CN214810728U - Continuous synthesis device of prothioconazole - Google Patents
Continuous synthesis device of prothioconazole Download PDFInfo
- Publication number
- CN214810728U CN214810728U CN202120240287.0U CN202120240287U CN214810728U CN 214810728 U CN214810728 U CN 214810728U CN 202120240287 U CN202120240287 U CN 202120240287U CN 214810728 U CN214810728 U CN 214810728U
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- Prior art keywords
- reactor main
- main body
- air outlet
- gas
- inlet pipe
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- MNHVNIJQQRJYDH-UHFFFAOYSA-N 2-[2-(1-chlorocyclopropyl)-3-(2-chlorophenyl)-2-hydroxypropyl]-1,2-dihydro-1,2,4-triazole-3-thione Chemical compound N1=CNC(=S)N1CC(C1(Cl)CC1)(O)CC1=CC=CC=C1Cl MNHVNIJQQRJYDH-UHFFFAOYSA-N 0.000 title claims abstract description 18
- 239000005825 Prothioconazole Substances 0.000 title claims abstract description 18
- 230000015572 biosynthetic process Effects 0.000 title claims abstract description 16
- 238000003786 synthesis reaction Methods 0.000 title claims abstract description 16
- 239000007788 liquid Substances 0.000 claims abstract description 42
- 238000000926 separation method Methods 0.000 claims abstract description 34
- 238000010992 reflux Methods 0.000 claims abstract description 22
- 239000000463 material Substances 0.000 claims abstract description 9
- 238000005192 partition Methods 0.000 claims description 5
- 238000004519 manufacturing process Methods 0.000 abstract description 6
- 238000006243 chemical reaction Methods 0.000 description 7
- 201000010099 disease Diseases 0.000 description 5
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 5
- 241000221662 Sclerotinia Species 0.000 description 3
- 241000209140 Triticum Species 0.000 description 3
- 235000021307 Triticum Nutrition 0.000 description 3
- 244000309464 bull Species 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000005457 optimization Methods 0.000 description 3
- 235000017060 Arachis glabrata Nutrition 0.000 description 2
- 244000105624 Arachis hypogaea Species 0.000 description 2
- 235000010777 Arachis hypogaea Nutrition 0.000 description 2
- 235000018262 Arachis monticola Nutrition 0.000 description 2
- 240000005979 Hordeum vulgare Species 0.000 description 2
- 235000007340 Hordeum vulgare Nutrition 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 235000020232 peanut Nutrition 0.000 description 2
- 241001530056 Athelia rolfsii Species 0.000 description 1
- 241000221785 Erysiphales Species 0.000 description 1
- 206010027146 Melanoderma Diseases 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 244000046052 Phaseolus vulgaris Species 0.000 description 1
- 235000010627 Phaseolus vulgaris Nutrition 0.000 description 1
- 241000233647 Phytophthora nicotianae var. parasitica Species 0.000 description 1
- 230000006978 adaptation Effects 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 239000003899 bactericide agent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 235000013339 cereals Nutrition 0.000 description 1
- 230000006806 disease prevention Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000008029 eradication Effects 0.000 description 1
- 238000011010 flushing procedure Methods 0.000 description 1
- 230000005923 long-lasting effect Effects 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 230000009885 systemic effect Effects 0.000 description 1
- QPDUQKTYZRXRBC-UHFFFAOYSA-N triazole-4-thione Chemical compound S=C1C=NN=N1 QPDUQKTYZRXRBC-UHFFFAOYSA-N 0.000 description 1
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Abstract
The utility model relates to a continuous synthesizer of prothioconazole. The continuous synthesis device for prothioconazole comprises a reactor main body, wherein an air outlet channel is arranged inside the reactor main body, the reactor main body is connected with a first inlet pipe and a second inlet pipe, the first inlet pipe is positioned above the second inlet pipe, a feed plate is fixedly connected inside the reactor main body, a plurality of feed holes are formed in the outer surface of the feed plate, the feed plate disperses materials input by the first inlet pipe, the lower end of the air outlet channel is positioned above the feed plate, the lower end of the air outlet channel is sealed, the upper end of the air outlet channel is connected with an air outlet pipe, and a plurality of groups of reflux plates are fixedly connected inside the reactor main body; this serialization synthesizer of prothioconazole, simple structure, convenient operation, it is nimble to use, is convenient for realize the continuous type gas-liquid separation of ladder, has improved production efficiency and security performance, has reduced manufacturing cost, and the use is promoted in the trade of being convenient for.
