internal.
Further, the lower extreme fixedly connected with discharging pipe of the cauldron body through the setting of inlet pipe, conveniently adds the material to the inside of the cauldron body, and the sealed lid of sealed is rotated respectively through the screw thread with the inside of feed liquor pipe to the discharging pipe.
Further, the left side fixedly connected with inlet pipe of kettle cover.
Furthermore, the inside blanking cover that is connected with through the screw thread rotation of the upper end of inlet pipe.
Further, the inside lower extreme joint of feed liquor pipe has the sealing washer, the upper end that leads to the liquid pipe and the inside sliding seal of sealing washer, the sealing washer makes the feed liquor pipe hug closely sealedly with the junction that leads to the liquid pipe, avoids liquid to leak outward from junction between them.
Further, the lower extreme left side fixedly connected with gag lever post of kettle cover, the gag lever post slides and passes the otic placode, slides through the gag lever post and passes the otic placode for the inside fixed connection of otic placode and breach, thereby carry out fixed mounting to liquid pipe.
Further, the lower extreme left side of the cauldron body is equipped with the constant head tank, the inside slip joint of locating piece and constant head tank carries out spacing fixed to the lower extreme that leads to the liquid pipe through the inside slip joint of locating piece and constant head tank.
Compared with the prior art, the utility model has the advantages of:
(1) this scheme passes through the setting of manometer and thermometer, the automatic test function of the cauldron body has been increased, and it is automatic with the agitator to drive the pivot through the motor shaft, the convenient object to the internal portion of cauldron stirs, make the internal portion of cauldron stir the misce bene, simultaneously through the breach, the otic placode is connected with the setting of gag lever post, conveniently carry out spacing fixed to the upper end of leading to the liquid pipe, the locating piece is pegged graft with the constant head tank slip, conveniently carry out spacing fixed to the lower extreme that leads to the liquid pipe, and conveniently lead to the installation and the dismantlement of liquid pipe, and convenient to use, the dispersion pipe conveniently makes liquid homodisperse in the cauldron is internal.
(2) The lower extreme fixedly connected with discharging pipe of the cauldron body, the left side fixedly connected with inlet pipe of kettle cover, the upper end of inlet pipe is inside to be connected with the blanking cover through the screw thread rotation, through the setting of inlet pipe, conveniently adds the material to the inside of the cauldron body, and the discharging pipe rotates sealed lid with the inside of feed liquor pipe respectively through the screw thread.
(3) The inside lower extreme joint of feed liquor pipe has the sealing washer, leads to the upper end of liquid pipe and the inside sliding seal of sealing washer, and the sealing washer makes the feed liquor pipe hug closely sealedly with the junction that leads to the liquid pipe, avoids liquid to leak outward from junction between them.
(4) The lower extreme left side fixedly connected with gag lever post of kettle cover, the gag lever post slides and passes the otic placode, slides through the gag lever post and passes the otic placode for the inside fixed connection of otic placode and breach, thereby carry out fixed mounting to liquid pipe.
(5) The lower extreme left side of the cauldron body is equipped with the constant head tank, and the locating piece carries out spacing fixed to the lower extreme that leads to the liquid pipe through the inside slip joint of locating piece and constant head tank with the inside slip joint of constant head tank.
Drawings
FIG. 1 is a partial sectional view of the overall structure of the present invention;
FIG. 2 is a bottom view of the kettle cover of the present invention;
FIG. 3 is a top view of the kettle body of the present invention;
fig. 4 is a top cross-sectional view of the kettle body of the present invention.
The reference numbers in the figures illustrate:
1 kettle body, 2 discharging pipes, 3 kettle covers, 4 supporting frames, 5 motors, 6 motor shafts, 7 cutting sleeves, 8 rotating shafts, 9 stirrers, 10 feeding pipes, 11 plugging covers, 12 pressure gauges, 13 thermometers, 14 temperature measuring pipes, 15 liquid inlet pipes, 16 sealing rings, 17 gaps, 18 lug plates, 19 limiting rods, 20 liquid through pipes, 21 dispersion pipes, 22 positioning blocks and 23 positioning grooves.
