CN214486821U - Reaction device for preparing macroporous polyaspartic acid hydrogel - Google Patents
Reaction device for preparing macroporous polyaspartic acid hydrogel Download PDFInfo
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- CN214486821U CN214486821U CN202120400719.XU CN202120400719U CN214486821U CN 214486821 U CN214486821 U CN 214486821U CN 202120400719 U CN202120400719 U CN 202120400719U CN 214486821 U CN214486821 U CN 214486821U
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- 229920000805 Polyaspartic acid Polymers 0.000 title claims abstract description 25
- 108010064470 polyaspartate Proteins 0.000 title claims abstract description 25
- 239000000017 hydrogel Substances 0.000 title claims description 23
- 238000010438 heat treatment Methods 0.000 claims abstract description 22
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 claims description 20
- 229920001971 elastomer Polymers 0.000 claims description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 16
- 238000005192 partition Methods 0.000 claims description 11
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 10
- 230000001936 parietal effect Effects 0.000 claims 2
- 239000002994 raw material Substances 0.000 abstract description 23
- 230000000694 effects Effects 0.000 abstract description 12
- 239000011435 rock Substances 0.000 abstract description 4
- 230000035939 shock Effects 0.000 abstract 2
- 230000000149 penetrating effect Effects 0.000 description 6
- OKTJSMMVPCPJKN-BJUDXGSMSA-N carbon-11 Chemical class [11C] OKTJSMMVPCPJKN-BJUDXGSMSA-N 0.000 description 3
- UWFRVQVNYNPBEF-UHFFFAOYSA-N 1-(2,4-dimethylphenyl)propan-1-one Chemical compound CCC(=O)C1=CC=C(C)C=C1C UWFRVQVNYNPBEF-UHFFFAOYSA-N 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 102100035024 Carboxypeptidase B Human genes 0.000 description 1
- 101000946524 Homo sapiens Carboxypeptidase B Proteins 0.000 description 1
- 239000003431 cross linking reagent Substances 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000002105 nanoparticle Substances 0.000 description 1
- 230000010355 oscillation Effects 0.000 description 1
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 description 1
- 229920000053 polysorbate 80 Polymers 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 229910021642 ultra pure water Inorganic materials 0.000 description 1
- 239000012498 ultrapure water Substances 0.000 description 1
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Abstract
The utility model discloses a reaction unit for preparing macropore polyaspartic acid aquogel, including reaction shell, shock subassembly, fixed subassembly, standing groove and heating device, it is located to shock the subassembly reaction shell middle part, fixed subassembly through the round pin axle with reaction shell left side wall is articulated. The utility model discloses a set up the standing groove with when the staff uses whole reaction unit to vibrate the raw materials, will save the household utensils that have the raw materials and insert on the baffle place downthehole, control through control panel the motor operation drives simultaneously pivot rotation activity first conical gear with under the cooperation of second conical gear, drive first commentaries on classics rod with the second commentaries on classics rod rotation activity under the effect of ejector pin, make the standing groove rocks, thereby can be right the household utensils that store the raw materials in the standing groove vibrate, have improved staff's work efficiency.
Description
Technical Field
The utility model relates to the technical field of chemical industry. In particular to a reaction device for preparing macroporous polyaspartic acid hydrogel.
Background
When the polyaspartic acid hydrogel is prepared, raw materials such as linear polyaspartic acid and ethylene glycol diglycidyl ether need to be used, oil-phase cyclohexane needs to be added, but cyclohexane has pungent smell, is easy to stimulate a human body, is extremely easy to burn and volatilize, so that a vessel for storing cyclohexane needs to be fixed, and the vessel for storing cyclohexane is prevented from falling on the ground; and the steps of shaking, heating in water bath and the like are required to be carried out on the raw materials, so that a reaction device for preparing the macroporous polyaspartic acid hydrogel is provided.
SUMMERY OF THE UTILITY MODEL
Therefore, the technical problem to be solved by the present invention is to provide a reaction apparatus for preparing macroporous polyaspartic acid hydrogel with high safety and multiple functions.
In order to solve the technical problem, the utility model provides a following technical scheme:
a reaction device for preparing macroporous polyaspartic acid hydrogel comprises a reaction shell, a vibration component, a fixing component, a placing groove and a heating device, wherein the vibration component is positioned in the middle of the reaction shell, the fixing component is hinged with the left side wall of the reaction shell through a pin shaft, a reaction bin is arranged in the reaction shell, and the placing groove is positioned in the reaction bin;
the heating device is positioned on the inner bottom wall of the placing groove, a partition plate is clamped on the inner side wall of the placing groove, clear water is arranged between the partition plate and the heating device, the outer side wall of the placing groove is fixedly connected with a first spring, and the other end of the first spring is fixedly connected to the inner side wall of the reaction shell;
the reaction shell is characterized in that a third groove is formed in the top of a boss convexly arranged at the left end of the reaction shell, activated carbon is arranged in the third groove, and the activated carbon is located under the fixed component.
According to the reaction device for preparing the macroporous polyaspartic acid hydrogel, the number of the first springs is two or more, the two or more first springs are divided into two groups, one group of the first springs is positioned between the outer side wall of the placing groove and the inner side wall of the reaction shell, the other group of the first springs is positioned between the outer bottom wall of the placing groove and the inner bottom wall of the reaction shell, and a placing bin is arranged in the placing groove;
the surface of the clapboard is provided with placing holes, rubber rings are glued in the placing holes, the number of the placing holes is two or more, and the placing holes are arranged on the clapboard;
the outer roof of reaction shell can dismantle through fixing bolt and be connected with the hinge, just reaction shell passes through hinge swing joint has the door, door right side top fixedly connected with handle, the outer diapire fixedly connected with base of reaction shell, the base is total four, and waits to all arrange the outer diapire of reaction shell.
The reaction device for preparing the macroporous polyaspartic acid hydrogel comprises a vibration assembly, a vibration assembly and a rotating shaft, wherein the rotating shaft is arranged in a bearing in the middle of the bottom wall of the reaction shell in a penetrating mode, the first rubber pad is located right below the rotating shaft, the top end of the first rubber pad is glued with a motor, an output shaft of the motor is in driving connection with the bottom end of the rotating shaft, the top end of the rotating shaft is fixedly connected with a first rotating rod, a top rod is welded on the side wall of the first rotating rod, and the top end of the first rotating rod is arranged in a bearing on the inner top wall of the left side of the reaction shell in a penetrating mode;
a first conical gear is sleeved in the middle of the rotating shaft, a second conical gear is meshed with the first conical gear, a second rotating rod is welded on the right side wall of the second conical gear, and the other end of the second rotating rod penetrates through a bearing at the bottom of the inner side wall of the reaction shell;
the number of the ejector rods is two or more, the two or more ejector rods are divided into two groups, and the two groups of ejector rods are respectively welded on the side walls of the first rotating roller and the second rotating roller;
the bottom of the first rubber pad and the base are on the same horizontal line.
The reaction device for preparing the macroporous polyaspartic acid hydrogel comprises a fixing component and a container body, wherein the right side wall of the connecting block is hinged with the outer left side wall of a reaction shell through a pin shaft, a first groove is formed in the top of the connecting block, a second rubber pad is glued to the inner side wall of the first groove, the container body is placed in the first groove, cyclohexane is stored in the container body, an internal thread pipe is arranged on the inner bottom wall of the first groove and is in threaded connection with the outlet end of the container body, a hose penetrates through the bottom wall of the internal thread pipe, and the inner diameter of a first end of the hose is larger than that of a second end of the hose;
a movable bin is arranged at the bottom of the connecting block, a first clamping block and a second clamping block are respectively arranged on the left side and the right side of the hose, a second spring is arranged between the first clamping block and the second clamping block, sliding blocks are arranged on the side walls of the first clamping block and the second clamping block, a sliding rail is fixedly connected to the bottom wall of the movable bin, and the bottom end of the sliding block is slidably connected into the sliding rail;
a first pull rope is arranged on the right side wall of the first clamping block, limiting rods are arranged on the right inner bottom wall and the inner top wall of the movable bin, the first pull rope is lapped on the surfaces of the limiting rods, and the other end of the first pull rope penetrates through a through hole formed in the left side wall of the connecting block and is fixedly connected with a first pull block;
a second pull rope is arranged on the left side wall of the second clamping block, and the other end of the second pull rope penetrates through a through hole formed in the left side wall of the connecting block and is fixedly connected with the middle of the side wall of the first pull block;
the second end of the hose penetrates through the movable bin and is arranged below the connecting block in a protruding mode.
