CN214782184U - Device for preparing high-purity beryllium by fused salt electrolysis - Google Patents
Device for preparing high-purity beryllium by fused salt electrolysis Download PDFInfo
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- CN214782184U CN214782184U CN202120611691.4U CN202120611691U CN214782184U CN 214782184 U CN214782184 U CN 214782184U CN 202120611691 U CN202120611691 U CN 202120611691U CN 214782184 U CN214782184 U CN 214782184U
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Abstract
The utility model discloses a device of high-purity beryllium of fused salt electrolysis preparation, including under casing and top case, the inside fixed mounting of under casing has the nickel crucible, and the top of nickel crucible both sides all communicates and has the electrolyte to advance the pipe, and the bottom intercommunication of nickel crucible has two electrolyte exit tubes, and the outside fixed mounting of nickel crucible has the resistance furnace, and the inside fixed mounting of nickel crucible has the mount pad, and the inside movable mounting of mount pad has positive pole diaphragm bag, and the inside of top case has been seted up the beryllium and has been drawed the room. Can carry out the rolling to the wire through the driving motor and the winding rod that set up to cathode nickel system drum and the positive pole industry beryllium board after finishing the electrolysis take out from electrolyte solution, do not need the manual work to take out, it is convenient to take out, conveniently extract high-purity beryllium, top case movable mounting can remove at the top of under casing in addition at the top of under casing, conveniently take out high-purity beryllium on the one hand, on the other hand accomplishes the back at the electrolysis, conveniently washs the inside of device main part, convenient next use.
Description
Technical Field
The utility model belongs to the technical field of the beryllium preparation, concretely relates to device of high-purity beryllium of fused salt electrolysis preparation.
Background
Beryllium is an indispensable precious material in the atomic energy, rocket, missile, aviation, space navigation and metallurgical industry, is widely applied to the fields of aerospace manufacturing and the like because of low density, good corrosion resistance and mechanical properties and excellent biocompatibility, and is called high-purity beryllium with the beryllium content of 3N or more, and a molten salt electrolysis method is one of the main methods for producing high-purity beryllium.
Most of the existing high-purity beryllium production devices place a cathode nickel cylinder and an anode industrial beryllium plate in the same electrolyte solution, and after the electrolytic reaction lasts for a period of time, the components of the electrolyte are easy to change, which can affect the quality of the high-purity beryllium.
SUMMERY OF THE UTILITY MODEL
Aiming at the defects existing in the prior art, the utility model aims to provide a device for preparing high-purity beryllium by electrolyzing molten salt, which solves the problems of influencing the quality of the high-purity beryllium and being inconvenient to take out.
In order to achieve the above object, the utility model provides a following technical scheme: a device for preparing high-purity beryllium through fused salt electrolysis comprises a bottom box and a top box, wherein a nickel crucible is fixedly arranged in the bottom box, electrolyte inlet pipes are communicated with the tops of two sides of the nickel crucible, two electrolyte outlet pipes are communicated with the bottom of the nickel crucible, a resistance furnace is fixedly arranged on the outer side of the nickel crucible, a mounting seat is fixedly arranged in the nickel crucible, an anode diaphragm bag is movably arranged in the mounting seat, a beryllium extraction chamber is arranged in the top box, a battery is fixedly arranged at the top of the beryllium extraction chamber, an anode of the battery is connected with an anode beryllium industrial plate through a lead, a cathode of the battery is connected with a cathode nickel cylinder through a lead, two circular holes are formed in the top of the top box, a top plate is movably arranged at the top of the top box, two argon inlet pipes are fixedly arranged in the top plate, and a motor box is fixedly arranged on one side of the top box, the inside fixed mounting of motor case has driving motor, driving motor's output fixed mounting has the winding rod, the positive fixed mounting of top case has control panel.
Preferably, the bottom fixed mounting of top case has the type of falling T slider, the spout has been seted up at the top of under casing, and the specification and size of spout and the specification and size looks adaptation of the type of falling T slider, the type of falling T slider slidable mounting is in the inside of spout.
Preferably, two specification sizes that the argon gas advances the pipe and specification sizes looks adaptation of two circular ports, and the position that the argon gas advances the pipe and the position of circular port is corresponding, the argon gas advances the pipe and runs through the top of overhead bin through the circular port to extend to the inside of beryllium extraction room.
Preferably, valves are fixedly installed inside the electrolyte inlet pipe and the electrolyte outlet pipe.