Detailed Description
The technical solution in the embodiment of the present invention will be clearly and completely described below with reference to the accompanying drawings in the embodiment of the present invention; obviously, the described embodiments are only a part of the embodiments of the present invention, and not all embodiments, and all other embodiments obtained by those skilled in the art without any inventive work are within the scope of the present invention based on the embodiments of the present invention.
Referring to fig. 1-4, a high pressure reactor for controlling hydrothermal and solvothermal reaction processes comprises a reactor body 1, referring to fig. 1, a reactor cover 3 is fixedly clamped at the upper end of the reactor body 1 through bolts, a support frame 4 is fixedly connected at the upper end of the reactor cover 3, a motor 5 is fixedly connected at the upper end of the support frame 4, the model of the motor 5 is YE2, a plug of the motor 5 is plugged with an external power supply, belonging to the prior art, a motor shaft 6 of the motor 5 is fixedly connected with a cutting sleeve 7, the cutting sleeve 7 is fixedly clamped with a rotating shaft 8 through bolts, the rotating shaft 8 is fixedly connected with a stirrer 9, a pressure gauge 12 is fixedly connected at the right side of the reactor cover 3, a thermometer 13 is fixedly connected at the right side of the reactor cover 3, a temperature measuring pipe 14 is fixedly connected at the lower end of the thermometer 13, a liquid inlet pipe 15 is fixedly connected at the left side of the upper end of a blocking cover 11, a notch 17 is arranged at the left side of the upper end of the reactor body 1, an inner part of the notch 17 is clamped with an ear plate 18, liquid pipe 20 is led to the right side fixedly connected with of otic placode 18, a plurality of dispersion pipes 21 of right side fixedly connected with of liquid pipe 20, the lower extreme fixedly connected with locating piece 22 of liquid pipe 20 leads to, setting through manometer 12 and thermometer 13, the automatic test function of the cauldron body 1 has been increased, and it is automatic with agitator 9 to drive pivot 8 through motor shaft 6, conveniently stir the object of the 1 inside of the cauldron body, make the object stirring misce bene of the 1 inside of the cauldron body, simultaneously through breach 17, otic placode 18 and gag lever post 19 set up and be connected, conveniently carry out spacing fixed to the upper end of leading to liquid pipe 20, locating piece 22 and constant head tank 23 slip grafting, conveniently carry out spacing fixed to the lower extreme of leading to liquid pipe 20, and conveniently lead to the installation and the dismantlement of liquid pipe 20, convenient use, dispersion pipe 21 conveniently makes liquid homodisperse in the cauldron body 1.
Please refer to fig. 1, a discharging pipe 2 is fixedly connected to the lower end of a kettle body 1, a feeding pipe 10 is fixedly connected to the left side of a kettle cover 3, a blocking cover 11 is rotatably connected to the inside of the upper end of the feeding pipe 10 through threads, materials are conveniently added to the inside of the kettle body 1 through the feeding pipe 10, the discharging pipe 2 and the inside of a liquid inlet pipe 15 respectively rotate to seal a sealing cover through threads, a sealing ring 16 is clamped at the lower end of the inside of the liquid inlet pipe 15, the upper end of a liquid through pipe 20 is sealed with the inside of the sealing ring 16 in a sliding manner, the sealing ring 16 enables the liquid inlet pipe 15 to be tightly attached to the joint of the liquid through pipe 20, and liquid leakage from the joint of the discharging pipe and the liquid through pipe is avoided.