Description
Technical Field
The utility model belongs to the technical field of the medicine processing, concretely relates to prothioconazole's serialization synthesizer.
Background
The prothioconazole is a novel broad-spectrum triazolethione bactericide, has good systemic activity, excellent protection, treatment and eradication activity and long lasting period, and a large number of field efficacy tests show that the prothioconazole has good safety to crops, good disease prevention and treatment effects and obvious yield increase, and is mainly used for preventing and treating a plurality of diseases of cereal crops such as wheat, barley, rape, peanut, rice, bean crops and the like. The prothioconazole almost has good control effect on all wheat diseases, such as powdery mildew, banded sclerotial blight, leaf spot, rust disease, sclerotinia rot, net blotch, leaf spot and the like of wheat and barley; can also prevent and control soil-borne diseases of the rape and the peanut, such as sclerotinia, and main leaf surface diseases, such as gray mold, black spot, brown spot, black shank, sclerotinia, rust and the like.
The prothioconazole is often used in combination with a conventional synthesis kettle in preparation, has long feeding and dripping time, more byproducts and continuous gas generation, is very easy to cause the material flushing of a large synthesis kettle, and has poor controllability and safety performance.
SUMMERY OF THE UTILITY MODEL
The utility model aims to solve the problems and provide a continuous synthesis device of prothioconazole with simple structure and reasonable design.
The utility model discloses a following technical scheme realizes above-mentioned purpose:
a continuous synthesis device for prothioconazole comprises a reactor main body, wherein an air outlet channel is arranged inside the reactor main body, the reactor main body is connected with a first inlet pipe and a second inlet pipe, the first inlet pipe is positioned above the second inlet pipe, a feed plate is fixedly connected inside the reactor main body, a plurality of feed holes are formed in the outer surface of the feed plate, the feed plate disperses materials input by the first inlet pipe, the lower end of the air outlet channel is positioned above the feed plate, the lower end of the air outlet channel is sealed, the upper end of the air outlet channel is connected with an air outlet pipe, a plurality of groups of reflux plates are fixedly connected inside the reactor main body, a reflux channel is arranged between two adjacent groups of reflux plates, the side wall of the air outlet channel is provided with an air outlet, and the air outlet is communicated with the reflux channel, the bottom of reactor main part is provided with a plurality of groups gas-liquid separation board, the gas-liquid separation board is vertical setting, the backward flow board is the slope setting, gas-liquid separation board and backward flow board one-to-one, every group the gas-liquid separation board is close to the end of its backward flow board that corresponds, the reactor main part still is connected with the drain pipe, the drain pipe with first inlet pipe is installed relatively.
As a further optimization scheme of the utility model, the height-adjustable of gas-liquid separation board.
As a further optimization scheme of the utility model, the lower terminal surface fixedly connected with stake body of reactor main part, the regulation mouth has been seted up to the lower extreme of reactor main part, the gas-liquid separation board can be located reciprocate in the regulation mouth.
As the utility model discloses a further optimization scheme, the gas-liquid separation board includes frame and partition plate spare, the lower extreme swing joint of frame has the bull stick, the head is twisted to the lower extreme fixedly connected with of bull stick, the regulation cavity has been seted up to the lower extreme of reactor main part, adjust the mouth set up in adjust the last cavity wall of cavity, the bull stick runs through adjust the cavity's lower chamber wall, and with this lower chamber wall threaded connection.
The beneficial effects of the utility model reside in that: the utility model can be used flexibly, and can analyze the liquid discharged from the liquid outlet pipe of the reactor main body, and if the liquid is not completely reacted, a plurality of reactor main bodies can be configured to be used together; the reactor main body is internally provided with a plurality of groups of reflux plates and reflux channels, the reflux channels are inclined due to the arrangement of the reflux plates and are convenient for liquid fluid, the reflux channels are communicated with the gas outlet channels through gas outlets, gas in reaction can conveniently enter the gas outlet channels through the gas outlets and can be discharged through the gas outlet pipes, and in actual use, tail gas treatment should be carried out on the gas discharged by the gas outlet pipes; the device can also adjust the height of the gas-liquid separation plate according to the amount of actual reaction materials, thereby adjusting the reaction space and realizing the stepped continuous gas-liquid separation; the whole device is simple in structure, convenient to operate, flexible to use, convenient to realize stepped continuous gas-liquid separation, capable of improving production efficiency and safety performance, capable of reducing production cost and convenient to popularize and use in the industry.