Preferably, the inside fixed mounting of motor case has the fixed plate, driving motor fixed mounting is in the inside of fixed plate, the access door is installed in the front of motor case.
Preferably, the bottom fixed mounting of under casing has the supporting leg, the supporting leg has four, and four supporting legs are the bottom of rectangle symmetric distribution at the under casing.
Compared with the prior art, the beneficial effects of the utility model are that:
1. can carry out the rolling to the wire through the driving motor and the winding rod that set up, thereby take out cathode nickel system drum and the positive pole industry beryllium board after finishing the electrolysis from electrolyte solution, do not need the manual work to take out, prevent that the staff from contacting electrolyte solution, it is convenient to take out, conveniently extract high-purity beryllium, top case movable mounting is at the top of under casing in addition, the top case can remove at the top of under casing, conveniently take out high-purity beryllium on the one hand, on the other hand is after the electrolysis is accomplished, conveniently wash inside the device main part, convenient next use.
2. The electrolyte which does not have electrolytic reaction can be isolated from the electrolyte which has electrolytic reaction through the arranged anode diaphragm bag, the electrolyte and the electrolyte are prevented from being mixed together to react, the components of the electrolyte solution are prevented from changing, the electrolytic reaction process is more stable, the quality of high-purity beryllium is improved, and the problem that the components of the electrolyte are easy to change after the cathode nickel cylinder and the anode industrial beryllium plate are placed in the same electrolyte solution and the electrolytic reaction is carried out for a period of time is solved.
Drawings
Fig. 1 is a schematic view of the three-dimensional appearance structure of the present invention;
FIG. 2 is a schematic view of the internal structure of the bottom case of the present invention;
fig. 3 is a schematic view of the internal structure of the top box of the present invention.
In the figure: 1. a bottom box; 2. a top box; 3. a motor case; 4. an access door; 5. an electrolyte inlet pipe; 6. supporting legs; 7. a top plate; 8. argon gas is fed into the tube; 9. a control panel; 10. a nickel crucible; 11. an electrolyte outlet pipe; 12. a mounting seat; 13. an anode separator bag; 14. a beryllium extraction chamber; 15. making a cylinder by cathode nickel; 16. a wire winding rod; 17. an anodic industrial beryllium plate; 18. an inverted T-shaped slider; 19. a drive motor; 20. a fixing plate; 21. a battery; 22. a circular hole; 23. and (4) a resistance furnace.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
The first embodiment is as follows:
referring to fig. 1-3, the present invention provides a technical solution: a device for preparing high-purity beryllium by fused salt electrolysis comprises a bottom box 1 and a top box 2, wherein a nickel crucible 10 is fixedly arranged in the bottom box 1, the tops of two sides of the nickel crucible 10 are respectively communicated with an electrolyte inlet pipe 5, the bottom of the nickel crucible 10 is communicated with two electrolyte outlet pipes 11, a resistance furnace 23 is fixedly arranged on the outer side of the nickel crucible 10, a mounting seat 12 is fixedly arranged in the nickel crucible 10, an anode diaphragm bag 13 is movably arranged in the mounting seat 12, a beryllium extraction chamber 14 is arranged in the top box 2, a battery 21 is fixedly arranged at the top of the beryllium extraction chamber 14, an anode industrial beryllium plate 17 is connected with an anode of the battery 21 through a positive lead, a cathode of the battery 21 is connected with a cathode nickel cylinder 15 through a lead, two round holes 22 are arranged at the top of the top box 2, a top plate 7 is movably arranged at the top of the top box 2, two argon inlet pipes 8 are fixedly arranged in the top plate 7, one side fixed mounting of top case 2 has motor case 3, and the inside fixed mounting of motor case 3 has driving motor 19, and driving motor 19's output fixed mounting has winding rod 16, and the front fixed mounting of top case 2 has control panel 9.