Referring to fig. 1, a limiting rod 19 is fixedly connected to the left side of the lower end of the kettle cover 3, the limiting rod 19 penetrates through the ear plate 18 in a sliding manner, and the limiting rod 19 penetrates through the ear plate 18 in a sliding manner, so that the ear plate 18 is fixedly connected with the inside of the notch 17, the liquid through pipe 20 is fixedly installed, a positioning groove 23 is formed in the left side of the lower end of the kettle body 1, the positioning block 22 is clamped with the inside of the positioning groove 23 in a sliding manner, and the lower end of the liquid through pipe 20 is limited and fixed by the clamping of the positioning block 22 with the inside of the positioning groove 23 in a sliding manner.
The liquid passing pipe 20 is arranged inside the kettle body 1 by the sliding clamping connection of the lug plate 18 inside the notch 17 and the sliding clamping connection of the positioning block 22 and the positioning groove 23 inside the kettle body, then the kettle cover 3 is connected to the upper end of the kettle body 1 by the sliding clamping connection of the bolt, the limiting rod 19 is enabled to pass through the lug plate 18 in a sliding manner, then the plug of the motor 5 is inserted, the motor shaft 6 of the motor 5 rotates, the motor shaft 6 drives the clamping sleeve 7 to rotate, the clamping sleeve 7 drives the rotating shaft 8 to rotate, the rotating shaft 8 drives the stirrer 9 to rotate, the stirrer 9 stirs objects inside the kettle body 1, the liquid inside the kettle body 1 is measured by the connection of the thermometer 13 and the temperature measuring pipe 14, the pressure is applied to the inside of the kettle body 1 by the setting of the pressure gauge 12, the automatic testing function of the kettle body 1 is increased by the setting of the pressure gauge 12 and the thermometer 13, and the rotating shaft 8 is driven by the motor shaft 6 to be automatic with the stirrer 9, the convenient object to the internal portion of cauldron is stirred for the internal portion of cauldron stirring misce bene, simultaneously through breach 17, otic placode 18 and gag lever post 19 set up and be connected, conveniently carry out spacing fixed to the upper end of leading to liquid pipe 20, locating piece 22 is pegged graft with constant head tank 23 slip, conveniently carry out spacing fixed to the lower extreme that leads to liquid pipe 20, and conveniently lead to the installation and the dismantlement of liquid pipe 20, facilitate the use, dispersion pipe 21 conveniently makes liquid homodisperse in the cauldron internal 1.
The above description is only the preferred embodiment of the present invention; the scope of the present invention is not limited thereto. Any person skilled in the art should also be able to cover the technical scope of the present invention by replacing or changing the technical solution and the improvement concept of the present invention with equivalents and modifications within the technical scope of the present invention.
Claims (7)
1. A high pressure batch autoclave for controlling hydrothermal and solvothermal reaction processes, comprising an autoclave body (1) and a closure (11), characterized in that: the kettle is characterized in that a kettle cover (3) is fixedly connected to the upper end of the kettle body (1) through a bolt, a support frame (4) is fixedly connected to the upper end of the kettle cover (3), a motor (5) is fixedly connected to the upper end of the support frame (4), a cutting sleeve (7) is fixedly connected to a motor shaft (6) of the motor (5), a rotating shaft (8) is connected to the cutting sleeve (7) through the bolt, a stirrer (9) is fixedly connected to the rotating shaft (8), a pressure gauge (12) is fixedly connected to the right side of the kettle cover (3), a thermometer (13) is fixedly connected to the right side of the kettle cover (3), a temperature measuring pipe (14) is fixedly connected to the lower end of the thermometer (13), a liquid inlet pipe (15) is fixedly connected to the left side of the upper end of the blocking cover (11), a notch (17) is arranged on the left side of the upper end of the kettle body (1), an inner sliding clamp of the notch (17) is connected with an ear plate (18), the right side fixedly connected with of otic placode (18) leads to liquid pipe (20), lead to a plurality of dispersion pipes of right side fixedly connected with (21) of liquid pipe (20), the lower extreme fixedly connected with locating piece (22) of liquid pipe (20).
2. An autoclave reactor for controlling hydrothermal and solvothermal reaction processes according to claim 1, wherein: the lower end of the kettle body (1) is fixedly connected with a discharge pipe (2).