According to the reaction device for preparing the macroporous polyaspartic acid hydrogel, the top of the connecting block is provided with the movable groove, the movable groove is internally provided with the positioning rod, the surface of the positioning rod is sleeved with the third spring, the first end and the second end of the third spring are respectively and fixedly connected with the first limiting block and the second limiting block, the first limiting block is slidably sleeved on the surface of the first end of the positioning rod, and the second limiting block is sleeved on the surface of the second end of the positioning rod;
the first end of the positioning rod penetrates through the connecting block, the left side of the connecting block is provided with a second pull block fixedly connected with through holes, the left side wall of the reaction shell is provided with a second groove, and the second end of the positioning rod is inserted into the second groove.
The technical scheme of the utility model following profitable technological effect has been obtained:
1. the utility model discloses a set up the standing groove with when the staff uses whole reaction unit to vibrate the raw materials, will save the household utensils that have the raw materials and insert on the baffle place downthehole, control through control panel the motor operation drives simultaneously pivot rotation activity first conical gear with under the cooperation of second conical gear, drive first commentaries on classics rod with the second commentaries on classics rod rotation activity under the effect of ejector pin, make the standing groove rocks, thereby can be right the household utensils that store the raw materials in the standing groove vibrate, have improved staff's work efficiency.
2. The utility model discloses a set up the standing groove heating device with the clear water when the staff carries out water-bath heating to the raw materials, will save the household utensils that have the raw materials and peg graft on the baffle place downtheholely, control through control panel heating device is right the baffle with between the heating device the clear water heats for soak and heat the household utensils that have the raw materials in the storage in the clear water are heated, thereby reach the purpose that carries out water-bath heating to the raw materials.
3. The utility model discloses a set up fixed subassembly, when the staff to the storage have cyclohexane the household utensils body when fixing, the pulling the second draws the piece, drives the locating lever breaks away from the second recess to rotatory activity the connecting block will the exit end of household utensils body is pegged graft in the first recess, and with internal thread pipe thread connects together the second draw the piece with under the effect of locating lever, will the connecting block recovery normal position to people can be with the storage have cyclohexane the household utensils body is fixed in the connecting block, prevents the household utensils body falls on the ground.
Drawings
FIG. 1 is a schematic view of a cross-sectional front view of a reaction apparatus for preparing a macroporous polyaspartic acid hydrogel according to the present invention;
FIG. 2 is a schematic front view of a reaction apparatus for preparing a macroporous polyaspartic acid hydrogel according to the present invention;
FIG. 3 is a schematic view of the front cross-sectional structure of a fixing member of a reaction apparatus for preparing a macroporous polyaspartic acid hydrogel according to the present invention;
FIG. 4 is a schematic view of a cross-sectional structure of a connecting block of a reaction apparatus for preparing a macroporous polyaspartic acid hydrogel according to the present invention;
FIG. 5 is a schematic view of the front cross-sectional structure of a third spring in a reaction apparatus for preparing a macroporous polyaspartic acid hydrogel according to the present invention.
The reference numbers in the figures denote: 1-a reaction housing; 2-oscillating assembly; 201-a first rubber mat; 202-a motor; 203-a rotating shaft; 204-a first bevel gear; 205-a first roller; 206-a mandril; 207-second bevel gear; 208-a second rotating stick; 3-placing the groove; 4-a first spring; 5-a separator; 6-a rubber ring; 7-placing holes; 8-clear water; 9-a fixed component; 901-connecting blocks; 902-a first groove; 903-a second rubber pad; 904-vessel body; 905-an internally threaded tube; 906-a hose; 907-active bin; 908-a first clamp block; 909-second spring; 910-a first pull cord; 911-a stop lever; 912-a second pull cord; 913 — a second clamp block; 914-first pull block; 915-a slide block; 916-a slide rail; 917-active groove; 918-positioning rod; 919-a third spring; 920-a first stopper; 921-a second stopper; 922-a second groove; 923-a second pulling block; 10-a third groove; 11-activated carbon; 12-a hinge; 13-a bin gate; 14-a handle; 15-a base; 16-placing a bin; 17-heating means.
Detailed Description
The reaction device for preparing the macroporous polyaspartic acid hydrogel comprises a reaction shell 1, a vibration component 2, a fixing component 9, a placing groove 3 and a heating device 17, wherein the vibration component 2 is located in the middle of the reaction shell 1, the fixing component 9 is hinged to the left side wall of the reaction shell 1 through a pin shaft, a reaction bin is arranged in the reaction shell 1, and the placing groove 3 is located in the reaction bin; the heating device 17 is positioned on the inner bottom wall of the placing groove 3, a partition plate 5 is clamped on the inner side wall of the placing groove 3, clear water 8 is arranged between the partition plate 5 and the heating device 17, the outer side wall of the placing groove 3 is fixedly connected with a first spring 4, and the other end of the first spring 4 is fixedly connected to the inner side wall of the reaction shell 1; a third groove 10 is formed in the top of a boss convexly arranged at the left end of the reaction shell 1, activated carbon 11 is arranged in the third groove 10, and the activated carbon 11 is located under the fixed component 9.
The number of the first springs 4 is two or more, the two or more first springs 4 are divided into two groups, one group of the first springs 4 is positioned between the outer side wall of the placing groove 3 and the inner side wall of the reaction shell 1, the other group of the first springs 4 is positioned between the outer bottom wall of the placing groove 3 and the inner bottom wall of the reaction shell 1, and a placing bin 16 is arranged in the placing groove 3; the surface of the partition board 5 is provided with a placing hole 7, a rubber ring 6 is glued in the placing hole 7, through the arrangement of the placing groove 3, the heating device 17 and the clean water 8, when a worker heats a raw material in a water bath, a vessel storing the raw material is inserted into the placing hole 7 on the partition board 5, the heating device 17 is controlled by a control panel to heat the clean water 8 between the partition board 5 and the heating device 17, so that the vessel storing the raw material and soaked in the heated clean water 8 is heated, the purpose of heating the raw material in the water bath is achieved, the number of the placing holes 7 is two or more, and the placing holes 7 are arranged on the partition board 5; the outer top wall of reaction shell 1 can be dismantled through fixing bolt and be connected with hinge 12, just reaction shell 1 passes through hinge 12 swing joint has door 13, door 13 right side top fixedly connected with handle 14, outer bottom wall fixedly connected with base 15 of reaction shell 1, base 15 is total four, and the equal range is in the outer diapire of reaction shell 1.
The oscillating assembly 2 comprises a first rubber pad 201 and a rotating shaft 203, the rotating shaft 203 is arranged in a bearing in the middle of the bottom wall of the reaction shell 1 in a penetrating manner, the first rubber pad 201 is positioned under the rotating shaft 203, a motor 202 is glued to the top end of the first rubber pad 201, an output shaft of the motor 202 is in driving connection with the bottom end of the rotating shaft 203, a first rotating rod 205 is fixedly connected to the top end of the rotating shaft 203, a top rod 206 is welded to the side wall of the first rotating rod 205, and the top end of the first rotating rod 205 is arranged in the bearing on the inner top wall of the left side of the reaction shell 1 in a penetrating manner; the middle part of the rotating shaft 203 is sleeved with a first conical gear 204, the first conical gear 204 is engaged with a second conical gear 207, the second rotating rod 208 is welded on the right side wall of the second conical gear 207, through the arrangement of the placing groove 3 and the oscillating assembly 2, when a worker oscillates raw materials by using the whole reaction device, a vessel in which the raw materials are stored is inserted into the placing hole 7 on the partition plate 5, the motor 202 is controlled to operate through the control panel, the rotating shaft 203 is driven to rotate, under the cooperation of the first conical gear 204 and the second conical gear 207, the first rotating rod 205 and the second rotating rod 208 are driven to rotate, under the action of the ejector rod 206, the placing groove 3 is made to rock, so that the vessel in which the raw materials are stored in the placing groove 3 is oscillated, and the working efficiency of the worker is improved, the other end of the second rotating rod 208 is arranged in a bearing at the bottom of the inner side wall of the reaction shell 1 in a penetrating manner; the number of the top rods 206 is two or more, the two or more top rods 206 are divided into two groups, and the two groups of top rods 206 are welded on the side walls of the first rotating roller 205 and the second rotating roller 208 respectively; the bottom of the first rubber pad 201 is on the same horizontal line with the base 15.
The fixing component 9 comprises a connecting block 901, the right side wall of the connecting block 901 is hinged to the outer left side wall of the reaction shell 1 through a pin shaft, a first groove 902 is formed in the top of the connecting block 901, a second rubber pad 903 is glued to the inner side wall of the first groove 902, a vessel body 904 is placed in the first groove 902, cyclohexane is stored in the vessel body 904, an internal threaded pipe 905 is arranged on the inner bottom wall of the first groove 902, the internal threaded pipe 905 is in threaded connection with the outlet end of the vessel body 904, a hose 906 is arranged on the bottom wall of the internal threaded pipe 905 in a penetrating mode, and the inner diameter of a first end of the hose 906 is larger than the inner diameter of a second end of the hose 906; a movable bin 907 is arranged at the bottom of the connecting block 901, a first clamping block 908 and a second clamping block 913 are respectively arranged on the left side and the right side of the hose 906, a second spring 909 is arranged between the first clamping block 908 and the second clamping block 913, sliding blocks 915 are arranged on the side walls of the first clamping block 908 and the second clamping block 913, a sliding rail 916 is fixedly connected to the bottom wall of the movable bin 907, and the bottom end of the sliding block 915 is slidably connected into the sliding rail 916; a first pull rope 910 is arranged on the right side wall of the first clamping block 908, a limiting rod 911 is arranged on the right inner bottom wall and the inner top wall of the movable bin 907, the first pull rope 910 is lapped on the surface of the limiting rod 911, and a first pull block 914 is fixedly connected to the other end of the first pull rope 910 through a through hole formed in the left side wall of the connecting block 901; a second pull rope 912 is arranged on the left side wall of the second clamping block 913, and the other end of the second pull rope 912 penetrates through a through hole formed in the left side wall of the connecting block 901 and is fixedly connected with the middle of the side wall of the first pull block 914; the second end of the hose 906 passes through the movable bin 907 and is arranged below the connecting block 901 in a protruding manner; a movable groove 917 is formed in the top of the connecting block 901, a positioning rod 918 is arranged in the movable groove 917, a third spring 919 is sleeved on the surface of the positioning rod 918, a first end and a second end of the third spring 919 are fixedly connected with a first limiting block 920 and a second limiting block 921 respectively, the first limiting block 920 is slidably sleeved on the surface of the first end of the positioning rod 918, and the second limiting block 921 is sleeved on the surface of the second end of the positioning rod 918; a first end of the positioning rod 918 is fixedly connected with a second pulling block 923 by passing through a through hole arranged at the left side of the connecting block 901, the left side wall of the reaction shell 1 is provided with a second groove 922, and by arranging the fixing component 9, when the worker fixes the vessel body 904 storing cyclohexane, the worker pulls the second pulling block 923 to drive the positioning rod 918 to separate from the second groove 922, the movable connecting block 901 is rotated to insert the outlet end of the vessel body 904 into the first groove 902, and is connected with the internal thread pipe 905 by screw thread, under the action of the second pulling block 923 and the positioning rod 918, the connecting block 901 is restored to the original position, therefore, the vessel body 904 storing cyclohexane can be fixed in the connecting block 901, the vessel body 904 is prevented from falling on the ground, and the second end of the positioning rod 918 is inserted in the second groove 922.
In the utility model, the oscillating component 2 positioned in the middle of the reaction shell 1 oscillates the placing groove 3 inside the reaction shell 1, thereby realizing the purpose of oscillating the raw materials in the placing groove 3; the first spring 4 fixedly connected to the side wall of the placing groove 3 provides support for the placing groove 3, and the elasticity of the first spring 4 is utilized to assist the placing groove 3 to vibrate; the cyclohexane is fixed by a fixing component 9 hinged with the reaction shell 1 through a pin shaft, so that a vessel storing the cyclohexane is prevented from falling on the ground, and the active carbon 11 stored in a third groove 10 arranged at the top of a boss convexly arranged at the left end of the reaction shell 1 absorbs the inadvertently dropped cyclohexane, so that the inadvertently dropped cyclohexane is prevented from damaging a human body.
