CN214808592U - Extraction device of 1-phenylpyridine - Google Patents
Extraction device of 1-phenylpyridine Download PDFInfo
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- CN214808592U CN214808592U CN202022994841.2U CN202022994841U CN214808592U CN 214808592 U CN214808592 U CN 214808592U CN 202022994841 U CN202022994841 U CN 202022994841U CN 214808592 U CN214808592 U CN 214808592U
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- extraction
- tank
- electric motor
- phenylpyridine
- liquid outlet
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- 238000000605 extraction Methods 0.000 title claims abstract description 72
- MOKUQYSJYISPJS-UHFFFAOYSA-N 1-phenyl-2h-pyridine Chemical compound C1C=CC=CN1C1=CC=CC=C1 MOKUQYSJYISPJS-UHFFFAOYSA-N 0.000 title claims abstract description 15
- 239000007788 liquid Substances 0.000 claims abstract description 31
- 239000000463 material Substances 0.000 claims abstract description 30
- 238000002156 mixing Methods 0.000 claims abstract description 26
- 238000003860 storage Methods 0.000 claims abstract description 18
- 238000003756 stirring Methods 0.000 claims description 10
- 230000000694 effects Effects 0.000 abstract description 3
- 238000005119 centrifugation Methods 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
- 230000008676 import Effects 0.000 description 3
- 238000005191 phase separation Methods 0.000 description 2
- 230000008859 change Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000012847 fine chemical Substances 0.000 description 1
- 238000009854 hydrometallurgy Methods 0.000 description 1
- 238000005304 joining Methods 0.000 description 1
- 238000000622 liquid--liquid extraction Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 238000004065 wastewater treatment Methods 0.000 description 1
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Abstract
The utility model relates to an extraction device of 1-phenylpyridine, including material storage jar (1), extractant storage tank (2), blending tank (3), extraction jar (4), material storage jar (1), extractant storage tank (2) pass through the pipeline and be connected with blending tank (3), the pipeline on install measuring pump (301), blending tank (3) be connected with extraction jar (4), the internally mounted of blending tank (3) stir-paddle (302), the top of blending tank (3) be provided with motor (303); the bottom of the extraction tank (4) is U-shaped, the lowest point of the bottom of the extraction tank (4) is connected with a driving motor (5), a lower-layer liquid outlet (401) is arranged at the bottom of the extraction tank (4), and the driving motor (5) drives the extraction tank (4) to rotate, so that centrifugal extraction is realized. The utility model has the advantages of structural design is reasonable, extraction efficiency is high, extraction effect is good.
Description
Technical Field
The utility model relates to a compound extraction equipment technical field, concretely relates to extraction device of 1-phenylpyridine.
Background
The centrifugal extraction technology is a practical technology for realizing liquid-liquid two-phase contact mass transfer and phase separation by means of a centrifugal force field, is a novel high-efficiency separation technology combining liquid-liquid extraction and a centrifugal technology, and has the characteristics of short contact time of two-phase materials, high phase separation speed, small residual quantity in equipment, wide operation comparison range and the like compared with other extraction technologies. The technology is now applied to numerous fields such as hydrometallurgy, pharmacy, wastewater treatment, nuclear energy, petrochemical industry, fine chemical industry and the like by a large number of researchers. The problem of extraction inefficiency exists at current 1-phenylpyridine in process of production, consequently the utility model designs an extraction device of 1-phenylpyridine that extraction efficiency is high.
SUMMERY OF THE UTILITY MODEL
In order to solve the problems existing in the prior art, the utility model provides an extraction device of 1-phenylpyridine, the concrete technical scheme is as follows:
the extraction device of the 1-phenylpyridine comprises a material storage tank (1), an extractant storage tank (2), a mixing tank (3) and an extraction tank (4), wherein the material storage tank (1) and the extractant storage tank (2) are connected with the mixing tank (3) through a pipeline, a metering pump (301) is installed on the pipeline, the mixing tank (3) is connected with the extraction tank (4), a stirring paddle (302) is installed inside the mixing tank (3), a motor (303) is arranged at the top of the mixing tank (3), and the motor (303) drives the stirring paddle (302) to stir;
the bottom of the extraction tank (4) is U-shaped, the lowest point of the bottom of the extraction tank (4) is connected with a driving motor (5), a lower-layer liquid outlet (401) is arranged at the bottom of the extraction tank (4), and the driving motor (5) drives the extraction tank (4) to rotate, so that centrifugal extraction is realized.
Furthermore, a material inlet (6) and an upper layer liquid outlet (7) are arranged at the top of the extraction tank (4), and switch valves (8) are arranged on the material inlet (6) and the upper layer liquid outlet (7).