3. An autoclave reactor for controlling hydrothermal and solvothermal reaction processes according to claim 1, wherein: the left side fixedly connected with inlet pipe (10) of kettle cover (3).
4. An autoclave reactor for controlling hydrothermal and solvothermal reaction processes according to claim 3, wherein: the upper end of the feeding pipe (10) is internally and rotatably connected with a blocking cover (11) through threads.
5. An autoclave reactor for controlling hydrothermal and solvothermal reaction processes according to claim 1, wherein: the inside lower extreme joint of feed liquor pipe (15) has sealing washer (16), the inside sliding seal of the upper end of leading to liquid pipe (20) and sealing washer (16).
6. An autoclave reactor for controlling hydrothermal and solvothermal reaction processes according to claim 4, wherein: the lower extreme left side fixedly connected with gag lever post (19) of kettle cover (3), gag lever post (19) slide and pass otic placode (18).
7. An autoclave reactor for controlling hydrothermal and solvothermal reaction processes according to claim 1, wherein: the lower extreme left side of the cauldron body (1) is equipped with constant head tank (23), locating piece (22) and the inside slip joint of constant head tank (23).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202023112675.5U CN214863367U (en) | 2020-12-22 | 2020-12-22 | High-pressure reaction kettle for controlling hydrothermal and solvothermal reaction processes |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202023112675.5U CN214863367U (en) | 2020-12-22 | 2020-12-22 | High-pressure reaction kettle for controlling hydrothermal and solvothermal reaction processes |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN214863367U true CN214863367U (en) | 2021-11-26 |
Family
ID=78903800
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202023112675.5U Active CN214863367U (en) | 2020-12-22 | 2020-12-22 | High-pressure reaction kettle for controlling hydrothermal and solvothermal reaction processes |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN214863367U (en) |
-
2020
- 2020-12-22 CN CN202023112675.5U patent/CN214863367U/en active Active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN214863367U (en) | High-pressure reaction kettle for controlling hydrothermal and solvothermal reaction processes | |
| CN207694795U (en) | A kind of chemical industry stirred autoclave | |
| CN218890526U (en) | High-pressure stirring reaction kettle | |
| CN210584932U (en) | Reaction kettle | |
| CN213348863U (en) | Resin reaction kettle | |
| CN211755014U (en) | Area protection reation kettle that hydroxyl silicone oil was used | |
| CN211755021U (en) | Chemical industry reation kettle with solid feeding device | |
| CN209576691U (en) | A kind of small-sized reaction kettle of applied chemistry | |
| CN211436211U (en) | A ward off glass reactor for chemical production | |
| CN208320813U (en) | A kind of enamel reaction still | |
| CN212237258U (en) | Chemical industry reation kettle of removable inner bag | |
| CN218131740U (en) | Prevent reation kettle discharge gate of jam | |
| CN108854894A (en) | A kind of stainless steel cauldron | |
| CN212576290U (en) | Novel reation kettle of production epoxy fatty acid methyl ester | |
| CN219984458U (en) | Chemistry test agitator | |
| CN218307920U (en) | A temperature self-adjusting formula reation kettle for chemical synthesis | |
| CN204865816U (en) | Safe reation kettle | |
| CN219559463U (en) | Stainless steel resin reaction kettle stirring device | |
| CN212143806U (en) | Pressure reation kettle convenient to wash | |
| CN210357146U (en) | Stirring device of reaction kettle | |
| CN211463127U (en) | Reaction stirring device convenient to install, fix and adjust | |
| CN218962597U (en) | Reation kettle is used in production of insulating waterproof sealant | |
| CN211865020U (en) | Intelligent heating and cooling double-effect unit for reaction kettle | |
| CN217747067U (en) | Reaction kettle for preparing high-adhesion polymer | |
| CN213556932U (en) | Chemical industry reation kettle feed arrangement |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant |