CN214486870U - Polyaniline apparatus for producing - Google Patents
Polyaniline apparatus for producing Download PDFInfo
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- CN214486870U CN214486870U CN202023028971.7U CN202023028971U CN214486870U CN 214486870 U CN214486870 U CN 214486870U CN 202023028971 U CN202023028971 U CN 202023028971U CN 214486870 U CN214486870 U CN 214486870U
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Abstract
The utility model relates to a polyaniline production technical field just discloses a polyaniline apparatus for producing, including reation kettle, reation kettle's right side is provided with cooling device, reation kettle's upper surface left side is fixed with the inlet pipe, reation kettle's upper surface right side is fixed with the outlet duct, reation kettle's upper surface middle part is fixed with the motor, the output of motor is fixed with the puddler, the one end that the motor was kept away from to the puddler runs through reation kettle's upper surface and is located reation kettle's inside, the surface mounting of puddler has the blade, reation kettle's interior diapire is fixed with the cooling tube, reation kettle's lower fixed surface has the base. This polyaniline apparatus for producing, through the cooperation that sets up honeycomb duct, tubular metal resonator and first refrigerator, can derive reaction liquid through the honeycomb duct, carries out cooling to reaction liquid through tubular metal resonator conduction temperature, avoids the interior high temperature pressure of reation kettle too big, has improved the device's security.
Description
Technical Field
The utility model relates to a polyaniline production technical field specifically is a polyaniline apparatus for producing.
Background
Polyaniline has the characteristics of cheap raw materials, simple and convenient synthesis, stable product performance, high conductivity, excellent corrosion resistance and the like, is widely applied to the fields of electronic products, luminescent materials, batteries, electrostatic shielding, microwave absorption, metal corrosion resistance and the like, and is a high polymer material with high commercial application value.
The prior polyaniline production device has large heat generated in the polymerization process, the temperature of the device rises quickly and the heat dissipation is slow, and although measures such as external cooling are adopted, the heat dissipation efficiency is low due to slow heat transfer, so that the production requirement can not be met.
SUMMERY OF THE UTILITY MODEL
Technical problem to be solved
To prior art's not enough in the above-mentioned background art, the utility model provides a polyaniline apparatus for producing to overcome the current polyaniline apparatus for producing who proposes in the above-mentioned background art, the heat that produces in polymerization process is big, and the temperature of device risees fast, the heat dissipation is slow, though adopted measures such as external cooling, nevertheless because the heat transfer leads to the radiating efficiency low slowly, can not satisfy the shortcoming of production needs.
(II) technical scheme
In order to achieve the above purpose, the utility model discloses a following technical scheme realizes:
a polyaniline production device comprises a reaction kettle, wherein a cooling device is arranged on the right side of the reaction kettle;
a feeding pipe is fixed on the left side of the upper surface of the reaction kettle, an air outlet pipe is fixed on the right side of the upper surface of the reaction kettle, a motor is fixed in the middle of the upper surface of the reaction kettle, a stirring rod is fixed at the output end of the motor, one end, far away from the motor, of the stirring rod penetrates through the upper surface of the reaction kettle and is located inside the reaction kettle, blades are fixed on the outer surface of the stirring rod, a cooling pipe is fixed on the inner bottom wall of the reaction kettle, a base is fixed on the lower surface of the reaction kettle, a discharging pipe is fixed on the left side of the reaction kettle, a flow guide pipe is fixed at the bottom of the right side of the reaction kettle, a metal pipe is sleeved on the outer surface of the flow guide pipe, and a first refrigerating machine is fixed in the middle of the lower surface of the metal pipe;
the cooling device comprises a water collecting tank, wherein a second refrigerator is fixed on the front side and the back top end of the water collecting tank, an air conditioning through pipe is fixed at the output end of the second refrigerator, a guide pump is fixed at the front end of the bottom on the right side of the water collecting tank, a return pipe is fixed at the output end of the guide pump, one end, far away from the guide pump, of the return pipe is fixed with the top of the left side of the reaction kettle, and one end, far away from the guide pump, of the return pipe is communicated with the inner cavity of the reaction kettle.
As an optimal technical solution of the utility model: the standing groove has been seted up to the upper surface of base, the inner wall of standing groove and reation kettle's surface contact can make reation kettle more stable place on the base like this, increase reation kettle's stability.
As an optimal technical solution of the utility model: the top inner wall of outlet duct is fixed with the filter screen, the filter screen is located reation kettle's top, can filter solid particle through setting up the filter screen, avoids direct discharge to cause the influence to the air.
Further, the inlet pipe is communicated with the inner cavity of the reaction kettle, and the outlet pipe is communicated with the inner cavity of the reaction kettle.
Further, the blades are located inside the reaction kettle and are uniformly distributed on the stirring rod.
Further, the discharging pipe is communicated with an inner cavity of the reaction kettle, a valve is mounted on the discharging pipe, the flow guide pipe is communicated with the inner cavity of the reaction kettle, and the inner wall of the metal pipe is in contact with the outer surface of the flow guide pipe.
Furthermore, the end of the cold air through pipe far away from the second refrigerator is positioned in the water collecting pool, and the input end of the guide pump is connected with the end of the guide pipe far away from the reaction kettle.
The working principle of the polyaniline production device is that when the polyaniline production device is needed to be used, raw materials are firstly introduced into a reaction kettle from a feed pipe, then the motor is started to drive the stirring rod and the blades to rotate to stir the solution, so as to accelerate the reaction speed of the solution, meanwhile, the first refrigerator is started to cool the metal pipe, the second refrigerator is started to cool the water in the water collecting pool, then the guide pump is started, the reaction liquid is cooled for the first time through the cooling pipe by the guide of the guide pump, then passes through the metal pipe by the guide pipe and then passes through the water collecting tank, the reaction liquid is continuously cooled for a plurality of times, and finally enters the reaction kettle through the return pipe, the overhigh temperature in the reaction kettle is relieved, the safety of the device is improved, after the reaction is finished, and (4) closing the motor, the first refrigerator, the second refrigerator and the guide pump, opening the valve after the reaction liquid is stable, and leading out the reaction liquid from the discharge pipe.
The electrical components presented therein may be electrically connected to an external controller, and the controller may be electrically connected to an external 220V commercial power, and the controller may be a conventional known device for controlling a computer or the like.
(III) advantageous effects
The utility model provides a polyaniline apparatus for producing possesses following beneficial effect:
(1) this polyaniline apparatus for producing, through the cooperation that sets up honeycomb duct, tubular metal resonator and first refrigerator, can derive reaction liquid through the honeycomb duct, carries out cooling to reaction liquid through tubular metal resonator conduction temperature, avoids the interior high temperature pressure of reation kettle too big, has improved the device's security.
(2) This polyaniline apparatus for producing through setting up the cooperation between catch basin, second refrigerator and the air conditioning siphunculus, can cool down to the water in the catch basin to the cooling to reaction liquid through setting up the setting of guiding pump and back flow, can carry out the mobile of circulation to reaction liquid, reduce the pressure in the reation kettle, increase the device's stability and security.
Drawings
FIG. 1 is a schematic perspective view of a polyaniline production apparatus according to the present invention;
FIG. 2 is a schematic view of the front view structure of the polyaniline production apparatus of the present invention;
FIG. 3 is a schematic diagram of a side view of the polyaniline production apparatus of the present invention;
FIG. 4 is a schematic cross-sectional view of a polyaniline production apparatus according to the present invention;
fig. 5 is a schematic view of the three-dimensional structure of the water collecting tank of the polyaniline production apparatus of the present invention.
In the figure: 1. a reaction kettle; 2. a cooling device; 3. a feed pipe; 4. an air outlet pipe; 5. a motor; 6. a stirring rod; 7. a blade; 8. a cooling tube; 9. a base; 10. a discharge pipe; 11. a flow guide pipe; 12. a metal tube; 13. a first refrigerator; 14. a water collecting tank; 15. a second refrigerator; 16. a cold air through pipe; 17. a diversion pump; 18. a return pipe.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments.