Drawings
Fig. 1 is a schematic view of the overall structure of the present invention;
fig. 2 is a schematic structural view of the gas-liquid separation plate of the present invention.
In the figure: 1. a reactor body; 2. an air outlet channel; 3. an air outlet; 4. an air outlet pipe; 5. a first feed tube; 6. a second feed tube; 7. adjusting the cavity; 8. a stent body; 9. a gas-liquid separation plate; 10. a rotating rod; 11. screwing the head; 12. a liquid outlet pipe; 13. a return plate; 14. a return channel; 15. and a feeding plate.
Detailed Description
The present application will now be described in further detail with reference to the drawings, it should be noted that the following detailed description is given for illustrative purposes only and is not to be construed as limiting the scope of the present application, as those skilled in the art will be able to make numerous insubstantial modifications and adaptations to the present application based on the above disclosure.
Example 1
As shown in fig. 1-2, a continuous synthesis device for prothioconazole, comprising a reactor main body 1, wherein an air outlet channel 2 is arranged inside the reactor main body 1, the reactor main body 1 is connected with a first inlet pipe 5 and a second inlet pipe 6, the first inlet pipe 5 is positioned above the second inlet pipe 6, a feed plate 15 is fixedly connected inside the reactor main body 1, a plurality of feed holes are formed on the outer surface of the feed plate 15, the feed plate 15 disperses the material input by the first inlet pipe 5, the lower end of the air outlet channel 2 is positioned above the feed plate 15, the lower end of the air outlet channel 2 is sealed, an air outlet pipe 4 is connected to the upper end of the air outlet channel 2, a plurality of reflux plates 13 are fixedly connected inside the reactor main body 1, and a reflux channel 14 is arranged between two adjacent reflux plates 13, gas outlet 3 has been seted up to outlet channel 2's lateral wall, gas outlet 3 with backflow channel 14 intercommunication, the bottom of reactor main part 1 is provided with a plurality of gas-liquid separation board 9 of group, gas-liquid separation board 9 is vertical setting, backflow board 13 is the slope setting, gas-liquid separation board 9 and backflow board 13 one-to-one, every group gas-liquid separation board 9 is close to the end of its corresponding backflow board 13, reactor main part 1 still is connected with drain pipe 12, drain pipe 12 with first inlet pipe 5 is installed relatively.
The height of the gas-liquid separation plate 9 is adjustable. In this embodiment, the height-adjustable specific setting is: the lower end face of the reactor main body 1 is fixedly connected with a support body 8, the lower end of the reactor main body 1 is provided with an adjusting opening, and the gas-liquid separation plate 9 can be positioned in the adjusting opening to move up and down. The gas-liquid separation plate 9 comprises a frame piece and a partition plate piece, the lower end of the frame piece is movably connected with a rotating rod 10, the lower end of the rotating rod 10 is fixedly connected with a twisting head 11, the lower end of the reactor main body 1 is provided with an adjusting cavity 7, an adjusting opening is formed in the upper cavity wall of the adjusting cavity 7, and the rotating rod 10 penetrates through the lower cavity wall of the adjusting cavity 7 and is in threaded connection with the lower cavity wall. In actual use, the screw head 11 is rotated, the rotating rod 10 is rotated, the upper end of the rotating rod 10 is movably connected with a frame of the gas-liquid separation plate 9 (the specific mode of movable connection can be matched with a bearing piece for use, and other modes of rotary connection can be selected for use), the rotating rod 10 is a screw rod piece, the rotating rod 10 is in threaded connection with the lower cavity wall of the adjusting cavity 7, therefore, after the rotating rod 10 rotates, the gas-liquid separation plate 9 moves upwards or downwards, the adjusting device is arranged before use, after the material amount needing to be reacted is judged, the gas-liquid separation plate 9 is adjusted, when the material amount is large, the gas-liquid separation plate 9 close to the feeding pipe is adjusted to be as low as possible, the adjusting device is adjusted by using a partition plate or a frame as a limit, an elastic sealing piece is arranged at the edge of the adjusting opening, and the adjusting opening can be well sealed by matching the partition plate with the frame.