The specific working process is as follows:
when in use, the whole reaction device is firstly placed at a proper position, and SiO with given mass is weighed2Adding nanoparticles and Tween 80 as surfactant into 1mL of ultrapure water, and ultrasonically dispersing the particlesAfter the mixture is uniform, 200mg of linear polyaspartic acid and 20mg of crosslinking agent ethylene glycol diglycidyl ether are added, and the substances are dissolved;
pulling a first pulling block 914, driving a first clamping block 908 and a second clamping block 913 to separate under the cooperation of a first pulling rope 910 and a second pulling rope 912, driving a second spring 909 to extend, so that cyclohexane in the vessel body 904 flows to the hose 906 and drips out of a second end of the hose 906, measuring an oil phase cyclohexane by using a liquid transfer gun, adding the oil phase cyclohexane into a previously prepared water phase in batches, mixing the two phases, then performing oscillation emulsification to obtain a high internal phase emulsion, heating a polymerized water phase by using a water bath at a certain temperature, and volatilizing to remove the oil phase to obtain a porous PASP hydrogel material;
when the vessel body 904 storing cyclohexane is fixed, the second pulling block 923 is pulled to drive the positioning rod 918 to be separated from the second groove 922, the movable connecting block 901 is rotated, the outlet end of the vessel body 904 is inserted into the first groove 902 and is in threaded connection with the internal threaded pipe 905, and the connecting block 901 is restored to the original position under the action of the second pulling block 923 and the positioning rod 918, so that the vessel body 904 storing cyclohexane can be fixed in the connecting block 901 by people, and the vessel body 904 is prevented from falling on the ground;
when the staff uses whole reaction unit to vibrate the raw materials, insert the household utensils that store the raw materials in placing hole 7 on baffle 5, through control panel control motor 202 operation, drive pivot 203 rotation activity simultaneously, under the cooperation of first conical gear 204 and second conical gear 207, drive first commentaries on classics rod 205 and second commentaries on classics rod 208 rotation activity, under the effect of ejector pin 206, make standing groove 3 rock, thereby can vibrate the household utensils that store the raw materials.
It should be understood that the above examples are only for clarity of illustration and are not intended to limit the embodiments. Other variations and modifications will be apparent to persons skilled in the art in light of the above description. And are neither required nor exhaustive of all embodiments. And obvious variations or modifications are possible which remain within the scope of the appended claims.
Claims (5)
1. The reaction device for preparing the macroporous polyaspartic acid hydrogel is characterized by comprising a reaction shell (1), a vibration component (2), a fixing component (9), a placing groove (3) and a heating device (17), wherein the vibration component (2) is positioned in the middle of the reaction shell (1), the fixing component (9) is hinged with the left side wall of the reaction shell (1) through a pin shaft, a reaction bin is arranged in the reaction shell (1), and the placing groove (3) is positioned in the reaction bin;
the heating device (17) is positioned on the inner bottom wall of the placing groove (3), a partition plate (5) is clamped on the inner side wall of the placing groove (3), clear water (8) is arranged between the partition plate (5) and the heating device (17), the outer side wall of the placing groove (3) is fixedly connected with a first spring (4), and the other end of the first spring (4) is fixedly connected to the inner side wall of the reaction shell (1);
the reaction shell (1) is characterized in that a third groove (10) is formed in the top of a boss which is convexly formed at the left end of the reaction shell (1), activated carbon (11) is arranged in the third groove (10), and the activated carbon (11) is located under the fixed component (9).
2. The reaction device for preparing macroporous polyaspartic acid hydrogel as claimed in claim 1, wherein the number of the first springs (4) is two or more, the two or more first springs (4) are divided into two groups, one group of the first springs (4) is located between the outer side wall of the placement tank (3) and the inner side wall of the reaction housing (1), the other group of the first springs (4) is located between the outer bottom wall of the placement tank (3) and the inner bottom wall of the reaction housing (1), and a placement bin (16) is arranged in the placement tank (3);
the surface of the clapboard (5) is provided with placing holes (7), rubber rings (6) are glued in the placing holes (7), the number of the placing holes (7) is two or more, and the placing holes (7) are arranged on the clapboard (5);
reaction housing (1) outer parietal can be dismantled through fixing bolt and be connected with hinge (12), just reaction housing (1) passes through hinge (12) swing joint has door (13), door (13) right side top fixedly connected with handle (14), outer parietal fixedly connected with base (15) of reaction housing (1), base (15) are total four, and wait all to arrange and be in the outer diapire of reaction housing (1).