In the embodiment, firstly, electrolyte solution is added into a nickel crucible 10 in a bottom box 1 through an electrolyte inlet pipe 5, after the addition is finished, a driving motor 19 is started to rotate reversely to drive a winding rod 16 to rotate reversely, a lead is released, a cathode nickel cylinder 15 and an anode industrial beryllium plate 17 are immersed into the electrolyte solution in the nickel crucible 10, then an external argon supply device is externally connected through two argon inlet pipes 8, argon is added into a beryllium extraction chamber 14 and the nickel crucible 10, then equipment is started to carry out electrolysis through a control panel 9, high-purity beryllium is extracted, the electrolyte which does not carry out the electrolysis reaction and the electrolyte which carries out the electrolysis reaction can be isolated through an anode diaphragm bag 13, the two are prevented from being mixed together to carry out the reaction, the components of the electrolyte solution are prevented from being changed, the process of the electrolysis reaction is more stable, the quality of the high-purity beryllium is improved, the problem that the cathode nickel cylinder 15 and the anode industrial beryllium plate 17 are placed in the same electrolyte solution is solved, after electrolytic reaction a period of time, the easy problem that changes of composition of electrolyte, after the electrolysis finishes, start driving motor 19 and carry out corotation, drive winding rod 16 and carry out the corotation, roll up the wire, thereby take out negative pole nickel system drum 15 and positive pole industry beryllium board 17 after finishing the electrolysis from the electrolyte solution, do not need the manual work to take out, prevent that the staff from contacting the electrolyte solution, it is convenient to take out, then promote top case 2, make the inside slip of spout at bottom case 1 top of the type of falling T slider 18 of top case 2 bottom, thereby the opening device, conveniently take out high-purity beryllium on the one hand, on the other hand is after the electrolysis is accomplished, conveniently wash the inside of device main part, make things convenient for next use.
Example two:
as shown in fig. 1-3, on the basis of the first embodiment, the utility model provides a technical solution: the bottom fixed mounting of top case 2 has inverted T type slider 18, and the spout has been seted up at the top of under casing 1, and the specification and dimension of spout and the specification and dimension looks adaptation of inverted T type slider 18, and inverted T type slider 18 slidable mounting is in the inside of spout.
In this embodiment, promote top case 2, make the type of falling T slider 18 of top case 2 bottom slide in the spout at bottom case 1 top inside to the opening device conveniently takes out high-purity beryllium on the one hand, and on the other hand is convenient after the electrolysis is accomplished to inside the washing of device main part, makes things convenient for next use.
Example three:
as shown in fig. 1-3, on the basis of the first embodiment and the second embodiment, the utility model provides a technical solution: specification and dimension of two argon gas inlet pipes 8 and specification and dimension looks adaptation of two circular ports 22, and the position that argon gas inlet pipe 8 and circular port 22 are corresponding, argon gas inlet pipe 8 runs through the top of roof box 2 through circular port 22, and extend to the inside that beryllium extracted room 14, the equal fixed mounting in inside that the electrolyte entered pipe 5 and electrolyte exit tube 11 has the valve, the inside fixed mounting of motor case 3 has fixed plate 20, 19 fixed mounting of driving motor is in the inside of fixed plate 20, access door 4 is installed in the front of motor case 3.
In this embodiment, two argon inlet pipes 8 are externally connected with an external argon supply device, argon is added into the beryllium extraction chamber 14 and the nickel crucible 10, and the access door 4 is used for conveniently overhauling the driving motor 19 in the motor box 3.
Example four:
as shown in fig. 1-3, on the basis of the first embodiment, the second embodiment and the third embodiment, the utility model provides a technical solution: the bottom fixed mounting of under casing 1 has supporting leg 6, and supporting leg 6 has four, and four supporting legs 6 are rectangle symmetric distribution in the bottom of under casing 1.
In this embodiment, the support legs 6 serve to support the apparatus as a whole.