In the continuous synthesis apparatus for prothioconazole, when in use, analysis is performed according to the liquid discharged from the liquid outlet pipe 12 of the reactor main body 1, and if the reaction is not completed, a plurality of reactor main bodies 1 can be arranged for use; the reactor main body 1 is internally provided with a plurality of groups of reflux plates 13 and reflux channels 14, the reflux channels 14 are inclined due to the arrangement of the reflux plates 13, so that liquid fluid is convenient, the reflux channels 14 are communicated with the gas outlet channel 2 through the gas outlet 3, so that gas in reaction enters the gas outlet channel 2 through the gas outlet 3 and is discharged through the gas outlet pipe 4, and in actual use, tail gas treatment should be carried out on the gas discharged from the gas outlet pipe 4; the device can also adjust the height of the gas-liquid separation plate 9 according to the amount of actual reaction materials, thereby adjusting the reaction space and realizing the stepped continuous gas-liquid separation; the whole device is simple in structure, convenient to operate, flexible to use, convenient to realize stepped continuous gas-liquid separation, capable of improving production efficiency and safety performance, capable of reducing production cost and convenient to popularize and use in the industry.
The above-mentioned embodiments only represent some embodiments of the present invention, and the description thereof is specific and detailed, but not to be construed as limiting the scope of the present invention. It should be noted that, for those skilled in the art, without departing from the spirit of the present invention, several variations and modifications can be made, which are within the scope of the present invention.
Claims (4)
1. The continuous synthesis device for prothioconazole is characterized by comprising a reactor main body, wherein an air outlet channel is arranged inside the reactor main body, the reactor main body is connected with a first inlet pipe and a second inlet pipe, the first inlet pipe is positioned above the second inlet pipe, a feed plate is fixedly connected inside the reactor main body, a plurality of feed holes are formed in the outer surface of the feed plate, the feed plate disperses the material input by the first inlet pipe, the lower end of the air outlet channel is positioned above the feed plate, the lower end of the air outlet channel is sealed, an air outlet pipe is connected at the upper end of the air outlet channel, a plurality of groups of reflux plates are fixedly connected inside the reactor main body, a reflux channel is arranged between two adjacent groups of reflux plates, an air outlet is formed in the side wall of the air outlet channel, and the air outlet is communicated with the reflux channel, the bottom of reactor main part is provided with a plurality of groups gas-liquid separation board, the gas-liquid separation board is vertical setting, the backward flow board is the slope setting, gas-liquid separation board and backward flow board one-to-one, every group the gas-liquid separation board is close to the end of its backward flow board that corresponds, the reactor main part still is connected with the drain pipe, the drain pipe with first inlet pipe is installed relatively.
2. The continuous synthesis device of prothioconazole according to claim 1, wherein the synthesis device comprises: the height of the gas-liquid separation plate is adjustable.
3. The continuous synthesis device of prothioconazole according to claim 2, wherein the synthesis device comprises: the lower end face of the reactor main body is fixedly connected with a support body, the lower end of the reactor main body is provided with an adjusting opening, and the gas-liquid separation plate can be positioned in the adjusting opening to move up and down.
4. The continuous synthesis device of prothioconazole according to claim 3, wherein the synthesis device comprises: the gas-liquid separation plate comprises a frame piece and a partition plate piece, the lower end of the frame piece is movably connected with a rotating rod, the lower end of the rotating rod is fixedly connected with a twisting head, the lower end of the reactor main body is provided with an adjusting cavity, an adjusting opening is formed in the upper cavity wall of the adjusting cavity, and the rotating rod penetrates through the lower cavity wall of the adjusting cavity and is in threaded connection with the lower cavity wall.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202120240287.0U CN214810728U (en) | 2021-01-28 | 2021-01-28 | Continuous synthesis device of prothioconazole |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202120240287.0U CN214810728U (en) | 2021-01-28 | 2021-01-28 | Continuous synthesis device of prothioconazole |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN214810728U true CN214810728U (en) | 2021-11-23 |
Family
ID=78953696
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202120240287.0U Expired - Fee Related CN214810728U (en) | 2021-01-28 | 2021-01-28 | Continuous synthesis device of prothioconazole |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN214810728U (en) |
-
2021
- 2021-01-28 CN CN202120240287.0U patent/CN214810728U/en not_active Expired - Fee Related
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| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20211123 |
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| CF01 | Termination of patent right due to non-payment of annual fee |