Referring to fig. 1-5, the present invention provides a polyaniline production apparatus;
as shown in figure 1, the reactor comprises a reaction kettle 1, wherein a cooling device 2 is arranged at the right side of the reaction kettle 1;
according to the illustration in fig. 2-4, a feed pipe 3 is fixed on the left side of the upper surface of a reaction kettle 1, the feed pipe 3 is communicated with the inner cavity of the reaction kettle 1, so that raw materials can be poured into the reaction kettle 1 from the feed pipe 3 conveniently, an outlet pipe 4 is fixed on the right side of the upper surface of the reaction kettle 1, the outlet pipe 4 is communicated with the inner cavity of the reaction kettle 1, a motor 5 is fixed in the middle of the upper surface of the reaction kettle 1, a stirring rod 6 is fixed at the output end of the motor 5, one end of the stirring rod 6, which is far away from the motor 5, penetrates through the upper surface of the reaction kettle 1 and is positioned inside the reaction kettle 1, blades 7 are fixed on the outer surface of the stirring rod 6, the blades 7 are positioned inside the reaction kettle 1, a plurality of the blades 7 are arranged, the blades 7 are uniformly distributed on the stirring rod 6, the blades 7 are arranged to make the solution mixed more uniform and the reaction more complete, a cooling pipe 8 is fixed on the inner bottom wall of the reaction kettle 1, a base 9 is fixed on the lower surface of the reaction kettle 1, a discharge pipe 10 is fixed on the left side of the reaction kettle 1, the discharge pipe 10 is communicated with the inner cavity of the reaction kettle 1, a valve is mounted on the discharge pipe 10 to facilitate the taking out of reaction liquid, a guide pipe 11 is fixed on the bottom of the right side of the reaction kettle 1, the guide pipe 11 is communicated with the inner cavity of the reaction kettle 1, a metal pipe 12 is sleeved on the outer surface of the guide pipe 11, the inner wall of the metal pipe 12 is in contact with the outer surface of the guide pipe 11, so that the guide pipe 11 can be cooled through the metal pipe 12, and a first refrigerator 13 is fixed in the middle of the lower surface of the metal pipe 12;
as shown in fig. 4-5, the cooling device 2 includes a water collecting tank 14, a second refrigerator 15 is fixed on top of the front and back of the water collecting tank 14, a cold air duct 16 is fixed on the output end of the second refrigerator 15, one end of the cold air duct 16 far from the second refrigerator 15 is located in the water collecting tank 14, so as to cool the water in the water collecting tank 14 and maintain a certain temperature, meanwhile, the water in the water collecting tank 14 does not need to be changed in a flowing way, so that the resources are saved, the front end of the bottom on the right side of the water collecting tank 14 is fixedly provided with the guide pump 17, the input end of the guide pump 17 is connected with one end of the guide pipe 11 far away from the reaction kettle 1, the reaction liquid can circularly flow through the guide pump 17, so that the reaction liquid can be rapidly cooled, a return pipe 18 is fixed at the output end of the guide pump 17, one end of the return pipe 18, which is far away from the guide pump 17, is fixed with the top of the left side of the reaction kettle 1, and one end of the return pipe 18, which is far away from the guide pump 17, is communicated with the inner cavity of the reaction kettle 1;
as shown in fig. 1, a preferred embodiment of the present invention is: the upper surface of the base 9 is provided with a placing groove, and the inner wall of the placing groove is in contact with the outer surface of the reaction kettle 1, so that the reaction kettle 1 can be placed on the base 9 more stably, and the stability of the reaction kettle 1 is improved;
as shown in fig. 2, a preferred embodiment of the present invention is: the filter screen is fixed with to the top inner wall of outlet duct 4, and the filter screen is located reation kettle 1's top, can filter solid particle through setting up the filter screen, avoids direct discharge to cause the influence to the air.
It should be noted that, in the present invention, unless explicitly stated or limited otherwise, the terms "disposed," "mounted," "connected," and "fixed" are to be understood in a broad sense, and may be, for example, either fixedly or detachably connected; or indirectly through an intermediary. The specific meaning of the above terms in the present invention can be understood according to specific situations by those skilled in the art.
The above, only be the concrete implementation of the preferred embodiment of the present invention, but the protection scope of the present invention is not limited thereto, and any person skilled in the art is in the technical scope of the present invention, according to the technical solution of the present invention and the utility model, the concept of which is equivalent to replace or change, should be covered within the protection scope of the present invention.