The utility model discloses a theory of operation and use flow: firstly, electrolyte solution is added into a nickel crucible 10 in a bottom box 1 through an electrolyte inlet pipe 5, after the addition is finished, a driving motor 19 is started to rotate reversely to drive a winding rod 16 to rotate reversely, a lead is released to enable a cathode nickel cylinder 15 and an anode industrial beryllium plate 17 to be immersed into the electrolyte solution in the nickel crucible 10, then an external argon supply device is connected through two argon inlet pipes 8, argon is added into a beryllium extraction chamber 14 and the nickel crucible 10, then equipment is started to carry out electrolysis through a control panel 9 to extract high-purity beryllium, electrolyte which does not carry out electrolytic reaction and electrolyte which carries out electrolytic reaction can be isolated through an arranged anode diaphragm bag 13, the electrolyte and the electrolyte are prevented from being mixed together to react, the components of the electrolyte solution are prevented from being changed, the electrolytic reaction process is more stable, the quality of the high-purity beryllium is improved, the problem that the cathode nickel cylinder 15 and the anode industrial beryllium plate 17 are placed in the same electrolyte solution is solved, after electrolytic reaction a period of time, the easy problem that changes of composition of electrolyte, after the electrolysis finishes, start driving motor 19 and carry out corotation, drive winding rod 16 and carry out the corotation, roll up the wire, thereby take out negative pole nickel system drum 15 and positive pole industry beryllium board 17 after finishing the electrolysis from the electrolyte solution, do not need the manual work to take out, prevent that the staff from contacting the electrolyte solution, it is convenient to take out, then promote top case 2, make the inside slip of spout at bottom case 1 top of the type of falling T slider 18 of top case 2 bottom, thereby the opening device, conveniently take out high-purity beryllium on the one hand, on the other hand is after the electrolysis is accomplished, conveniently wash the inside of device main part, make things convenient for next use.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (6)
1. The utility model provides a device of fused salt electrolysis preparation high-purity beryllium, includes bottom case (1) and top case (2), its characterized in that: a nickel crucible (10) is fixedly arranged in the bottom box (1), the tops of two sides of the nickel crucible (10) are communicated with an electrolyte inlet pipe (5), the bottom of the nickel crucible (10) is communicated with two electrolyte outlet pipes (11), a resistance furnace (23) is fixedly arranged on the outer side of the nickel crucible (10), a mounting seat (12) is fixedly arranged in the nickel crucible (10), an anode diaphragm bag (13) is movably arranged in the mounting seat (12), a beryllium extraction chamber (14) is arranged in the top box (2), a battery (21) is fixedly arranged at the top of the beryllium extraction chamber (14), the positive electrode of the battery (21) is connected with an anode industrial beryllium plate (17) through a lead, the negative electrode of the battery (21) is connected with a cathode nickel cylinder (15) through a lead, and the top of the top box (2) is provided with two circular holes (22), the top movable mounting of top case (2) has roof (7), the inside fixed mounting of roof (7) has two argon gas to advance pipe (8), one side fixed mounting of top case (2) has motor case (3), the inside fixed mounting of motor case (3) has driving motor (19), the output fixed mounting of driving motor (19) has winding pole (16), the positive fixed mounting of top case (2) has control panel (9).
2. The apparatus of claim 1 for preparing high-purity beryllium by molten salt electrolysis, which is characterized in that: the bottom fixed mounting of top case (2) has type of falling T slider (18), the spout has been seted up at the top of under casing (1), and the specification and size of spout and the specification and size looks adaptation of type of falling T slider (18), type of falling T slider (18) slidable mounting is in the inside of spout.
3. The apparatus of claim 1 for preparing high-purity beryllium by molten salt electrolysis, which is characterized in that: two specification and dimension that argon gas advances pipe (8) and specification and dimension looks adaptation of two circular ports (22), and the position that argon gas advances pipe (8) and circular port (22) correspond, argon gas advances pipe (8) and runs through the top of overhead bin (2) through circular port (22) to extend to the inside of beryllium extraction room (14).
4. The apparatus of claim 1 for preparing high-purity beryllium by molten salt electrolysis, which is characterized in that: and valves are fixedly arranged in the electrolyte inlet pipe (5) and the electrolyte outlet pipe (11).
5. The apparatus of claim 1 for preparing high-purity beryllium by molten salt electrolysis, which is characterized in that: the inside fixed mounting of motor case (3) has fixed plate (20), driving motor (19) fixed mounting is in the inside of fixed plate (20), access door (4) are installed in the front of motor case (3).
6. The apparatus of claim 1 for preparing high-purity beryllium by molten salt electrolysis, which is characterized in that: the bottom fixed mounting of under casing (1) has supporting leg (6), supporting leg (6) have four, and four supporting legs (6) are the bottom of rectangle symmetric distribution at under casing (1).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202120611691.4U CN214782184U (en) | 2021-03-25 | 2021-03-25 | Device for preparing high-purity beryllium by fused salt electrolysis |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202120611691.4U CN214782184U (en) | 2021-03-25 | 2021-03-25 | Device for preparing high-purity beryllium by fused salt electrolysis |
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| Publication Number | Publication Date |
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| CN214782184U true CN214782184U (en) | 2021-11-19 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN202120611691.4U Active CN214782184U (en) | 2021-03-25 | 2021-03-25 | Device for preparing high-purity beryllium by fused salt electrolysis |
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| CN (1) | CN214782184U (en) |
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- 2021-03-25 CN CN202120611691.4U patent/CN214782184U/en active Active
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