Furthermore, the bottom of blending tank (3) be provided with first flexible pipe (9), first flexible pipe (9) on be provided with ooff valve (8), first flexible pipe (9) be connected with first electric motor (10), first electric motor (10) drive the flexible from top to bottom of first flexible pipe (9), first flexible pipe (9) be located the material import directly over, first electric motor install on support (11).
Furthermore, a second telescopic pipe (12) is arranged above the upper layer liquid outlet (7), the second telescopic pipe (12) is connected with a second electric motor (13), the second electric motor (13) drives the second telescopic pipe (12) to move up and down, the second telescopic pipe (12) is connected with a pump (14) to pump out the upper layer liquid, and the second electric motor (13) is arranged on the support (11).
Furthermore, a bearing is arranged in the middle of the extraction tank (4), two ends of the bearing are fixed on the bracket,
furthermore, a strip-shaped transparent window (403) is arranged on the side wall of the extraction tank (4), and the strip-shaped transparent window (403) is strip-shaped from top to bottom along the side wall of the extraction tank.
Further, a switch valve (8) is arranged on the lower layer liquid outlet (401) to control the discharge of the lower layer liquid.
The utility model has the advantages that: the utility model provides an extract and centrifugation completion in same container among the extraction device, adjust the joining proportion of extractant and material simultaneously through the measuring pump, be provided with at the top and go up and down to take out the pipeline, guarantee that the bottom material flows from below, upper material from the upper strata is taken out, is provided with the bar perspective hole to detect the position of liquid level. The utility model has the advantages of structural design is reasonable, extraction efficiency is high, extraction effect is good.
Drawings
Fig. 1 is a schematic structural diagram of an extraction device of 1-phenylpyridine according to an embodiment of the present invention.
The device comprises a material storage tank 1, an extractant storage tank 2, a mixing tank 3, a metering pump 301, a stirring paddle 302, a motor 303, an extraction tank 4, a lower-layer liquid outlet 401, a strip-shaped transparent window 403, a driving motor 5, a material inlet 56, an upper-layer liquid outlet 7, a switch valve 8, a first telescopic pipe 9, a first electric motor 10, a support 11, a second telescopic pipe 12, a second electric motor 13, a pump 14 and a bearing 15.
The specific implementation mode is as follows:
in order to deepen understanding of the present invention, the following detailed description is made on the embodiments of the present invention with reference to the accompanying drawings.
It should be understood that the structure, ratio, size and the like shown in the drawings attached to the present specification are only used for matching with the content disclosed in the specification, so as to be known and read by those skilled in the art, and are not used for limiting the limit conditions that the present invention can be implemented, so that the present invention has no technical essential meaning, and any structure modification, ratio relation change or size adjustment should still fall within the scope that the technical content disclosed in the present invention can cover without affecting the function and the achievable purpose of the present invention.
Examples
With reference to figure 1 of the drawings,
a1-phenylpyridine extraction device comprises a material storage tank 1, an extractant storage tank 2, a mixing tank 3 and an extraction tank 4, wherein the material storage tank 1 and the extractant storage tank 2 are connected with the mixing tank 3 through pipelines, a metering pump 301 is installed on the pipeline, the mixing tank 3 is connected with the extraction tank 4, a stirring paddle 302 is installed inside the mixing tank 3, a motor 303 is arranged at the top of the mixing tank 3, and the motor 303 drives the stirring paddle 302 to stir;
the bottom of extraction jar 4 is the U type, and the minimum point of the bottom of extraction jar 4 is connected with driving motor 5, is provided with lower floor's liquid outlet 401 on the bottom of extraction jar 4, and driving motor 5 drives the rotation of extraction jar 4 to realize centrifugal extraction.
Further, the top of the extraction tank 4 is provided with a material inlet 6 and an upper layer liquid outlet 7, and the material inlet 6 and the upper layer liquid outlet 7 are both provided with a switch valve 8.
Furthermore, a first telescopic pipe 9 is arranged at the bottom end of the mixing tank 3, a switch valve 8 is arranged on the first telescopic pipe 9, the first telescopic pipe 9 is connected with a first electric motor 10, the first electric motor 10 drives the first telescopic pipe 9 to extend and retract up and down, the first telescopic pipe 9 is positioned right above the material inlet, and the first electric motor is arranged on a support 11.
Furthermore, a second telescopic pipe 12 is arranged above the upper layer liquid outlet 7, the second telescopic pipe 12 is connected with a second electric motor 13, the second electric motor 13 drives the second telescopic pipe 12 to move up and down, the second telescopic pipe 12 is connected with a pump 14 to pump out the upper layer liquid, and the second electric motor 13 is arranged on the support 11.
Furthermore, the middle part of the extraction tank 4 is provided with a bearing, two ends of the bearing are fixed on the bracket,
further, a strip-shaped transparent window 403 is arranged on the side wall of the extraction tank 4, and the strip-shaped transparent window 403 is strip-shaped from top to bottom along the side wall of the extraction tank.