Claims (7)
1. A polyaniline production device comprises a reaction kettle (1), and is characterized in that a cooling device (2) is arranged on the right side of the reaction kettle (1);
the upper surface left side of reation kettle (1) is fixed with inlet pipe (3), the upper surface right side of reation kettle (1) is fixed with outlet duct (4), the upper surface middle part of reation kettle (1) is fixed with motor (5), the output of motor (5) is fixed with puddler (6), the one end that motor (5) were kept away from in puddler (6) runs through the upper surface of reation kettle (1) and is located the inside of reation kettle (1), the external fixed surface of puddler (6) has blade (7), the interior diapire of reation kettle (1) is fixed with cooling tube (8), the lower fixed surface of reation kettle (1) has base (9), the left side of reation kettle (1) is fixed with discharging pipe (10), the right side bottom of reation kettle (1) is fixed with honeycomb duct (11), the surface cover of honeycomb duct (11) is equipped with metal pipe (12), a first refrigerator (13) is fixed in the middle of the lower surface of the metal pipe (12);
cooling device (2) include catch basin (14), the front and the back top of catch basin (14) all are fixed with second refrigerator (15), the output of second refrigerator (15) is fixed with air conditioning siphunculus (16), the bottom front end on catch basin (14) right side is fixed with guiding pump (17), the output of guiding pump (17) is fixed with back flow (18), the one end that guiding pump (17) were kept away from in back flow (18) is fixed with reation kettle (1) left side top, the one end that guiding pump (17) were kept away from in back flow (18) is linked together with reation kettle (1) inner chamber.
2. The polyaniline production apparatus as claimed in claim 1, wherein a placement groove is formed on the upper surface of the base (9), and the inner wall of the placement groove is in contact with the outer surface of the reaction kettle (1).
3. The polyaniline production apparatus as claimed in claim 1, wherein a filter screen is fixed to the inner wall of the top end of the gas outlet pipe (4), and the filter screen is located above the reaction kettle (1).
4. The polyaniline production apparatus as claimed in claim 1, wherein the feeding pipe (3) is in communication with the inner cavity of the reaction vessel (1), and the gas outlet pipe (4) is in communication with the inner cavity of the reaction vessel (1).
5. The polyaniline production apparatus as claimed in claim 1, wherein said blades (7) are located inside the reaction vessel (1), and said blades (7) are provided in plurality, and a plurality of said blades (7) are uniformly distributed on the stirring rod (6).
6. The polyaniline production apparatus as claimed in claim 1, wherein the discharge pipe (10) is in communication with the inner cavity of the reaction vessel (1), the discharge pipe (10) is provided with a valve, the flow guide pipe (11) is in communication with the inner cavity of the reaction vessel (1), and the inner wall of the metal pipe (12) is in contact with the outer surface of the flow guide pipe (11).
7. The polyaniline production apparatus as claimed in claim 1, wherein the end of the cold gas duct (16) away from the second refrigerator (15) is located in the water collecting tank (14), and the input end of the diversion pump (17) is connected to the end of the diversion pipe (11) away from the reaction vessel (1).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202023028971.7U CN214486870U (en) | 2020-12-16 | 2020-12-16 | Polyaniline apparatus for producing |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202023028971.7U CN214486870U (en) | 2020-12-16 | 2020-12-16 | Polyaniline apparatus for producing |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN214486870U true CN214486870U (en) | 2021-10-26 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202023028971.7U Active CN214486870U (en) | 2020-12-16 | 2020-12-16 | Polyaniline apparatus for producing |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN214486870U (en) |
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2020
- 2020-12-16 CN CN202023028971.7U patent/CN214486870U/en active Active
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20230704 Address after: Room 1125, Floor 11, Building 1, No. 85, Mingnan Road, Songjiang District, Shanghai, 201600 Patentee after: SHANGHAI GAOZHUN PHARMACEUTICAL Co.,Ltd. Address before: 510220 No. 28, Zhongnan Shi Road, Gongye Avenue, Haizhu District, Guangzhou, Guangdong Patentee before: Liu Shaobo |
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| TR01 | Transfer of patent right |