3. The reaction device for preparing macroporous polyaspartic acid hydrogel as claimed in claim 2, wherein the oscillating assembly (2) comprises a first rubber pad (201) and a rotating shaft (203), the rotating shaft (203) is inserted into a bearing in the middle of the bottom wall of the reaction housing (1), the first rubber pad (201) is located right below the rotating shaft (203), a motor (202) is glued to the top end of the first rubber pad (201), an output shaft of the motor (202) is in driving connection with the bottom end of the rotating shaft (203), a first rotating rod (205) is fixedly connected to the top end of the rotating shaft (203), a top rod (206) is welded to the side wall of the first rotating rod (205), and the top end of the first rotating rod (205) is inserted into a bearing in the top wall of the left side of the reaction housing (1);
a first conical gear (204) is sleeved in the middle of the rotating shaft (203), a second conical gear (207) is meshed with the first conical gear (204), a second rotating rod (208) is welded on the right side wall of the second conical gear (207), and the other end of the second rotating rod (208) penetrates through a bearing at the bottom of the inner side wall of the reaction shell (1);
the number of the top rods (206) is two or more, the two or more top rods (206) are divided into two groups, and the two groups of top rods (206) are respectively welded on the side walls of the first rotating roller (205) and the second rotating roller (208);
the bottom of the first rubber pad (201) and the base (15) are on the same horizontal line.
4. The reaction device for preparing macroporous polyaspartic acid hydrogel of claim 1, characterized in that the fixing component (9) comprises a connecting block (901), the right side wall of the connecting block (901) is hinged with the outer left side wall of the reaction shell (1) through a pin shaft, the top of the connecting block (901) is provided with a first groove (902), a second rubber pad (903) is glued on the inner side wall of the first groove (902), a vessel body (904) is placed in the first groove (902), cyclohexane is stored in the vessel body (904), an internal threaded pipe (905) is arranged on the inner bottom wall of the first groove (902), the internal threaded pipe (905) is in threaded connection with the outlet end of the vessel body (904), a hose (906) penetrates through the bottom wall of the internally threaded pipe (905), and the inner diameter of a first end of the hose (906) is larger than that of a second end;
a movable bin (907) is arranged at the bottom of the connecting block (901), a first clamping block (908) and a second clamping block (913) are respectively arranged on the left side and the right side of the hose (906), a second spring (909) is arranged between the first clamping block (908) and the second clamping block (913), sliding blocks (915) are arranged on the side walls of the first clamping block (908) and the second clamping block (913), a sliding rail (916) is fixedly connected to the inner bottom wall of the movable bin (907), and the bottom end of the sliding block (915) is slidably connected into the sliding rail (916);
a first pull rope (910) is arranged on the right side wall of the first clamping block (908), a limiting rod (911) is arranged on the right inner bottom wall and the inner top wall of the movable bin (907), the first pull rope (910) is lapped on the surface of the limiting rod (911), and a first pull block (914) is fixedly connected to the other end of the first pull rope (910) through a through hole formed in the left side wall of the connecting block (901);
a second pull rope (912) is arranged on the left side wall of the second clamping block (913), and the other end of the second pull rope (912) penetrates through a through hole formed in the left side wall of the connecting block (901) and is fixedly connected with the middle of the side wall of the first pull block (914);
the second end of the hose (906) penetrates through the movable bin (907) and is arranged below the connecting block (901) in a protruding mode.
5. The reaction device for preparing macroporous polyaspartic acid hydrogel according to claim 4, wherein a movable groove (917) is formed at the top of the connecting block (901), a positioning rod (918) is arranged in the movable groove (917), a third spring (919) is sleeved on the surface of the positioning rod (918), a first limiting block (920) and a second limiting block (921) are fixedly connected to the first end and the second end of the third spring (919) respectively, the first limiting block (920) is slidably sleeved on the surface of the first end of the positioning rod (918), and the second limiting block (921) is sleeved on the surface of the second end of the positioning rod (918);
the first end of the positioning rod (918) penetrates through the left side of the connecting block (901) and is fixedly connected with a second pulling block (923), the left side wall of the reaction shell (1) is provided with a second groove (922), and the second end of the positioning rod (918) is inserted into the second groove (922).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202120400719.XU CN214486821U (en) | 2021-02-23 | 2021-02-23 | Reaction device for preparing macroporous polyaspartic acid hydrogel |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202120400719.XU CN214486821U (en) | 2021-02-23 | 2021-02-23 | Reaction device for preparing macroporous polyaspartic acid hydrogel |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN214486821U true CN214486821U (en) | 2021-10-26 |
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ID=78221161
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202120400719.XU Expired - Fee Related CN214486821U (en) | 2021-02-23 | 2021-02-23 | Reaction device for preparing macroporous polyaspartic acid hydrogel |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN214486821U (en) |
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2021
- 2021-02-23 CN CN202120400719.XU patent/CN214486821U/en not_active Expired - Fee Related
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