Further, an on-off valve 8 is disposed on the lower layer liquid outlet 401 to control the discharge of the lower layer liquid.
In the use, put into the blending tank intensive mixing with material and extractant, then, through adjusting electric motor, make first flexible pipe extension, stretch into the material import with first flexible pipe, get into the extraction jar with the material, with first flexible pipe withdrawal, close the ooff valve on the material import, carry out the centrifugation, the centrifugation finishes, open the ooff valve of extraction jar bottom, emit lower floor's liquid, when getting rid of upper liquid, stretch into upper liquid export with the scalable pipe of second, take upper liquid out, thereby realize the centrifugal extraction process.
To extract and the centrifugation is accomplished in same container among this extraction device, adjusts the proportion of adding of extractant and material simultaneously through the measuring pump, is provided with the lift at the top and takes out the pipeline, guarantees that the bottom material flows from below, and the upper material is taken out from the upper strata, is provided with the bar and sees through the hole to detect the position of liquid level. The utility model has the advantages of structural design is reasonable, extraction efficiency is high, extraction effect is good.
The technical means disclosed by the scheme of the utility model is not limited to the technical means disclosed by the technical means, but also comprises the technical scheme consisting of the equivalent replacement of the technical features. The present invention is not to be considered as the best thing, and belongs to the common general knowledge of the technicians in the field.
Claims (7)
1. The extraction device of the 1-phenylpyridine is characterized by comprising a material storage tank (1), an extracting agent storage tank (2), a mixing tank (3) and an extraction tank (4), wherein the material storage tank (1) and the extracting agent storage tank (2) are connected with the mixing tank (3) through a pipeline, a metering pump (301) is installed on the pipeline, the mixing tank (3) is connected with the extraction tank (4), a stirring paddle (302) is installed inside the mixing tank (3), a motor (303) is arranged at the top of the mixing tank (3), and the motor (303) drives the stirring paddle (302) to stir;
the bottom of the extraction tank (4) is U-shaped, the lowest point of the bottom of the extraction tank (4) is connected with a driving motor (5), a lower-layer liquid outlet (401) is arranged at the bottom of the extraction tank (4), and the driving motor (5) drives the extraction tank (4) to rotate, so that centrifugal extraction is realized.
2. The extraction device of 1-phenylpyridine according to claim 1, characterized in that the top of the extraction tank (4) is provided with a material inlet (6) and an upper liquid outlet (7), and the material inlet (6) and the upper liquid outlet (7) are both provided with a switch valve (8).
3. The extraction device of 1-phenylpyridine according to claim 2, characterized in that the bottom end of the mixing tank (3) is provided with a first telescopic pipe (9), the first telescopic pipe (9) is provided with a switch valve (8), the first telescopic pipe (9) is connected with a first electric motor (10), the first electric motor (10) drives the first telescopic pipe (9) to extend and retract up and down, the first telescopic pipe (9) is positioned right above the material inlet, and the first electric motor is mounted on a support (11).
4. A device for extracting 1-phenylpyridine according to claim 3, characterized in that a second telescopic tube (12) is arranged above the upper liquid outlet (7), said second telescopic tube (12) is connected with a second electric motor (13), said second electric motor (13) drives the second telescopic tube (12) to move up and down, said second telescopic tube (12) is connected with a pump (14) to pump the upper liquid out, said second electric motor (13) is arranged on the support (11).
5. The extraction device of 1-phenylpyridine according to claim 4, characterized in that the middle of the extraction tank (4) is provided with a bearing, and the two ends of the bearing are fixed on a bracket.
6. The extraction device of 1-phenylpyridine according to claim 1, characterized in that the side wall of the extraction tank (4) is provided with a strip-shaped transparent window (403), and the strip-shaped transparent window (403) is strip-shaped from top to bottom along the side wall of the extraction tank.
7. An extraction apparatus according to claim 1, wherein the lower liquid outlet (401) is provided with a switch valve (8) to control the discharge of the lower liquid.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202022994841.2U CN214808592U (en) | 2020-12-14 | 2020-12-14 | Extraction device of 1-phenylpyridine |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202022994841.2U CN214808592U (en) | 2020-12-14 | 2020-12-14 | Extraction device of 1-phenylpyridine |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN214808592U true CN214808592U (en) | 2021-11-23 |
Family
ID=78802955
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202022994841.2U Expired - Fee Related CN214808592U (en) | 2020-12-14 | 2020-12-14 | Extraction device of 1-phenylpyridine |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN214808592U (en) |
-
2020
- 2020-12-14 CN CN202022994841.2U patent/CN214808592U/en not_active Expired - Fee Related
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| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20211123 |